Download
Share
Print this page
IKA C 7000 Operating Instructions Manual
  1. Manuals
  2. Brands
  3. IKA Manuals
  4. Laboratory Equipment
  5. C 7000
  6. Operating instructions manual
IKA C 7000 Operating Instructions Manual

IKA C 7000 Operating Instructions Manual

Calorimeter system with cooler
Hide thumbs

Advertisement

Quick Links

Download this manual
IKA C 7000 Operating Instructions Manual

Advertisement

loading
Need help?

Need help?

Do you have a question about the C 7000 and is the answer not in the manual?

Questions and answers

Related Manuals for IKA C 7000

Summary of Contents for IKA C 7000

  • Page 1 Artisan Technology Group is your source for quality new and certified-used/pre-owned equipment SERVICE CENTER REPAIRS WE BUY USED EQUIPMENT • FAST SHIPPING AND DELIVERY Experienced engineers and technicians on staff Sell your excess, underutilized, and idle used equipment at our full-service, in-house repair center We also offer credit for buy-backs and trade-ins •...

  • Page 2: Cooler C 7002

    ® WERKE 30 807 01 a ® Calorimeter System C 7000 with Cooler C 7002 3(5$7,1* ,16758&7,216 Vers. 07 09.07 Reg.-No. 4343-01 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 3 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 4 89 / 336 / CCE e 2006 / 95 / CCE, in accordo ai seguenti regola- menti e documenti: DIN EN IEC 61 010-1 e DIN EN IEC 61 326-1. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 5 Failure to observe this information may result in inaccurate measurement results. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 6: Table Of Contents

    Connecting the mains lead .............. 6-1 Connecting peripherals..............6-1 Switching the system on ..............6-2 Display and control elements ............6-2 Menu structure ................6-4 Configuration of the C 7000 Calorimeter .......... 6-6 Examples of entries................. 6-8 Switching off ................. 6-11 ® -WERKE C 7000 Ver.

  • Page 7: Table Of Contents

    Maintenance ................... 9-1 Recommendations for cleaning ............9-1 0HVVDJHV DQG 7URXEOHVKRRWLQJ   10.1 Messages from the C 7000 Calorimeter ......... 10-1 10.2 Fault without signal from Calorimeter ..........10-4 10.3 Signals from the C 7002 Cooler ............. 10-4 $FFHVVRULHV DQG &RQVXPDEOHV  11.1 Accessories ..................
  • Page 8 ,QWHQGHG SXU LQWHQGHG SXU The C 7000 calorimeter system may only be used to determine the gross calorific SRVH SRVH value of solid and liquid materials in accordance with DIN 51900 and ISO 1928. For this purpose, use only original IKA®...

  • Page 9: Maintenance

    An individual application is understood here to mean a series of experiments that are performed under roughly the same conditions in terms of pressure and tem- perature Experiment autoclaves must be operated in special chambers (C 7000). 5HSHDWHG WHVWV The decomposition vessel must be subject to repeated tests (internal tests and pressure tests) by a person with professional training.
  • Page 10 GDQJHU WKRVH ZRUNLQJ ZLWK LW RU WKLUG SDUWLHV You can obtain a copy of the pres- sure vessel regulation from Carl Heymann Verlag or Beuth Verlag. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 11 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 12: Accessories

     :DUUDQW\ In accordance with IKA warranty conditions, the warranty period is 12 months. For claims under the warranty please contact your local dealer. You may also send the machine direct to our works, enclosing the delivery invoice and giving reasons for the claim.
  • Page 13  8VHU 1RWHV 3DJH   :DUUDQW\ DQG /LDELOLW\ ® Please read through these Operating Instructions attentively. IKA only accepts responsibility for the safety, reliability and performance of the device if: • the unit has been used in accordance with the operating instructions;...
  • Page 14 3DJH   6\VWHP )HDWXUHV The C 7000 calorimeter is used for the routine determination of the gross calorific value of solid and liquid substances. The system accessories ensure that it can be individually adapted to laboratory tasks (see also Section 11).
  • Page 15 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 16: Installation Location

    30 bar is also required. A shut-off valve for the oxygen supply must be in- stalled. Observe the instructions on handling oxygen given in Section 1 "For your safety”. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 17: Unpacking

    &  &  %DVLF YHUVLRQ %DVLF YHUVLRQ VHW  VHW  Main unit C 7000 including - Mains cable - Electrical fuses - Benzoic acid C 723 - Carrying and venting handle C 7010.8 for decomposition vessel - Operating instruction...
  • Page 18 PC connection, RS 232 Balance connection RS 232 Printer connection, Centronics Fuses Socket for mains cable &  with main fuse 5HDU YLHZ ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 19 Button for manually opening and closing &RROHU &  the cooling jaws )URQW YLHZ Cooling jaws ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 20 C 7002 is connected using the cable supplied to the calorimeter C 7000 (see illustrations Cooler C 7002 Rear view, Position 2, and C 7000 Rear view, Position 3). During the cooling operation, the decomposition vessel is cooled to the temperature of the measuring cell.
  • Page 21 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 22 The standard gross calorific value is then determined from the measured value and the analysis data. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 23 7.2 min. main test) The C 7000 calorimeter is designed for an energy input of up to 30 000 J, and oper- ates reliably in ambient temperatures between 18 ° C and 30 ° C. For good meas- urement results, temperature variations must be avoided.
  • Page 24 5HSURGXFLELOLW\ > @ (QHUJ\ LQSXW  - 3UHWHVW GXUDWLRQ >PLQ@ 5HSURGXFLELOLW\ > @ 3UHWHVW GXUDWLRQ  PLQ (QHUJ\ LQSXW >-@ ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 25 In most cases, an additional combus- tion aid is not required, because the crucible itself fulfils this role. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 26 The acid content of this solution can be determined using suitable equipment. ® You can obtain details of suitable equipment for the purpose from IKA or from your authorised dealer.  &RPSOHWH &RPEXVWLRQ To determine the gross calorific value correctly, it is of fundamental importance that the sample has burnt completely.
  • Page 27 RI WKH V\VWHP PXVW EH GHWHUPLQHG ZLWK HDFK YHVVHO For more detailed information on calibration, please refer to the relevant standards. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 28 3DJH   &RPPLVVLRQLQJ Once the components of the C 7000 calorimeter have been unpacked and brought to the location chosen for the instrument (see Chapter 3, Section 3.2 "Installation Location"), the mains lead and peripherals can be connected.  &RQQHFWLQJ WKH PDLQV OHDG...
  • Page 29 - p . o u t p u t d e l . =RQHV RI /&' GLVSOD\ ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 30 SUHVVLQJ PHP VDYH 4. FWUO EXWWRQ: the FWUO button is used in conjunction with number keys to enter spe- cial functions. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 31: Menu Structure

     0HQX VWUXFWXUH The menu structure of the C 7000 calorimeter comprises three main menus, PHQX , PHQX , and PHQX , which have the following functions: PHQX  Entry of pre- and post-test parameters, output and erasure of tests.
  • Page 32 3DJH  MENU STRUCTURE FOR C 7000 CALORIMETER PHQX  SUHSDU ¡ £ ¢ Entry of pre-test parameters DIWHUS ¡ ¥ ¤ Entry of post-test parameters RXWSXW ¡ ¥ ¦ Data output /&' ¡ £ ¢ Shows test data on LCD-display IUHH ¡...
  • Page 33 The parameters for the balance must be taken from the balance manual. For the C 7000 calorimeter, the sub-menu EDODQFH contains the following inter- face parameters (the preset values are in bold type): EDXGUDWH...
  • Page 34 100 milliseconds. However, if combustion is incomplete, first check the connections of the ignition wire to the electrodes in the decomposition ves- sel. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 35 Setting the time interval for output of results • Configuration for a balance All three examples assume that the C 7000 calorimeter has been switched on, and that PHQX  of the main menu is shown in the LCD-display: m e n u 1...
  • Page 36 . c a l c u l . u n i t p r e . t i m e ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 37 . P C b a l a n c e d a t e t i m e ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 38 PHQXV PHQX  PHQX  RU PHQX  Switch off the calorimeter and the cooler by operating their mains switches. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 39 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 40 Fill the decomposition vessel manually with oxygen at 30 bar, quality 3.5, using the ® C 48 oxygen filling station. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 41 0HDVXUHPHQW In the C 7000 calorimeter, measurement is fully automatic. &RROLQJ The decomposition vessel is removed from the C 7000 calorimeter and placed in the C 7002 cooler, where it is automatically cooled to the temperature of the calorimeter. 9HQW The decomposition vessel is vented using the C 7010.8 vent handle or venting sta-...
  • Page 42 5HFRPPHQGDWLRQV IRU FDOLEUDWLRQ • At a starting temperature of 25 ° C, the C 7000 calorimeter has a maximum tem- perature increase of 25 K. For accurate results, a combustion test should yield a temperature increase of approximately 20 Kelvin. If you do not use benzoic acid for calibration, the quantity of material should be adjusted to meet this condition.
  • Page 43 3, conductors II and III must be separated. Code number Conductors to be separated ⊗ ⊗ ⊗ ⊗ ⊗ ⊗ ⊗ ⊗ ⊗ ⊗ ⊗ ⊗ ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 44 Note in this regard Operating Instructions C 7010 or C 7012. The C 7000 calorimeter is a precision instrument for routine measurement of the gross calorific value of solid and liquid substances. Accurate measurement is only possible if the all the individual steps in a test are carried out with care.
  • Page 45 HWF  ZH UHFRPPHQG WKDW ZDWHU LV DOZD\V DGGHG :KHQ ZRUNLQJ ZLWK VXEVWDQFHV FRQWDLQLQJ KDORJHQV GHFRPSRVLWLRQ YHVVHO 6XEVWDQFHV FRQWDLQLQJ &  PXVW EH XVHG KDORJHQV ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 46 You can now load the sample into the decomposition vessel. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 47 C 14, because the crucible is then in di- rect contact with the ignition wire. 6HFXULQJ WKH FRWWRQ WKUHDG Cotton thread ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 48 This ensures that during the ignition phase the burning thread falls on the sample and ignites it. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 49 Place the union nut onto the lower section and tighten by hand. The decomposition vessel can now be filled. ® Finally, the decomposition vessel is filled with oxygen at 30 bar using the C 48 IKA oxygen filling station. Follow the operating instructions for the C 48 oxygen filling station.
  • Page 50 VXSSOLHG E\ WKH FRWWRQ WKUHDG PXVW EH DGGHG PDQXDOO\ button. The enquiry VDPSOH PDVV appears in the LCD- ↵ Confirm by pressing the display. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 51: Corrections

    A charge-related pre-setting in the order of 26450 J/g will be displayed. This is the ® calorific value of the benzoic acid tablets supplied by IKA . If you are going to use a different substance for calibration, use the key panel to enter the correct value; the ↵...
  • Page 52 Pressing the button starts the calibration or calorific value determination. From now on, the C 7000 calorimeter takes control. The measurement process is made up of a pre-test and the main test. The current phase of the test is shown on the LCD-display.

  • Page 53: Calibration

    In the second line of the LCD-display, the enquiry PHP VDYH appears briefly. Wait until this enquiry disappears again. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 54 Combustion residues in the crucible, e.g. carbon or ash, must also be wiped off carefully with an absorptive, lint-free cloth. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 55 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 56 The individual data for date, sample code and sample status are logically linked by an AND relationship. This means that only tests that fulfil all three specified criteria will be selected. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 57 [ is the number of tests still free. An acoustic signal sounds at the same time. Acknowledge this message by pressing the button. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 58 LCD-display. This is to prevent values being changed unintentionally. ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 59: Evaluation Of Tests

    The sub-menu DIWHUS has input fields for parameters which are dependent on the calculation mode selected. Parameters that are determined with the sample in the ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 60 Calculation modes: FRDO  W FRDO  W DVK DQ Percentage of ash. Calculation modes: FRDO  W FRDO  W ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 61 EXWWRQ blinks to indicate the end of the simu- entered. The green LED near the EXWWRQ, and exit this program. lated test. Acknowledge this with the ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 62 You can obtain further information direct from our Service De- partment. )RU PDLQWHQDQFH RI WKH GHFRPSRVLWLRQ YHVVHO VHH WKH & &  RSHUDW LQJ LQVWUXFWLRQV  5HFRPPHQGDWLRQV IRU FOHDQLQJ ® ® Clean your IKA instrument only with these IKA -approved cleaning agents: &RQWDPLQDQW &OHDQLQJ DJHQW • Dyes Isopropanol •...
  • Page 63 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 64 3DJH   0HVVDJHV DQG 7URXEOHVKRRWLQJ The C 7000 calorimeter is subjected to stringent quality checks during manufacture, should malfunctions occur despite this care, you will find in this section a selection of corrective measures for dealing with a range of fault situations. Most messages and fault indications appear on the LCD-display.
  • Page 65 PHPRU\ IRU WHVWV IXOO The available memory is full Erase tests no longer needed (PHQX , sub-menu GHO). (100 tests). ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 66 Possibly too many consumers are supply has been detected. connected to a single socket, which has caused a brief voltage drop. Connect C 7000 to a separate socket. 37 SDUDPHWHUV PLVVLQJ A test can only be carried out Enter pre-test parameters.
  • Page 67 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 68 Benzoic acid tablets (50 pieces, ca. 25 g) C 14 Combustible crucibles (100 pieces) C 15 Paraffin strips (600 pieces) ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 69 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 70 Cooling power (only Peltier elements) 80 W (with cooling water supply at 2 l/min) Water inlet pressure max. 9 bar ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 71 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...

  • Page 72: Recommendations For Calibration

    Heat capacity .........7-2 Time ..........6-6 Heat of solution...... 5-5, 7-5 Highly volatile substances....7-5 Water ..........5-1 Water addition....... 7-5 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 73 ® -WERKE C 7000 Ver. 07 09.07 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 74 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 75 Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com...
  • Page 76 Artisan Technology Group is your source for quality new and certified-used/pre-owned equipment SERVICE CENTER REPAIRS WE BUY USED EQUIPMENT • FAST SHIPPING AND DELIVERY Experienced engineers and technicians on staff Sell your excess, underutilized, and idle used equipment at our full-service, in-house repair center We also offer credit for buy-backs and trade-ins •...

This manual is also suitable for:

C 7002