Waters 600 HPLC Pump Manuals

Manuals and User Guides for Waters 600 HPLC Pump. We have 1 Waters 600 HPLC Pump manual available for free PDF download: User Manual

Waters 600 User Manual

Waters 600 User Manual (258 pages)

multisolvent delivery system

Brand: Waters | Category: Water Pump | Size: 8 MB

Table of Contents

Intended Use
15
Table of Contents
17
Preface

25
Chapter 1 Introduction

29
- Waters 600E System Overview
  29
- Waters 600E System Modules
  31
  - Waters 600 Controller
    31
  - Waters 600E Pump
    34
- Powerline Controller Features
  37
- Gradient Controller Features
  37
- Options and Accessories
  38
Chapter 2 Basic Operation

41
- Powering up the System
  41
  - Powering up IEEE-488 Components
    41
  - Powering up the Stand-Alone 600E System
    44
- Running Diagnostics
  44
  - Powerup Self-Diagnostics
    44
  - Running Extended Diagnostics
    45
- Using the Controller Front Panel
  45
  - Keypad
    46
  - Function Keys
    47
  - Screen Keys
    48
- Comparing Controller Types
  49
  - Powerline Controller Configuration
    50
  - Gradient Controller Configuration
    52
- Powering down the System
  53
Chapter 3 Preparing Your 600E System for Operation

55
- Sparging Eluents
  56
- Priming the Pump
  59
- Daily Routine Operation
  62
- Flushing the System
  63
- Equilibrating the System
  66
- Changing Eluents
  69
  - Adding Fresh Eluent
    69
  - Changing between Incompatible Eluents
    70
Chapter 4 Setting Powerline Controller Operating Parameters

73
Chapter 5 Running Powerline in Direct Control Mode

113
- Setting Run Conditions
  114
  - Setting Pump Parameters
    116
  - Setting External Event Switches
    118
  - Setting Autoinjector Parameters
    119
  - Setting Detector Parameters
    121
- Performing a Direct Control Run
  122
  - Setting the Run Time
    124
  - Downloading Operating Parameters
    124
  - Equilibrating the System
    125
  - Starting a Run
    125
  - Stopping the Pump
    126
  - Aborting a Run
    127
  - Changing Parameters During a Run
    127
- Running a Method from the Direct Control Screen
  127
Chapter 6 Creating Powerline Methods

129
- Creating a Gradient Table
  130
- Creating an Event Table
  139
  - Documenting the Event Table
    140
  - Programming the Event Table
    143
  - Entering Parameter Values in the Event Table
    146
  - Editing the Event Table
    147
- Creating a Detector Table
  147
- Creating a Method Table
  152
  - Method Table Overview
    152
  - Programming the Method Table
    153
  - Entering Parameter Values in the Method Table
    156
  - Editing the Method Table
    158
Chapter 7 Running Powerline Methods

161
- Using an Injector
  161
- Setting Initial Operating Parameters
  164
- Starting a Run
  167
  - Accessing the Operate Methods Screen
    167
  - Downloading Operating Parameters
    169
  - Running a Method
    170
- Modifying Conditions While Running
  171
  - Changing Parameters
    172
  - Holding Conditions Constant
    172
  - Stopping Flow
    172
  - Modifying Gradient, Event, and Detector Tables
    173
  - Modifying the Method Table
    174
  - Aborting the Method
    174
Chapter 8 Setting Gradient Controller Operating Parameters

177
- Setting up the 600 as a Gradient Controller
  178
  - Configuring the Controller Type
    180
  - Communicating with a Data System
    182
- Setting up the 600E Pump
  185
  - Accessing the Pump Setup Screen
    186
  - Setting Pump Setup Parameters
    188
  - Exiting the Pump Setup Screen
    192
Chapter 9 Running Gradient Controller in Isocratic Mode

193
- Setting Run Conditions
  194
  - Setting Pump Parameters
    196
  - Setting External Event Switches
    198
- Performing an Isocratic Run
  199
  - Equilibrating the System
    199
  - Starting a Run
    200
  - Changing Parameters While Running
    200
  - Stopping the Pump
    200
Chapter 10 Creating Gradient Controller Time-Based Tables

201
- Creating a Gradient Table
  201
- Creating an Event Table
  210
  - Documenting the Event Table
    210
  - Programming the Event Table
    213
  - Entering Parameter Values into the Event Table
    216
  - Editing the Event Table
    216
Chapter 11 Running Gradients

217
- Using an Injector
  217
  - Using the Rheodyne 7725I Manual Injector
    217
  - Using a Non-Powerline Autoinjector
    219
- Setting Initial Operating Parameters
  219
- Starting a Run
  222
  - Accessing the Operate Gradient Screen
    222
  - Running a Gradient
    223
- Modifying Conditions While Running
  225
  - Changing Parameters
    225
  - Holding Conditions Constant
    225
  - Stopping Flow
    226
  - Modifying Gradient and Event Tables
    226
  - Switching to Another Table
    227
  - Aborting the Run
    228
Appendix A Specifications

229
Appendix B Eluent Considerations

235
Eluent Considerations

235
- Eluent Compatibility with the 600E System
  235
- Clean Eluent
  239
- B.2 Clean Eluent
  239
- Eluent Miscibility
  240
  - B.3 Eluent Miscibility
    240
  - Eluent Properties Table
    241
  - Using Miscibility Numbers (M-Numbers)
    242
- Head Height
  243
- Eluent Viscosity
  243
- B.4 Head Height
  243
- Eluent Degassing
  244
  - Conditions Affecting Gas Dissolution
    244
  - B.6 Eluent Degassing
    244
  - Eluent Degassing Methods
    246
Appendix C Analysis Plan

249
Index

251

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