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Waters 600 Manuals
Manuals and User Guides for Waters 600. We have
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Waters 600 manual available for free PDF download: User Manual
Waters 600 User Manual (258 pages)
multisolvent delivery system
Brand:
Waters
| Category:
Water Pump
| Size: 8.57 MB
Table of Contents
Intended Use
15
Table of Contents
17
Preface
25
Chapter 1 Introduction
29
Waters 600E System Overview
29
Waters 600E System Modules
31
Waters 600 Controller
31
Waters 600E Pump
34
Powerline Controller Features
37
Gradient Controller Features
37
Options and Accessories
38
Chapter 2 Basic Operation
41
Powering up the System
41
Powering up IEEE-488 Components
41
Powering up the Stand-Alone 600E System
44
Running Diagnostics
44
Powerup Self-Diagnostics
44
Running Extended Diagnostics
45
Using the Controller Front Panel
45
Keypad
46
Function Keys
47
Screen Keys
48
Comparing Controller Types
49
Powerline Controller Configuration
50
Gradient Controller Configuration
52
Powering down the System
53
Chapter 3 Preparing Your 600E System for Operation
55
Sparging Eluents
56
Priming the Pump
59
Daily Routine Operation
62
Flushing the System
63
Flushing the System Fluid Lines
64
Flushing the Rheodyne Manual Injector
64
Purging the Autoinjector
65
Reconnecting the Column after Flushing the System
65
Equilibrating the System
66
Changing Eluents
69
Adding Fresh Eluent
69
Changing between Incompatible Eluents
70
Chapter 4 Setting Powerline Controller Operating Parameters
73
Setting up the 600 as a Powerline Controller
75
Configuring the Controller Type
77
Selecting an Integrator
79
Selecting the Report Type
82
Verifying that Powerline Devices Are Active
89
Setting up the 600E Pump
91
Accessing the Pump Setup Screen
93
Setting Pump Setup Parameters
94
Exiting the Pump Setup Screen
99
Setting up the Autoinjector
99
Accessing the Autoinjector Setup Screen
101
Setting Autoinjector Setup Parameters
102
Exiting the Autoinjector Setup Screen
103
Setting up Dissolution Control
104
Setting up the Detectors
104
Accessing the Detector Setup Screen
107
Setting Detector Setup Parameters
108
Exiting the Detector Setup Screen
111
Chapter 5 Running Powerline in Direct Control Mode
113
Setting Run Conditions
114
Setting Pump Parameters
116
Setting External Event Switches
118
Setting Autoinjector Parameters
119
Setting Detector Parameters
121
Performing a Direct Control Run
122
Setting the Run Time
124
Downloading Operating Parameters
124
Equilibrating the System
125
Starting a Run
125
Stopping the Pump
126
Aborting a Run
127
Changing Parameters During a Run
127
Running a Method from the Direct Control Screen
127
Chapter 6 Creating Powerline Methods
129
Creating a Gradient Table
130
Documenting the Gradient Table
131
Programming the Gradient Table
133
Entering Parameter Values in the Gradient Table
136
Editing the Gradient Table
137
Creating an Event Table
139
Documenting the Event Table
140
Programming the Event Table
143
Entering Parameter Values in the Event Table
146
Editing the Event Table
147
Creating a Detector Table
147
Documenting the Detector Table
147
Programming the Detector Table
148
Entering Parameter Values in the Detector Table
151
Editing the Detector Table
152
Creating a Method Table
152
Method Table Overview
152
Programming the Method Table
153
Entering Parameter Values in the Method Table
156
Editing the Method Table
158
Chapter 7 Running Powerline Methods
161
Using an Injector
161
Using the Rheodyne 7725I Manual Injector
161
Using a Powerline Autoinjector
163
Using a Non-Powerline Autoinjector
163
Setting Initial Operating Parameters
164
Starting a Run
167
Accessing the Operate Methods Screen
167
Downloading Operating Parameters
169
Running a Method
170
Modifying Conditions While Running
171
Changing Parameters
172
Holding Conditions Constant
172
Stopping Flow
172
Modifying Gradient, Event, and Detector Tables
173
Modifying the Method Table
174
Aborting the Method
174
Chapter 8 Setting Gradient Controller Operating Parameters
177
Setting up the 600 as a Gradient Controller
178
Configuring the Controller Type
180
Communicating with a Data System
182
Setting up the 600E Pump
185
Accessing the Pump Setup Screen
186
Setting Pump Setup Parameters
188
Exiting the Pump Setup Screen
192
Chapter 9 Running Gradient Controller in Isocratic Mode
193
Setting Run Conditions
194
Setting Pump Parameters
196
Setting External Event Switches
198
Performing an Isocratic Run
199
Equilibrating the System
199
Starting a Run
200
Changing Parameters While Running
200
Stopping the Pump
200
Chapter 10 Creating Gradient Controller Time-Based Tables
201
Creating a Gradient Table
201
Documenting the Gradient Table
202
Programming the Gradient Table
204
Entering Parameter Values into the Gradient Table
207
Editing the Gradient Table
208
Creating an Event Table
210
Documenting the Event Table
210
Programming the Event Table
213
Entering Parameter Values into the Event Table
216
Editing the Event Table
216
Chapter 11 Running Gradients
217
Using an Injector
217
Using the Rheodyne 7725I Manual Injector
217
Using a Non-Powerline Autoinjector
219
Setting Initial Operating Parameters
219
Starting a Run
222
Accessing the Operate Gradient Screen
222
Running a Gradient
223
Modifying Conditions While Running
225
Changing Parameters
225
Holding Conditions Constant
225
Stopping Flow
226
Modifying Gradient and Event Tables
226
Switching to Another Table
227
Aborting the Run
228
Appendix A Specifications
229
Appendix B Eluent Considerations
235
Eluent Considerations
235
Eluent Compatibility with the 600E System
235
Clean Eluent
239
B.2 Clean Eluent
239
Eluent Miscibility
240
B.3 Eluent Miscibility
240
Eluent Properties Table
241
Using Miscibility Numbers (M-Numbers)
242
Head Height
243
Eluent Viscosity
243
B.4 Head Height
243
Eluent Degassing
244
Conditions Affecting Gas Dissolution
244
B.6 Eluent Degassing
244
Eluent Degassing Methods
246
Appendix C Analysis Plan
249
Index
251
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