Page 1 Agilent 1290 Infinity Quaternary Pump User Manual Agilent Technologies...
Page 2 (June 1987) or any equivalent agency regu- lation or contract clause. Use, duplication or disclosure of Software is subject to Agi- lent Technologies’ standard commercial license terms, and non-DOD Departments and Agencies of the U.S. Government will 1290 Infinity Quaternary Pump User Manual...
Page 3 3 Installing the Module This chapter gives information about the preferred stack setup for your system and the installation of your Agilent 1290 Infinity Quaternary Pump. 4 Using the Module This chapter explains the operational parameters of the Agilent 1290 Infinity Quaternary Pump.
Page 4 In This Guide... 8 Test Functions and Calibrations This chapter describes the tests for the module. 9 Maintenance This chapter describes the maintenance of the Agilent 1290 Infinity Quaternary Pump. 10 Parts and Materials This chapter provides information on parts for maintenance.
Page 5: Table Of Contents
Setting up the Pump with the Instrument Control Interface Flushing the Filter Purging the Pump Solvent Information Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Algae Growth in HPLC Systems 1290 Infinity Quaternary Pump User Manual...
Page 6 Replacing the Inlet Valve Replacing the Outlet Valve Removing the Jet Weaver Installing the Jet Weaver Replacing the Seal Wash Pump Replacing the Multi-Channel Gradient Valve (MCGV) Releasing a Stuck Inlet Valve Remove the Pump Head Assembly 1290 Infinity Quaternary Pump User Manual...
Page 7 Multi Purpose Valve Solvent Cabinet Cover Parts Leak Parts Accessory Kit HPLC System Tool Kit 11 Identifying Cables Cable Overview Analog cables Remote Cables BCD Cables CAN/LAN Cable RS-232 Cable Kit Agilent 1200 Module to Printer 1290 Infinity Quaternary Pump User Manual...
Page 8 Dynamic Host Configuration Protocol (DHCP) Link Configuration Selection Manual Configuration PC and User Interface Software Setup Setup 14 Appendix General Safety Information Waste Electrical and Electronic Equipment (WEE) Directive Radio Interference Sound Emission Agilent Technologies on Internet 1290 Infinity Quaternary Pump User Manual...
Page 9 1290 Infinity Quaternary Pump User Manual Introduction Features Overview of the Quaternary Pump Operating Principle Positions of the Multi Purpose Valve System Overview Leak and Waste Handling This chapter gives an introduction to the module, instrument overview and internal connectors.
Page 10: Introduction Features
• Fast defill function for improved intake and delivery performance. • Two pistons in series design for increased reliability. • High resolution piston movement control for smooth and reliable motion. For specifications, see “Performance Specifications” on page 26. 1290 Infinity Quaternary Pump User Manual...
Page 11: Overview Of The Quaternary Pump
Jet Weaver high-performance mixer, automatic back-flushing of the optional inline filter or for diagnostic. The Agilent 1290 Infinity Quaternary Pump is suitable for a wide range of columns and HPLC und UHPLC applications starting from typical 250 x 4.6 mm HPLC columns going down to high resolution 50 x 2.1 mm UHPLC columns and can be used in a flow range between 0.05 –...
Page 12: Operating Principle
A high resolution encoder unit is attached to the pump drives, which divides a single turn into 65000 steps. Each step corresponds to a volume of about 300 pL, which allows an extremely precise control. 1290 Infinity Quaternary Pump User Manual...
Page 13 Introduction Operating Principle Figure 1 The hydraulic path 1290 Infinity Quaternary Pump User Manual...
Page 14: Positions Of The Multi Purpose Valve
Multi Purpose Valve. The flow leaves the valve through port 4 to the system (autosampler etc.). Figure 2 Valve position in normal operating mode without mixer 1290 Infinity Quaternary Pump User Manual...
Page 15 Introduction Positions of the Multi Purpose Valve Purge Mode In purge mode, the flow is diverted to the waste container. Figure 3 Valve position in purge mode 1290 Infinity Quaternary Pump User Manual...
Page 16 In this mode, the flow passes an optional Jet Weaver and the optional inline filter. This configuration is recommended for special applications which require an increased mixing efficiency. Figure 4 Valve position in normal operating mode with Jet Weaver 1290 Infinity Quaternary Pump User Manual...
Page 17 7. Figure 5 Valve position in filter flush mode Damage to the valve C AU T I O N ➔ Use the filter flush mode only if the optional inline filter is installed. 1290 Infinity Quaternary Pump User Manual...
Page 18: System Overview
System Overview System Overview Leak and Waste Handling The 1200 Infinity Series has been designed for safe leak and waste handling. It is important that all security concepts are understood and instructions are carefully followed. 1290 Infinity Quaternary Pump User Manual...
Page 19 Introduction System Overview Figure 6 Leak and waste handling concept (overview - typical stack configuration as an example) 1290 Infinity Quaternary Pump User Manual...
Page 20 The waste tube of the purge valve (6) guides solvents to waste. The waste tube connected to the leak pan outlet on each of the bottom instruments (7) guides the solvent to a suitable waste container. 1290 Infinity Quaternary Pump User Manual...
Page 21: Site Requirements And Specifications
1290 Infinity Quaternary Pump User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter provides information on environmental requirements, physical and performance specifications. Agilent Technologies...
Page 22: Site Requirements
➔ Make sure the power connector of the instrument can be easily reached and unplugged. ➔ Provide sufficient space behind the power socket of the instrument to unplug the cable. 1290 Infinity Quaternary Pump User Manual...
Page 23 Never use the power cords that Agilent Technologies supplies with this instrument for any other equipment. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. Absence of ground connection WA R N I N G The absence of ground connection can lead to electric shock or short circuit.
Page 24 Do not store, ship or use your module under conditions where temperature fluctuations could cause condensation within the module. ➔ If your module was shipped in cold weather, leave it in its box and allow it to warm slowly to room temperature to avoid condensation. 1290 Infinity Quaternary Pump User Manual...
Page 25: Physical Specifications
Operating altitude Up to 2000 m (6562 ft) Non-operating altitude Up to 4600 m (15092 ft) For storing the module Safety standards: Installation category II, Pollution degree 2 For indoor use only. IEC, CSA, UL 1290 Infinity Quaternary Pump User Manual...
Page 26: Performance Specifications
1 – 99 % or 5 µL/min per channel, whatever is greater. Composition precision <0.15 % RSD, or 0.02 min SD, whatever is Based on retention time greater (1 mL/min). at constant room temperature 1290 Infinity Quaternary Pump User Manual...
Page 27 Electronic records of maintenance and errors. Housing All materials recyclable. 1290 Infinity Quaternary Pump User Manual...
Page 28 Site Requirements and Specifications Performance Specifications 1290 Infinity Quaternary Pump User Manual...
Page 29: Installing The Module
Removing the Transport Foam Installing the Pump Flow Connections to the Pump Installation of Seal Wash Function This chapter gives information about the preferred stack setup for your system and the installation of your Agilent 1290 Infinity Quaternary Pump. Agilent Technologies...
Page 30: Unpacking The Module
For parts identification please check the illustrated parts breakdown in “Parts and Materials” on page 215. Please report any missing or damaged parts to your local Agilent Technologies sales and service office. 1290 Infinity Quaternary Pump User Manual...
Page 31: Optimizing The Stack Configuration
Installing the Module Optimizing the Stack Configuration Optimizing the Stack Configuration If your module is part of a complete Agilent 1290 Infinity Liquid Chromatograph, you can ensure optimum performance by installing the following configurations. These configurations optimize the system flow path, ensuring minimum delay volume.
Page 32 Installing the Module Optimizing the Stack Configuration Figure 7 Recommended stack configuration for 1290 Infinity with quaternary pump (front view) 1290 Infinity Quaternary Pump User Manual...
Page 33 Installing the Module Optimizing the Stack Configuration Figure 8 Recommended stack configuration for 1290 Infinity with quaternary pump (rear view) 1290 Infinity Quaternary Pump User Manual...
Page 34: Two Stack Configuration
A slightly longer capillary is required between the pump and autosampler. (See Figure 9 on page 34 and Figure 10 page 35). Figure 9 Recommended two stack configuration for 1290 Infinity with quaternary pump (front view) 1290 Infinity Quaternary Pump User Manual...
Page 35 Installing the Module Optimizing the Stack Configuration Figure 10 Recommended two stack configuration for 1290 Infinity with quaternary pump (rear view) 1290 Infinity Quaternary Pump User Manual...
Page 36: Installation Information On Leak And Waste Handling
A printed copy of the guideline has been shipped with the solvent cabinet, electronic copies are available on the Internet. Recommendations for Solvent Cabinet N O T E For details, see the usage guideline for the Agilent 1200 Infinity Series Solvent Cabinets. 1290 Infinity Quaternary Pump User Manual...
Page 37 Leak pan's outlet port (A), leak funnel (B) and corrugated waste tube (C) Waste tube of the sampler’s needle wash Condense drain outlet of the autosampler cooler Waste tube of the purge valve Waste tube 1290 Infinity Quaternary Pump User Manual...
Page 38 ➔ Do not bend tubes. ➔ Do not immerse tube end in waste liquid. ➔ Do not intubate tubes in other tubes. ➔ For correct tubing follow instructions on label attached to the module. 1290 Infinity Quaternary Pump User Manual...
Page 39 Installing the Module Installation Information on Leak and Waste Handling Figure 12 Warning label (illustration for correct waste tubing) 1290 Infinity Quaternary Pump User Manual...
Page 40: Removing The Transport Foam
Installing the Module Removing the Transport Foam Removing the Transport Foam Open the front cover of the module. Carfully remove the protective foam. Close the front cover. 1290 Infinity Quaternary Pump User Manual...
Page 41: Installing The Pump
1 Place the module on the bench in a horizontal position. 2 Ensure the power switch on the front of the module is OFF (switch stands out). Figure 13 Front view of the quaternary pump 1290 Infinity Quaternary Pump User Manual...
Page 42 Figure 14 Rear view of the quaternary pump In an Agilent 1290 Infinity System, the individual modules are connected by CAN cables. N O T E An Agilent 1200 Series Instant Pilot can be connected to the CAN bus of any module.
Page 43: Flow Connections To The Pump
MCGV, pump heads, pressure sensor, and Multi Purpose Valve. This section describes the installation of additional flow connections. Parts required Description Other modules G4220-68755 Accessory Kit 5067-4644 Solvent Cabinet Kit 1290 Infinity Pump Preparations Pump is installed in the LC system. 1290 Infinity Quaternary Pump User Manual...
Page 44 5 Connect the inlet tubes of the bottle-head assemblies to the inlet connectors A to D at the left hand side of the vacuum degasser. Fix the tubes in the tubing grommets of the pump. 1290 Infinity Quaternary Pump User Manual...
Page 45 6 Connect the capillary from the autosampler to port 4 of the Multi Purpose Valve. 7 Connect the waste tubing to port 7 of the Multi Purpose Valve and place it in your waste system. 1290 Infinity Quaternary Pump User Manual...
Page 46 Installing the Module Flow Connections to the Pump 8 If the pump is not part of an Agilent 1290 Infinity system stack or placed on the bottom of a stack, connect the waste tube to the waste outlet of the pump leak handling system.
Page 47: Installation Of Seal Wash Function
Installation of Seal Wash Function Installation of Seal Wash Function The 1290 Infinity Quaternary Pump has a built-in seal wash function. The Seal Wash Function is recommended when using buffers or other non-volatile solvents or additives that could deposit on pistons and seals. It is used for regularly cleaning these parts automatically.
Page 48 Installing the Module Installation of Seal Wash Function 1290 Infinity Quaternary Pump User Manual...
Page 49: Using The Module
The Pump User Interface (Dashboard Panel) Control Settings Method Parameter Settings Flushing the Filter Purging the Pump Solvent Information Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Normal Phase Applications Solvent Handling Agilent Technologies...
Page 50 Using the Module Installation of Seal Wash Function Algae Growth in HPLC Systems How to Prevent and-or Reduce the Algae Problem This chapter explains the operational parameters of the Agilent 1290 Infinity Quaternary Pump. 1290 Infinity Quaternary Pump User Manual...
Page 51: Magnets
Using the Module Magnets Magnets This stack exemplarily shows the magnets' positions in the modules. 1290 Infinity Quaternary Pump User Manual...
Page 52: Turn On/Off
Using the Module Turn on/off Turn on/off Power switch: On Turn instrument On/Off with the control software. Power switch: Off 1290 Infinity Quaternary Pump User Manual...
Page 53 Using the Module Turn on/off 1290 Infinity Quaternary Pump User Manual...
Page 54: Status Indicators
5. Resident mode (blinking) - for example during update of main firmware. 6. Bootloader mode (fast blinking). Try to re-boot the module or try a cold-start. Then try a firmware update. 1290 Infinity Quaternary Pump User Manual...
Page 55: Leak And Waste Handling
N O T E For details, see the usage guideline for the Agilent 1200 Infinity Series Solvent Cabinets. For details on correct installation, see section Installation Information on Leak and Waste Handling in the service manual. 1290 Infinity Quaternary Pump User Manual...
Page 56: Best Practices
• Purge each channel with fresh solvent at 2.5 – 3 mL/min for 5 min. • Equilibrate your system with composition of your application for 15 min. Use conditioning for 1290 Infinity II Pumps and G7104C. Weekly tasks • Change seal wash solvent (10 % / 90 % isopropanol/water) and bottle.
Page 57: Power Up / Shut-Down The Pump
• Equilibrate your system with composition of your application for 15 min. Use conditioning for 1290 Infinity II Pumps and G7104C. Long-term shut-down of the system • Flush system with water to remove buffer.
Page 58 The seal wash function regularly cleans these parts automatically. Seal Wash Dialog in OpenLAB Software (1290 Infinity Pumps only): • Seal Wash settings are NO method parameters • Find dialog under Control •...
Page 59: How To Deal With Solvents
• Use lower channels (A and/or D) for buffer solutions. • Regularly flush all MCGV channels with water to remove possible salt deposits. • Check compatibility of buffers and organic solvents to avoid precipitation. 1290 Infinity Quaternary Pump User Manual...
Page 60: Optional Inline Filter
• exchange the filter frit on a regular basis. Damage to the valve C AU T I O N ➔ Use the filter flush mode only if the optional inline filter is installed. See Technote G7167-90130 for further reference. 1290 Infinity Quaternary Pump User Manual...
Page 61: Setting Up The Pump With The Instrument Control Interface
The Quaternary Pump configuration parameters are in two sections: • Communication • Options Communication: The parameters in this dialog box are detected automatically during autoconfiguration. • Device name, • Type ID, • Serial number, • Firmware revision, • Connection settings 1290 Infinity Quaternary Pump User Manual...
Page 62 Configure Solvent Type Catalogs: Displays the Solvent Type Catalogs dialog box, which allows you to import and export solvent calibration data. See “Importing Solvent Calibration Tables” on page 99. Please refer to the online help of your user interface for more detailed information. 1290 Infinity Quaternary Pump User Manual...
Page 63: The Pump User Interface (Dashboard Panel)
The pressure setpoints. The red line shows the current maximum pressure limit; the green area shows the current pressure (also shown as text). The current solvent flow rate (in mL/min) is displayed above the pressure display. 1290 Infinity Quaternary Pump User Manual...
Page 64 “Instrument Configuration” on page 61). Tuning Indicates the tuning efforts of 1290 Infinity pumps. For pumps operating as expected, the signal should stay in a range of -1 to +1 within the full scale of -2 to +2. Pressure Limit The current maximum pressure limit.
Page 65 Allows you to flush a clogged inline filter, which is connected to the Multi Purpose Valve, see “Filter Flush Mode” page 17. Use the pump self-test for checking the filter back pressure. Do not use this option if no filter is installed! 1290 Infinity Quaternary Pump User Manual...
Page 66: Control Settings
• On all the time: The seal wash is active when the pump is on or in standby mode. Automatic Turn On Module can be turned on at a specified date/time. This feature can only be used if the module power switch is turned on. 1290 Infinity Quaternary Pump User Manual...
Page 67 Conditioning may be necessary if the pump may contain air, for example after running out of solvent, after a long period of standby or after service or repair. 1290 Infinity Quaternary Pump User Manual...
Page 68: Method Parameter Settings
• Used: Mark this check box if you want to use this solvent or blend in the method. • %: Enter the percentage of the solvent or blend in this field. • Name: Type a name for the solvent or blend in this field. 1290 Infinity Quaternary Pump User Manual...
Page 69 70 ISET Set the ISET parameters in this dialog box. For further information on ISET, please refer to the Online Help or to the Agilent 1290 Infinity with ISET User Manual (p/n G4220-90313). 1290 Infinity Quaternary Pump User Manual...
Page 70 You can set a limit on the rate of change of the solvent flow to protect your Gradient 1000.000 mL/min/min analytical column. You can set individual values for Flow ramp up and Flow in steps of ramp down. 0.001 mL/min/min Default value: 100.000 mL/min/min 1290 Infinity Quaternary Pump User Manual...
Page 71 • Change Solvent Composition - You can only use solvents, which have been enabled in the solvents section. • Function centric view - This checkbox allows you displaying parameter changes instead of a time table. 1290 Infinity Quaternary Pump User Manual...
Page 72 Final conc. For the relationship of stock concentration and concentration in the mixture, the composition accuracy needs to be considered (see “Performance Specifications” on page 26). • Conc. unit: The concentration can be defined as mM (mmol/L) or as %. 1290 Infinity Quaternary Pump User Manual...
Page 73: Flushing The Filter
Using the Module Flushing the Filter Flushing the Filter For highest performance and robustness, the 1290 Infinity Quaternary Pump uses 3 solvent filters: 1 Solvent inlet filter, 20 μm pore size (5041-2168) as part of Bottle Head Assembly (G4220-60007) have a large pore size of about 20 μm and filter out particles before they reach the pump.
Page 74 Using the Module Flushing the Filter In the instrument control panel of Agilent user interfaces, use the context menu and select Flush Filter On, see also “Context Menu” on page 65. 1290 Infinity Quaternary Pump User Manual...
Page 75: Purging The Pump
The pump should never be used for priming/purging empty tubings (never let the pump N O T E run dry). Use a syringe to draw enough solvent for completely filling the tubings to the pump inlet before continuing to prime with the pump. 1290 Infinity Quaternary Pump User Manual...
Page 76 6 Observe the pressure fluctuations. The system is air free as soon as the pressure is stable. 7 Change solvents and column according to the analytical conditions and purge the system to change solvents. 1290 Infinity Quaternary Pump User Manual...
Page 77: Solvent Information
• Avoid or minimize the use of solvents that may corrode parts in the flow path. Consider specifications for the pH range given for different materials like flow cells, valve materials etc. and recommendations in subsequent sections. 1290 Infinity Quaternary Pump User Manual...
Page 78 UHMW-PE, SST Pressure sensor Multi Purpose Valve Polyimide, SST, DLC Ultra clean tubings are available for the use with high-end MS detectors. They are also compatible to THF. Inlet Weaver, Jet Weaver, Heat Exchanger 1290 Infinity Quaternary Pump User Manual...
Page 79 (cresols, salicylic acid etc.). When used above room temperature, PEEK is sensitive to bases and various organic solvents, which can cause it to swell. Under such conditions normal 1290 Infinity Quaternary Pump User Manual...
Page 80 Polyethylene (PE) Agilent uses UHMW (ultra-high molecular weight)-PE/PTFE blends for yellow piston and wash seals, which are used in 1290 Infinity pumps, 1290 Infinity II pumps, the G7104C and for normal phase applications in 1260 Infinity pumps. Polyethylene has a good stability for most common inorganic solvents including acids and bases in a pH range of 1 to 12.5.
Page 81 (about pH 0.1) at room temperature is about 13 μm/year. At room temperature, titanium is resistant to concentrations of about 5 % sulfuric acid (about pH 0.3). Addition of nitric acid to hydrochloric or sulfuric acids 1290 Infinity Quaternary Pump User Manual...
Page 82 Zirconium Oxide is inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. Platinum/Iridium Platinum/Iridium is inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. 1290 Infinity Quaternary Pump User Manual...
Page 83 DMF (dimethyl formamide). Sapphire, Ruby and Al -based ceramics Sapphire, ruby and ceramics based on aluminum oxide Al are inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. 1290 Infinity Quaternary Pump User Manual...
Page 84: Solvent Recommendation For Agilent 1290 Infinity And 1290 Infinity Ii And 1260 Infinity Ii Flexible Pumps
Using the Module Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps While the Agilent 1290 Infinity, 1290 Infinity II, and 1260 Infinity II Flexible Pumps guarantee a high performance with a wide variety of solvents, other solvents may cause harm to the pump or to the (U)HPLC system.
Page 85: Normal Phase Applications
Using the Module Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Normal Phase Applications Valves for Normal Phase Applications Current passive inlet valves and outlet ball valves used with Agilent Infinity and Infinity II pumps do not work well while running nonpolar solvents for normal phase applications (for example, hexane and heptane).
Page 86: Solvent Handling
Using the Module Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Table 7 Recommended valves for normal phase applications Binary or High Speed Pumps Quaternary or Flexible Pumps Inlet valves 1290 Infinity Inlet Valve Type N...
Page 87 Using the Module Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Handling of Buffers The following recommendations should be observed when using buffer solutions: • Buffers and aqueous solutions are possible sources of algae contamination, for avoiding related problems, please read “Algae Growth in HPLC...
Page 88 Using the Module Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Handling of Acetonitrile Acetonitrile is a solvent that is frequently used in reversed-phase chromatography. Despite of its common use, it can be a source of issues if not handled correctly.
Page 89: Algae Growth In Hplc Systems
• Use the amber solvent bottle ( Solvent bottle, amber, 1000 mL (9301-6526)) supplied with the instrument for your aqueous mobile phase. • If possible add a few mg/L sodium azide or a few percent organic solvent to the aqueous mobile phase. 1290 Infinity Quaternary Pump User Manual...
Page 90 Using the Module Algae Growth in HPLC Systems 1290 Infinity Quaternary Pump User Manual...
Page 91: How To Optimize The Performance Of Your Module
1290 Infinity Quaternary Pump User Manual How to Optimize the Performance of Your Module Operational Hints for the Multi Channel Gradient Valve (MCGV) Delay Volume and Extra-Column Volume Delay Volume How to Configure the Optimum Delay Volume How to Achieve Higher Resolution...
Page 92: Operational Hints For The Multi Channel Gradient Valve (Mcgv)
(flow/retention time stability), a blockage or internal leak of the pump. Avoid the use of such solvent combinations, as they can cause irreproducible chromatographic results. 1290 Infinity Quaternary Pump User Manual...
Page 93: Delay Volume And Extra-Column Volume
For the 1290 Infinity Quaternary Pump, all pump parts downstream the MCGV contribute to the delay volume, i.e. inlet weaver, pump heads, capillary connections, filters and the optional Jet Weaver.
Page 94: How To Configure The Optimum Delay Volume
This ensures best results for most applications. Per default, the 1290 Infinity Quaternary Pump does not require and include a Jet Weaver, as solvents are mixed in the MCGV and mixing is further improved in the inlet weaver, pump heads and subsequent parts in the flow path.
Page 95 How to Optimize the Performance of Your Module How to Configure the Optimum Delay Volume Figure 16 The Jet Weaver mixer The installation procedure is illustrated in “Installing the Jet Weaver” page 161. 1290 Infinity Quaternary Pump User Manual...
Page 96: How To Achieve Higher Resolution
The resolution equation shows that the next most significant term is the plate count or efficiency, N, and this can be optimized in a number of ways. N is inversely proportional to the particle size and directly proportional to the 1290 Infinity Quaternary Pump User Manual...
Page 97 = time length of gradient (or segment of gradient) (min), • F = flow (ml/min), • V = column delay volume, • Δ%B = change in fraction of solvent B during the gradient, • S = constant (ca. 4-5 for small molecules). 1290 Infinity Quaternary Pump User Manual...
Page 98 40 °C) can generate higher peak capacity than a longer STM column by virtue of running it faster. (Refer to Petersson et al., J.Sep.Sci, 31, 2346-2357, 2008, Maximizing peak capacity and separation speed in liquid chromatography). 1290 Infinity Quaternary Pump User Manual...
Page 99: Using Solvent Calibration Tables
5 Navigate to the location of the solvent calibration table and click Open. The new solvent will now appear in the Solvent Type Catalogs. The imported solvent is now available for selection as a solvent type in the pump's method parameters. 1290 Infinity Quaternary Pump User Manual...
Page 100 How to Optimize the Performance of Your Module Using Solvent Calibration Tables 1290 Infinity Quaternary Pump User Manual...
Page 101: Troubleshooting And Diagnostics
1290 Infinity Quaternary Pump User Manual Troubleshooting and Diagnostics Available Tests vs User Interfaces Agilent Lab Advisor Software Overview about the troubleshooting and diagnostic features. Agilent Technologies...
Page 102: Available Tests Vs User Interfaces
• Preferred tool should be the Agilent Lab Advisor software, see “Agilent Lab Advisor Software” on page 103. • The Agilent ChemStation may not include any maintenance/test functions. • Screenshots used within these procedures are based on the Agilent Lab Advisor software. 1290 Infinity Quaternary Pump User Manual...
Page 103: Agilent Lab Advisor Software
Agilent 1200 Infinity and Agilent InfinityLab LC Series instrument. The tests and diagnostic features that are provided by the Agilent Lab Advisor software may differ from the descriptions in this manual. For details, refer to the Agilent Lab Advisor software help files. 1290 Infinity Quaternary Pump User Manual...
Page 104 Troubleshooting and Diagnostics Agilent Lab Advisor Software 1290 Infinity Quaternary Pump User Manual...
Page 105: Error Information
1290 Infinity Quaternary Pump User Manual Error Information What Are Error Messages General Error Messages Timeout Shutdown Remote Timeout Lost CAN Partner Leak Sensor Short Leak Sensor Open Compensation Sensor Open Compensation Sensor Short Fan Failed Leak Pump Error Messages...
Page 106 Seal wash pump was missing when tried to turn on Valve hardware overcurrent (MCGV) Invalid degasser pressure signal This chapter describes the meaning of error messages, and provides information on probable causes and suggested actions how to recover from error conditions. 1290 Infinity Quaternary Pump User Manual...
Page 107: What Are Error Messages
In all cases, error propagation is done via the CAN bus or via an APG/ERI remote cable (see documentation for the APG/ERI interface). 1290 Infinity Quaternary Pump User Manual...
Page 108: General Error Messages
Check the logbook for the occurrence and A not-ready condition was present during a source of a not-ready condition. Restart the sequence or multiple-injection run for a analysis where required. period longer than the timeout threshold. 1290 Infinity Quaternary Pump User Manual...
Page 109: Shutdown
Check the vacuum degasser for an error The degasser failed to generate sufficient condition. Refer to the Service Manual for the vacuum for solvent degassing. degasser or the pump that has the degasser built-in. 1290 Infinity Quaternary Pump User Manual...
Page 110: Remote Timeout
• Ensure all CAN cables are installed correctly. Exchange the CAN cable. Defective CAN cable. Switch off the system. Restart the system, and Defective main board in another module. determine which module or modules are not recognized by the system. 1290 Infinity Quaternary Pump User Manual...
Page 111: Leak Sensor Short
Leak sensor not connected to the main representative. board. Please contact your Agilent service Defective leak sensor. representative. Please contact your Agilent service Leak sensor incorrectly routed, being representative. pinched by a metal component. 1290 Infinity Quaternary Pump User Manual...
Page 112: Compensation Sensor Open
Please contact your Agilent service Loose connection between the power representative. switch board and the main board Please contact your Agilent service Defective power switch assembly representative. Please contact your Agilent service Defective main board. representative. 1290 Infinity Quaternary Pump User Manual...
Page 113: Compensation Sensor Short
Please contact your Agilent service Defective power switch assembly representative. Please contact your Agilent service Loose connection between the power representative. switch board and the main board Please contact your Agilent service Defective main board. representative. 1290 Infinity Quaternary Pump User Manual...
Page 114: Fan Failed
Probable cause Suggested actions Please contact your Agilent service Fan cable disconnected. representative. Please contact your Agilent service Defective fan. representative. Please contact your Agilent service Defective main board. representative. 1290 Infinity Quaternary Pump User Manual...
Page 115: Leak
Loose or leaking purge valve, inlet valve, or If there are still signs of a leak, exchange the outlet valve. appropriate seal (purge valve, inlet valve, outlet valve). Exchange the pump seals. Defective pump seals. 1290 Infinity Quaternary Pump User Manual...
Page 116: Pump Error Messages
• Parameter: None Probable cause Suggested actions Check for leaks. Leak Check bottle filling. Bottle empty Check solvent. Wrong solvent (viscosity) Check flow rate and lower pressure limit. Inappropriate setting Replace column. Column degradation 1290 Infinity Quaternary Pump User Manual...
Page 117: Target Pressure Not Reached For Quaternary Pump Degasser
The counter for the waste volume has exceeded the limit, which has been set in the user interface. • Parameter: None Probable cause Suggested actions Empty waste container. The waste container is full. • Reset waste counter. Inappropriate setting for waste counter. • Adjust waste counter limit. 1290 Infinity Quaternary Pump User Manual...
Page 118: Flow Rate Limit Exceeded
The quaternary pump has been shut down by the control software or control module during an analysis. • Parameter: 0 for off, 1 for standby. Probable cause Suggested actions Restart pump. Pump has been shut down. 1290 Infinity Quaternary Pump User Manual...
Page 119: Reading The Pump Encoder Tag Failed
Pump drive blocked or encoder failed Error ID: 29214 Pump drive blocked or encoder failed. • Parameter: None Probable cause Suggested actions Please contact your Agilent service Blockage of the pump drive Drive encoder representative. failed. 1290 Infinity Quaternary Pump User Manual...
Page 120: Drive Current Too Low
• Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Check for blockage of e.g. outlet valve filter frit, Blockage of system before pressure sensor. Multi Purpose Valve, heat exchanger. Please contact your Agilent service Drive motor defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 121: Drive Timeout
• Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Check for blockage of e.g. outlet valve filter frit, Blockage of system before pressure sensor. Multi Purpose Valve, heat exchanger. Please contact your Agilent service Drive motor defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 122: Deliver Underrun
Defect encoder. representative. Pump drive encoder defect Error ID: 29209 Defect pump drive encoder. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Defect encoder. representative. 1290 Infinity Quaternary Pump User Manual...
Page 123: Multi Purpose Valve Failed
Error ID: 29232 Invalid pump drive encoder signals have been detected. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 124: Drive Position Limit
Error ID: 29237, 29238, 29239, 29215 An error has occurred for the pump drive encoder. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 125: Writing The Multi Purpose Valve Tag Failed
Error ID: 29211 The pump drive encoder has generated no signal. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 126: Pump Drive Error
Probable cause Suggested actions Please contact your Agilent service Wiper shifted representative. Replace, clean or repair pump head. Pump head blocks piston movement Please contact your Agilent service Pump drive motor is mechanically blocked. representative. 1290 Infinity Quaternary Pump User Manual...
Page 127: Pump Drive Stop Not Found
Probable cause Suggested actions Verify control software, macros, manual Incorrect parameters have been sent to the commands. instrument by the control software or manual changes. 1290 Infinity Quaternary Pump User Manual...
Page 128: Timeout: Wait For Run Volume
(for example the flow rate). Probable cause Suggested actions Verify control software, macros, manual Incorrect parameters have been sent to the commands. instrument by the control software or manual changes. 1290 Infinity Quaternary Pump User Manual...
Page 129: Timeout: Wait For Flow
Run system pressure test for identifying and Leak localizing the leak. Tighten leak. Drive Encoder failed Error ID: 29210 Drive encoder failed during pump drive calibration. Probable cause Suggested actions Contact Agilent support. Internal error. 1290 Infinity Quaternary Pump User Manual...
Page 130: Drive Phases Differ Too Much In Electric Resistance
Suggested actions Please contact your Agilent service Leak in degasser chamber or degasser representative. tubing. Please contact your Agilent service Defect vacuum pump. representative. Block unused degasser channels. Degasser chamber empty or connected to air. 1290 Infinity Quaternary Pump User Manual...
Page 131: Seal Wash Pump Was Missing When Tried To Turn On
Error ID: 29227 Power consumption too high for one of the MCGV valves. Probable cause Suggested actions Replace MCGV. Cable defect. Replace MCGV. Valve defect Please contact your Agilent service Defective main board. representative. 1290 Infinity Quaternary Pump User Manual...
Page 132: Invalid Degasser Pressure Signal
Error ID: 29253 The degasser pressure signal is invalid. Probable cause Suggested actions Please contact your Agilent service Degasser might be disconnected representative. Please contact your Agilent service Pressure sensor might be defective representative. 1290 Infinity Quaternary Pump User Manual...
Page 133: Test Functions And Calibrations
1290 Infinity Quaternary Pump User Manual Test Functions and Calibrations Pump Leak Rate Test Troubleshooting the Pump Leak Rate Test System Pressure Test This chapter describes the tests for the module. Agilent Technologies...
Page 134: Pump Leak Rate Test
The result as well as the applied limits are displayed after the automatic evaluation. The limits are: • The allowed leak limit for the secondary piston is ≤3 μL/min • The allowed leak limit for the primary piston is ≤30 μL/min 1290 Infinity Quaternary Pump User Manual...
Page 135 If the test does not pass, check the system for leaks or call a local Agilent representative. Figure 17 on page 135 and Figure 18 on page 136 show a typical test run. Figure 17 Static (secondary) Leak Test 1290 Infinity Quaternary Pump User Manual...
Page 136 Test Functions and Calibrations Pump Leak Rate Test Figure 18 Dynamic (primary) Leak Test 1290 Infinity Quaternary Pump User Manual...
Page 137 • Leak in Inlet Valve • Check for moving air bubbles in tubing directly to the Inlet Valve • Purge the lines with water to remove dirt • Knock at the valve, clean or replace it 1290 Infinity Quaternary Pump User Manual...
Page 138 Remove the SW tubes from the support ring and check for leaks • Replace the piston seals and clean the pistons • Ensure that seals are lubricated when pushed in • Use abrasive mesh >5000 grit 1290 Infinity Quaternary Pump User Manual...
Page 139: System Pressure Test
If the test does not pass, check the system for leaks or call a local Agilent representative. Figure 19 on page 140 shows a typical test run. 1290 Infinity Quaternary Pump User Manual...
Page 140 Test Functions and Calibrations System Pressure Test Figure 19 System Pressure Test 1290 Infinity Quaternary Pump User Manual...
Page 141: Maintenance
1290 Infinity Quaternary Pump User Manual Maintenance Introduction to Maintenance Warnings and Cautions Overview of Maintenance Cleaning the Module Installing Fittings and Capillaries Replacing the Pressure Sensor Replacing the Inlet Weaver Replacing the Inlet Valve Replacing the Outlet Valve Removing the Jet Weaver...
Page 142 System Pressure Test Replacing Parts of the Inline Filter Installing the Valve Rail Kit Replacing Module Firmware Preparing the Pump Module for Transport This chapter describes the maintenance of the Agilent 1290 Infinity Quaternary Pump. 1290 Infinity Quaternary Pump User Manual...
Page 143: Introduction To Maintenance
Introduction to Maintenance Figure 20 on page 143 shows the main user-accessible assemblies of the Agilent 1290 Infinity Quaternary Pump. These parts can be accessed from the front (simple repairs) and don’t require to remove the pump from the system stack.
Page 144: Warnings And Cautions
C AU T I O N ➔ If you connect external equipment to the instrument, make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment. 1290 Infinity Quaternary Pump User Manual...
Page 145: Overview Of Maintenance
Maintenance Overview of Maintenance Overview of Maintenance The following pages describe maintenance (simple repairs) of the module that can be carried out without opening the main cover. 1290 Infinity Quaternary Pump User Manual...
Page 146: Cleaning The Module
WA R N I N G hazard and damage the module ➔ Do not use an excessively damp cloth during cleaning. ➔ Drain all solvent lines before opening any connections in the flow path. 1290 Infinity Quaternary Pump User Manual...
Page 147: Installing Fittings And Capillaries
The lifetime of a fitting depends on how firmly it has been tightened; firm tightening N O T E reduces the lifetime. If fitting has been overtightened, replace it. 1 Install fittings and capillaries. 2 Tighten fittings and capillaries. 1290 Infinity Quaternary Pump User Manual...
Page 148: Replacing The Pressure Sensor
Working on connections to the pressure sensor may slightly change the displayed N O T E pressure. In case of a pressure offset at ambient pressure, a pressure offset calibration may be run. 1290 Infinity Quaternary Pump User Manual...
Page 149 Carefully pull out the pressure sensor for about 2 cm. Connect the new pressure sensor to the pressure sensor Then unscrew the cable from the pressure sensor. connector. 1290 Infinity Quaternary Pump User Manual...
Page 150 Connect the capillary from the pump head outlet to the pressure sensor inlet. Two arrow signs on the pressure sensor indicate the flow direction. If applicable, connect the outlet of the pressure sensor to the central port of the Multi Purpose Valve. 1290 Infinity Quaternary Pump User Manual...
Page 151: Replacing The Inlet Weaver
Open the screw at the bottom of the inlet valve. Open the fitting at the center of the multi-channel gradient valve (MCGV). Do not open the screw marked with the red cross. Remove the inlet weaver from the MCGV. 1290 Infinity Quaternary Pump User Manual...
Page 152 Pull the inlet weaver out of the inlet valve. Insert the new inlet weaver to the inlet valve. Fix the weaver with the plastic screw. Fix the fitting of the new inlet weaver to the MCGV. Reconnect tubings between MCGV and degasser. 1290 Infinity Quaternary Pump User Manual...
Page 153: Replacing The Inlet Valve
151 With a 14 mm wrench, unscrew the inlet valve and Install the new inlet valve and tighten it using a torque remove it. wrench with a 14 mm bit set to 10 Nm. 1290 Infinity Quaternary Pump User Manual...
Page 154 Maintenance Replacing the Inlet Valve Next Steps: Insert the inlet weaver, see “Replacing the Inlet Weaver” on page 151. Purge and condition the system to remove air. 1290 Infinity Quaternary Pump User Manual...
Page 155: Replacing The Outlet Valve
Internal gold seal for Outlet Valve Preparations • Switch off pump at the main power switch • Remove the front cover • Use an optional solvent shutoff valve or lift up solvent filters inside solvent bottles for avoiding leakages 1290 Infinity Quaternary Pump User Manual...
Page 156 The seal can be heat exchanger. Then lift up the capillary and remove it replaced separately as needed. from the primary pump head. 1290 Infinity Quaternary Pump User Manual...
Page 157 Replacing the Outlet Valve Unscrew the outlet valve with a 14 mm wrench. Insert the new outlet valve and tighten it using a torque wrench with a 14 mm bit set to 10 Nm. 1290 Infinity Quaternary Pump User Manual...
Page 158 Purge and condition the system to remove air. outlet valve. Using a torque wrench with a 2.5 mm hex bit, set 3 Nm and close the hex screw at the top of the outlet. 1290 Infinity Quaternary Pump User Manual...
Page 159: Removing The Jet Weaver
• Switch off the pump at the main power switch. Remove capillary connections from the Jet Weaver to Open the screw, which fixes the Jet Weaver to the front the Multi Purpose Valve. panel. 1290 Infinity Quaternary Pump User Manual...
Page 160 If no other Jet Weaver shall be installed, use plastic panel (2). fittings for closing unused ports of the valve and install the metal lid. Otherwise continue at “Installing the Jet Weaver” page 161. 1290 Infinity Quaternary Pump User Manual...
Page 161: Installing The Jet Weaver
Switch off the pump at the main power switch Open the screw of the Jet Weaver metal lid. Remove the metal lid by lifting it up (1) and pulling it out of the front panel (2). 1290 Infinity Quaternary Pump User Manual...
Page 162 Connect the inlet capillary of the Jet Weaver to port 2 of Configure the Jet Weaver as mixer in the user interface, the Multi Purpose Valve. Connect the outlet capillary to “Instrument Configuration” on page 61. port 1. 1290 Infinity Quaternary Pump User Manual...
Page 163: Replacing The Seal Wash Pump
Remove the flow connections from and to the seal wash pump. For removing the seal wash pump, press the clips (1) and Insert the pump clips to the holes in the module housing. pull the pump to the front (2). 1290 Infinity Quaternary Pump User Manual...
Page 164 Maintenance Replacing the Seal Wash Pump Fix tubings of the peristaltic pump to the primary pump head outlet and secondary pump head inlet. 1290 Infinity Quaternary Pump User Manual...
Page 165: Replacing The Multi-Channel Gradient Valve (Mcgv)
For best performance and life time, use lower channels A and D for aqueous solvents in N O T E buffer applications, see “Operational Hints for the Multi Channel Gradient Valve (MCGV)” on page 92 for details. 1290 Infinity Quaternary Pump User Manual...
Page 166 Use the mounting tool for removing tubing connections Remove the inlet weaver, see “Replacing the Inlet between the degassing unit and the MCGV. Weaver” on page 151. Remove the waste funnel. Remove the cover from the MCGV. 1290 Infinity Quaternary Pump User Manual...
Page 167 Disconnect the MCGV cable (1), unscrew the two Place the new MCGV into position. screws (2, 3) and remove the valve. N O T E Make sure that channel A of the MCGV is put at the bottom-right position. 1290 Infinity Quaternary Pump User Manual...
Page 168 MCGV cover. Install the inlet weaver, see “Replacing the Inlet Weaver” on page 151. Reconnect solvent tubes for channels A-D from the MCGV to the degasser outlets. 1290 Infinity Quaternary Pump User Manual...
Page 169: Releasing A Stuck Inlet Valve
Open the fitting at the center of the multi-channel the MCGV such that you can access the inlet weaver. gradient valve (MCGV). Do not open the screw marked with the red cross. Remove the inlet weaver from the MCGV. 1290 Infinity Quaternary Pump User Manual...
Page 170 Fill the syringe with a suitable wash solvent. Connect the syringe and adapter to the inlet weaver. N O T E For salt deposits, warm water is a good choice. For organic deposits, use ethanol or acetone. 1290 Infinity Quaternary Pump User Manual...
Page 171 Maintenance Releasing a Stuck Inlet Valve Push the syringe for flushing the inlet valve and pump Restore original connections. Flush the system for head. several minutes. 1290 Infinity Quaternary Pump User Manual...
Page 172: Remove The Pump Head Assembly
Remove the capillary connection from the outlet filter on Remove/Install Pump Head and follow instructions the secondary pump head to the pressure sensor. given on the screen. Remove flow connections of the seal wash function. 1290 Infinity Quaternary Pump User Manual...
Page 173 Loosen the inlet valve. Keep the inlet valve installed to bottom of the left primary pump head (1) and remove the the pump head assembly. inlet weaver by first pushing it downwards (2) and then pulling it out to the left (3). 1290 Infinity Quaternary Pump User Manual...
Page 174 Open the four screws holding the pump heads. while loosening the outlet valve. Keep the outlet valve installed to the pump head assembly. N O T E Open all screws step by step, not screw by screw. 1290 Infinity Quaternary Pump User Manual...
Page 175 Maintenance Remove the Pump Head Assembly Remove the complete pump head assembly by holding Remove the seal wash tubing interconnecting the two both heads and pulling it to the front. pump heads. 1290 Infinity Quaternary Pump User Manual...
Page 176: Pump Head Maintenance (Tool Free)
Pump Head Maintenance (Tool Free) Pump Head Maintenance (Tool Free) Infinity II Flexible Pumps (G7104A/C) and 1290 Infinity II High Speed Pumps (G7120A) are equipped with Long Life Pump Heads. Long Life Pump Heads offer a significantly increased lifetime of pistons and seals compared to other pump heads.
Page 177: Disassemble Longlife Pump Heads
Remove the heat exchanger capillary by pushing the the heat exchanger capillary. connector up and pulling it out of the valve. N O T E A gold seal between outlet valve and heat exchanger capillary is used for a tight connection. 1290 Infinity Quaternary Pump User Manual...
Page 178 Binary/High Speed Pumps only: Remove the high primary pump head. pressure filter from the secondary pump head. N O T E Clean the valves by sonication, if appropriate. A good cleaning solution is 50 % isopropanol in water. 1290 Infinity Quaternary Pump User Manual...
Page 179 Remove the piston by pressing it out of the seal holder from the pump chambers. with a finger. Remove the seal holder from the spring housing. Screw the pin of the seal handling device into the piston seal. 1290 Infinity Quaternary Pump User Manual...
Page 180 The side with the backup ring has a bigger diameter and a sharp edge to hold the piston seal. The other side has no sharp edge and holds the smaller wash seal. 1290 Infinity Quaternary Pump User Manual...
Page 181 Maintenance Pump Head Maintenance (Tool Free) Repeat for the other seal holder. Clean the piston with abrasive paper. Rinse pump heads and pistons with isopropanol. 1290 Infinity Quaternary Pump User Manual...
Page 182: Replace The Heat Exchanger
➔ The heat exchanger does not need to be removed for pump head maintenance. Remove the 19 mm screw at the front of the secondary Remove the front plate. pump head. 1290 Infinity Quaternary Pump User Manual...
Page 183 If removed, first insert the spacer fitting. Then insert the Use the 19 mm screw for fixing the front plate. new heat exchanger to the opening in the pump head and lift it over the pins. Insert and fix the screw. 1290 Infinity Quaternary Pump User Manual...
Page 184: Assemble Longlife Pump Heads
5043-1400 Pump Head Holder 5067-6197 Seal Handling Device Isopropanol Parts required Description 0905-1719 PE Seal 0905-1175 Wash seal (PTFE) Seals must be exchanged in both primary and secondary pump heads. N O T E 1290 Infinity Quaternary Pump User Manual...
Page 185 Seal Handling Device. The metal spring of the piston seal must be visible. Take care that the Seal Handling Device is seating flush Repeat for the other pump chamber. and press the seal into the pump chamber. 1290 Infinity Quaternary Pump User Manual...
Page 186 Repeat for the other seal holder. and press the wash seal into the seal holder. N O T E The Seal Handling Device has a cavity to fit over the pins of the seal wash tubings. 1290 Infinity Quaternary Pump User Manual...
Page 187 Mind the correct orientation: The backup ring must Both spring housings are identical, there is no risk face upwards and the seal holder must sit correcly. when mixing them, but make sure that the seal holder is oriented correctly. 1290 Infinity Quaternary Pump User Manual...
Page 188 Mount the pump head to the module. Do not fix the to approx. 5 Nm in a crosswise manner. screws at this stage! N O T E When the wrench clicks, the set torque is reached. Do not overtighten the screws. 1290 Infinity Quaternary Pump User Manual...
Page 189 Counter the outlet valve and tighten the lock screw of Attach the seal wash tubing interconnecting the two the heat exchanger capillary with a torque wrench set to pump heads. approx. 3 Nm. 1290 Infinity Quaternary Pump User Manual...
Page 190 Maintenance Pump Head Maintenance (Tool Free) Insert the screws that later fix the pump head assembly to the module housing. 1290 Infinity Quaternary Pump User Manual...
Page 191: Install The Pump Head Assembly
Install the new pump head assembly by tightening the screws step by step. Apply 5 Nm using a torque hex key, which is included to the 1290 Infinity Service Kit p/n 5067-4699. 1290 Infinity Quaternary Pump User Manual...
Page 192 Maintenance Install the Pump Head Assembly Connect the capillary from the pressure sensor to the Install the seal wash tubings to the seal wash pump head outlet filter. connectors. 1290 Infinity Quaternary Pump User Manual...
Page 193: Replacing The Multi Purpose Valve
Remove all capillary connections from the Multi Purpose Valve. Remove the clamp with the inline filter (if installed). Unscrew the black union nut and remove the head of the purge valve by pulling it to the front. 1290 Infinity Quaternary Pump User Manual...
Page 194 Replacing the Multi Purpose Valve Put the new valve head onto the valve drive such that the lobe fits to the groove. Screw the valve head onto the valve drive using the union nut. 1290 Infinity Quaternary Pump User Manual...
Page 195 • Port 8 is connected to the inlet of the optional inline filter Block unused ports with blank nuts. If the optional inline filter is not installed, connect ports 5 and 8 with a capillary (Capillary ST 0.17 x 120 mm, SLV/SV (5067-5416)). 1290 Infinity Quaternary Pump User Manual...
Page 196: Replacing Parts Of The Multi Purpose Valve
Description 8710-2394 9/64 inch hex key Parts required Description 1534-4045 Bearing ring 5068-0123 Rotor seal, Multi Purpose Valve 1290 Infinity Quaternary Pump, 1200 bar 5068-0120 Stator ring 5068-0001 Stator head 1535-4857 Stator screws, 10/pk Preparations Remove all capillary connections from the Multi Purpose Valve.
Page 197 Maintenance Replacing Parts of the Multi Purpose Valve 3 Reassemble the valve head and mount it to the valve drive. 1290 Infinity Quaternary Pump User Manual...
Page 198: Replacing The Outlet Filter
Torque wrench head, 14 mm for torque wrench Parts required Description G4204-60004 Outlet filter Quaternary Pump/Flexible Pump Remove the capillary from the outlet filter to the Remove the outlet filter using a 14 mm wrench. pressure sensor. 1290 Infinity Quaternary Pump User Manual...
Page 199 Maintenance Replacing the Outlet Filter Mount the new outlet filter. Using a torque wrench set to Mount the capillary connection to the pressure sensor. 16 Nm is recommended. 1290 Infinity Quaternary Pump User Manual...
Page 200: Installing The Inline Filter
Capillary ST, 0.17 mm x 90 mm G4204-40000 Clamp for In-Line Filter Preparations Turn the pump off. Remove the capillary between ports 5 and 8 from the Clip the inline filter clamp to the Multi Purpose Valve. Multi Purpose Valve. 1290 Infinity Quaternary Pump User Manual...
Page 201 Install the integrated capillary of the inline filter to port 5 Install the removable capillary of the inline filter to port 8 of the Multi Purpose Valve. of the Multi Purpose Valve. 1290 Infinity Quaternary Pump User Manual...
Page 202: Removing The Inline Filter
Open-end wrench 1/4 — 5/16 inch Parts required Description 5067-5416 Capillary ST 0.17 x 120 mm, SLV/SV Remove the capillaries from the Multi Purpose Valve to Remove the clamp with the inline filter (if installed). the inline filter. 1290 Infinity Quaternary Pump User Manual...
Page 203 Maintenance Removing the Inline Filter Install the capillary between ports 5 and 8 of the Multi Purpose Valve. 1290 Infinity Quaternary Pump User Manual...
Page 204: Replacing Parts Of The Inline Filter
Use Capillary ST 0.17 x 120 mm, SLV/SV (5067-5416) instead. The inline filter can be cleaned using the back-flush function in the user interface of your N O T E Agilent instrument control software. 1290 Infinity Quaternary Pump User Manual...
Page 205 Remove the inline filter from the clamp attached to the the inline filter. Multi Purpose Valve. Use two 5/16 wrenches for opening the inline filter. Replace the filter frit and reassemble the inline filter. 1290 Infinity Quaternary Pump User Manual...
Page 206 Replacing Parts of the Inline Filter Put the inline filter to the clamp and install its capillaries. The integrated capillary is connected to port 5 of the Multi Purpose Valve. The removable capillary is connected to port 8. 1290 Infinity Quaternary Pump User Manual...
Page 207: Installing The Valve Rail Kit
1 The valve rail is fixed to the pump cover by 4 screws. The position of the lower screws is marked on the module cover. First tighten these screws, and then tighten the upper screws. 1290 Infinity Quaternary Pump User Manual...
Page 208: Replacing Module Firmware
Update Tool and the documentation from the Agilent web. • http://www.agilent.com/en-us/firmwareDownload?whid=69761 2 For loading the firmware into the module follow the instructions in the documentation. Module Specific Information There is no specific information for this module. 1290 Infinity Quaternary Pump User Manual...
Page 209: Preparing The Pump Module For Transport
2 Remove solvent inlet tubes from solvent reservoirs and tubing clips at other modules. 3 Remove tubings between the seal wash function and solvent bottle/waste. 4 Remove cable and capillary connections to other modules. 5 Remove the module from the stack. 6 Remove the waste tube. 1290 Infinity Quaternary Pump User Manual...
Page 210 Maintenance Preparing the Pump Module for Transport 7 Disconnect the degasser outlet tubings at the MCGV one after another. Use a syringe for removing liquid from the degasser and the solvent tubings. 1290 Infinity Quaternary Pump User Manual...
Page 211 Maintenance Preparing the Pump Module for Transport 8 Reconnect the degasser outlet tubings to the MCGV. Remove the degasser inlet tubings. 1290 Infinity Quaternary Pump User Manual...
Page 212 Maintenance Preparing the Pump Module for Transport 9 You may keep internal tubing and capillary connections. 1290 Infinity Quaternary Pump User Manual...
Page 213 10 Carefully insert the protective foam to the front part of the instrument. Do not damage any tubing or capillary connections. 11 Close the front cover. 12 For transport or shipment, put the module and accessory kit to the original shipment box. 1290 Infinity Quaternary Pump User Manual...
Page 214 Maintenance Preparing the Pump Module for Transport 1290 Infinity Quaternary Pump User Manual...
Page 215: Parts And Materials
1290 Infinity Quaternary Pump User Manual Parts and Materials Overview of Main Assemblies Flow Connections Seal Wash Function Pump Heads Pump Head Assembly Parts Primary Pump Head Parts Secondary Pump Head Parts Multi Purpose Valve Solvent Cabinet Cover Parts Leak Parts...
Page 216: Overview Of Main Assemblies
Parts and Materials Overview of Main Assemblies Overview of Main Assemblies Figure 21 Overview of maintenance parts 1290 Infinity Quaternary Pump User Manual...
Page 217 Multi channel gradient valve (MCGV) 5041-8365 Blank plug for MCGV G1311-60070 Degasser 4 Channels for Quaternary Pump 5065-4445 Peristaltic pump with Pharmed tubing G4220-60001 Pressure sensor 1200 bar G4204-68000 Jet Weaver 380 µL for Quaternary Pump/Flexible Pump (OPTIONAL) 1290 Infinity Quaternary Pump User Manual...
Page 218: Flow Connections
Tubing Kit 140 mm - Ultra Clean Tubing (tubes from SSV to shutoff valve or degassing unit to MCGV) G4220-60017 Bottle Head Assembly Ultra Clean Tubing (bottle heads and tubing to shutoff panel / degasser) 1290 Infinity Quaternary Pump User Manual...
Page 219: Seal Wash Function
Parts and Materials Seal Wash Function Seal Wash Function Figure 23 Seal Wash Pump Description 5065-4445 Peristaltic pump with Pharmed tubing 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m 1290 Infinity Quaternary Pump User Manual...
Page 220: Pump Heads
The following pages contain parts information for LongLife Pump Heads. For parts information on other pump head types, please refer to Agilent 1290 Infinity II Easy Maintenance Pump Head Technical Note (01200-90120) and to Agilent 1290 Infinity Pump Head Maintenance Technical Note (G4220-90122). 1290 Infinity Quaternary Pump User Manual...
Page 221: Pump Head Assembly Parts
Inlet Valve Quaternary Pump/Flexible Pump G4220-60028 Outlet valve (primary pump head) G4220-20020 Internal gold seal for Outlet Valve (not shown) 5042-9966 Cap Outlet Valve G1312-60001 Adapter G4220-81013 Heat Exchanger G4220-40001 Link Plate 0960-2971 RF Transponder 1290 Infinity Quaternary Pump User Manual...
Page 222: Primary Pump Head Parts
Primary Pump Head Assembly Pendulum (G4220-60661) Item Description 5067-5975 Plunger Assy ZrO 0515-6154 Screw-Socket-HD-Cap Hex-Recess M5X0.8 40 G4220-60046 Preload-Support Assembly LL 0905-1175 Wash seal (PTFE) G4220-60616 Seal Holder Integrated Assembly EM/LL 0905-1719 PE Seal G4220-60533 Body Head Primary EM/LL 1290 Infinity Quaternary Pump User Manual...
Page 223: Secondary Pump Head Parts
0905-1175 Wash seal (PTFE) G4220-60616 Seal Holder Integrated Assembly EM/LL 0905-1719 PE Seal G4220-25513 Body Head Secondary EM/LL G4220-20001 Spacer Fitting G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20000 G4220-20003 Pump Head Screw 1290 Infinity Quaternary Pump User Manual...
Page 224: Multi Purpose Valve
Parts and Materials Multi Purpose Valve Multi Purpose Valve Figure 25 Multi-purpose valve parts 1290 Infinity Quaternary Pump User Manual...
Page 225 Description 5067-4174 Multi Purpose Valve Head 1535-4857 Stator screws, 10/pk 5068-0001 Stator head 5068-0120 Stator ring 5068-0123 Rotor seal, Multi Purpose Valve 1290 Infinity Quaternary Pump, 1200 bar 1535-4045 Bearing ring 5068-0106 Spanner nut 1290 Infinity Quaternary Pump User Manual...
Page 226: Solvent Cabinet
Parts and Materials Solvent Cabinet Solvent Cabinet Figure 26 Solvent Cabinet Parts (1) Figure 27 Solvent Cabinet Parts (2) 1290 Infinity Quaternary Pump User Manual...
Page 227 Description 5065-9981 Solvent cabinet 1200 Infinity, including all plastic parts 5043-0207 Name plate 1260 5065-9954 Front panel, solvent cabinet 5042-8907 Leak panel 9301-1450 Solvent bottle, amber 9301-1420 Solvent bottle, transparent G4220-60007 Bottle Head Assembly 1290 Infinity Quaternary Pump User Manual...
Page 228: Cover Parts
Cover Parts Cover Parts Figure 28 Cover parts Item Description 5067-5396 1290 Infinity Quaternary Pump Cover Kit (base, top, left, right) 5042-9964 Name plate for Agilent 1290 series 5067-4683 Front Panel 5042-8914 Serial number plate 1290 Infinity Quaternary Pump User Manual...
Page 229: Leak Parts
Leak parts Item Description 5041-8389 Leak funnel holder 5041-8388 Leak funnel 5062-2463 Corrugated tubing, PP, 6.5 mm id, 5 m G1361-47100 Sealing lip 5042-9922 Leak panel G4280-40016 Power Switch Coupler ZL 5041-8381 Power switch button 1290 Infinity Quaternary Pump User Manual...
Page 230: Accessory Kit
Parts and Materials Accessory Kit Accessory Kit The Accessory Kit 1290 Infinity Quaternary Pump (G4204-68705) contains: Item Description 5063-6527 Leak tubing assembly, 1 m 5181-1519 CAN cable, Agilent module to module, 1 m 5042-9967 Tubing clip (set of 5 clips)
Page 231: Hplc System Tool Kit
Parts and Materials HPLC System Tool Kit HPLC System Tool Kit 1290 Infinity Quaternary Pump User Manual...
Page 232 Parts and Materials HPLC System Tool Kit 1290 Infinity Quaternary Pump User Manual...
Page 233: Identifying Cables
1290 Infinity Quaternary Pump User Manual Identifying Cables Cable Overview Analog cables Remote Cables BCD Cables CAN/LAN Cable RS-232 Cable Kit Agilent 1200 Module to Printer This chapter provides information on cables used with the Agilent 1200 Infinity Series modules.
Page 234: Cable Overview
Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent module to 3394/6 integrators...
Page 235 It is also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity Quaternary Pump User Manual...
Page 236: Analog Cables
The other end depends on the instrument to which connection is being made. Agilent Module to 3394/6 Integrators p/n 35900-60750 Pin 3394/6 Pin Agilent Signal Name module Not connected Shield Analog - Center Analog + 1290 Infinity Quaternary Pump User Manual...
Page 237 Pin BNC Pin Agilent Signal Name module Shield Shield Analog - Center Center Analog + Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog + 1290 Infinity Quaternary Pump User Manual...
Page 238: Remote Cables
Identifying Cables Remote Cables Remote Cables One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. Agilent Module to 3396A Integrators...
Page 239 3 - Gray Start 4 - Blue Shut down 5 - Pink connected 6 - Yellow Power on High 7 - Red Ready High 8 - Green Stop 9 - Black Start request 13, 15 connected 1290 Infinity Quaternary Pump User Manual...
Page 240 01046-60201 Wire Color Pin Agilent Signal Name Active module (TTL) White Digital ground Brown Prepare run Gray Start Blue Shut down Pink connected Yellow Power on High Ready High Green Stop Black Start request 1290 Infinity Quaternary Pump User Manual...
Page 241: Bcd Cables
Black BCD 0 Orange BCD 3 BCD 2 Brown BCD 1 Gray Digital ground Gray Gray/pink BCD 11 Red/blue BCD 10 White/green BCD 9 Brown/green BCD 8 not connected not connected + 5 V 1290 Infinity Quaternary Pump User Manual...
Page 242 Agilent Module to 3396 Integrators p/n 03396-60560 Pin 3396 Pin Agilent Signal Name BCD Digit module BCD 5 BCD 7 BCD 6 BCD 4 BCD0 BCD 3 BCD 2 BCD 1 Digital ground + 5 V 1290 Infinity Quaternary Pump User Manual...
Page 243: Can/Lan Cable
CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) 1290 Infinity Quaternary Pump User Manual...
Page 244: Rs-232 Cable Kit
It is also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity Quaternary Pump User Manual...
Page 245: Agilent 1200 Module To Printer
Agilent 1200 Module to Printer Description 5181-1529 Cable Printer Serial & Parallel, is a SUB-D 9 pin female vs. Centronics connector on the other end (NOT FOR FW UPDATE). For use with G1323 Control Module. 1290 Infinity Quaternary Pump User Manual...
Page 246 Identifying Cables Agilent 1200 Module to Printer 1290 Infinity Quaternary Pump User Manual...
Page 247: Hardware Information
1290 Infinity Quaternary Pump User Manual Hardware Information Firmware Description Electrical Connections Rear View of the Module Interfaces Overview Interfaces Setting the 8-bit Configuration Switch Special Settings Early Maintenance Feedback Instrument Layout This chapter describes the pump in more detail on hardware and electronics.
Page 248: Firmware Description
• run synchronization through APG remote, • error handling, • diagnostic functions, • or module specific functions like • internal events such as lamp control, filter movements, • raw data collection and conversion to absorbance. 1290 Infinity Quaternary Pump User Manual...
Page 249 Update of main system can be done in the resident system only. Update of the resident N O T E system can be done in the main system only. Main and resident firmware must be from the same set. Figure 30 Firmware Update Mechanism 1290 Infinity Quaternary Pump User Manual...
Page 250 All this specific information is described in the documentation provided with the firmware update tools. The firmware update tools, firmware and documentation are available from the Agilent web. • http://www.agilent.com/en-us/firmwareDownload?whid=69761 1290 Infinity Quaternary Pump User Manual...
Page 251: Electrical Connections
There are no externally accessible fuses, because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations.
Page 252: Rear View Of The Module
Hardware Information Electrical Connections Rear View of the Module Figure 31 Rear of quaternary pump 1290 Infinity Quaternary Pump User Manual...
Page 253: Interfaces
G1364C FC-AS G1330B/K1330B μ CAN-DC- OUT for CAN G1364D FC- slaves G1367E HiP ALS K1367E HiP ALS Clinical Ed. G1377A HiP micro ALS G2258A DL ALS G5664A Bio-inert FC-AS G5667A Bio-inert Autosampler G4226A ALS 1290 Infinity Quaternary Pump User Manual...
Page 254 K1321B FLD Clinical Ed. G1321C FLD G1362A RID G4280A ELSD EXT Contact AUTOZERO Others G1170A Valve Drive G1316A/C TCC K1316C TCC Clinical Ed. G1322A DEG K1322A DEG Clinical Ed. G1379B DEG G4225A DEG K4225A DEG Clinical Ed. 1290 Infinity Quaternary Pump User Manual...
Page 255 • CAN connectors as interface to other modules • LAN connector as interface to the control software • RS-232C as interface to a computer • REMOTE connector as interface to other Agilent products • Analog output connector(s) for signal output 1290 Infinity Quaternary Pump User Manual...
Page 256: Overview Interfaces
There is no configuration possible on main boards with on-board LAN. These are N O T E pre-configured for • 19200 baud, • 8 data bit with no parity and • one start bit and one stop bit are always used (not selectable). 1290 Infinity Quaternary Pump User Manual...
Page 257 RS-232C Connection Table Direction Function Ground Figure 32 RS-232 Cable Analog Signal Output The analog signal output can be distributed to a recording device. For details refer to the description of the module’s main board. 1290 Infinity Quaternary Pump User Manual...
Page 258 APG Remote The APG Remote connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. Remote control allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.
Page 259 The module includes a DC-Out (24 VDC) power line that is intended to be used with certain modules that operate as CAN slaves, for example external valves. The line has a limited output of 1.7 A and is self resetting. 1290 Infinity Quaternary Pump User Manual...
Page 260: Setting The 8-Bit Configuration Switch
• For boot/test modes switches 1+2 must be UP plus required mode. For normal operation use the default (best) settings. N O T E Figure 33 Location of Configuration Switch (example shows a G4212A DAD) 1290 Infinity Quaternary Pump User Manual...
Page 261 When selecting the mode TEST, the LAN settings are: Auto-Negotiation & Using Stored. N O T E For explanation of "Boot Resident System" and "Revert to Default Data (Coldstart)" refer N O T E “Special Settings” on page 262. 1290 Infinity Quaternary Pump User Manual...
Page 262: Special Settings
Forced cold start erases all methods and data stored in the non-volatile memory. Exceptions are calibration settings, diagnosis and repair log books which will not be erased. ➔ Save your methods and data before executing a forced cold start. 1290 Infinity Quaternary Pump User Manual...
Page 263 Setting the 8-bit Configuration Switch If you use the following switch settings and power the instrument up again, a forced cold start has been completed. Table 13 Forced Cold Start Settings (On-board LAN) Mode Select TEST/BOOT 1290 Infinity Quaternary Pump User Manual...
Page 264: Early Maintenance Feedback
EMF limits, and then reset the EMF counters to zero. The next time the EMF counters exceed the new EMF limits, the EMF flag will be displayed, providing a reminder that maintenance needs to be scheduled. 1290 Infinity Quaternary Pump User Manual...
Page 265: Instrument Layout
• the plastic layers help cushion the electronic and mechanical parts from physical shock, and • the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself. 1290 Infinity Quaternary Pump User Manual...
Page 266 Hardware Information Instrument Layout 1290 Infinity Quaternary Pump User Manual...
Page 267 1290 Infinity Quaternary Pump User Manual LAN Configuration What You Have To Do First TCP/IP Parameter Configuration Configuration Switch Initialization Mode Selection Dynamic Host Configuration Protocol (DHCP) General Information (DHCP) Setup (DHCP) Link Configuration Selection Manual Configuration With Telnet With the Instant Pilot (G4208A)
Page 268: Lan Configuration What You Have To Do First
268) to • the PC network card using a crossover network cable (point-to-point) or • a hub or switch using a standard LAN cable. Figure 35 Location of LAN interfaces and MAC label 1290 Infinity Quaternary Pump User Manual...
Page 269: Tcp/Ip Parameter Configuration
(short form ‘init mode’) defines how to determine the active TCP/IP parameters after power-on. The parameters may be derived from non-volatile memory or initialized with known default values. The initialization mode is selected by the configuration switch, see Table 15 page 271. 1290 Infinity Quaternary Pump User Manual...
Page 270: Configuration Switch
To perform any LAN configuration, SW1 and SW2 must be set to OFF. N O T E Table 14 Factory Default Settings Link Configuration speed and duplex mode determined by auto-negotiation, for details see “Link Configuration Selection” on page 276 1290 Infinity Quaternary Pump User Manual...
Page 271: Initialization Mode Selection
When initialization mode Using Stored is selected, the parameters are taken from the non-volatile memory of the module. The TCP/IP connection will be established using these parameters. The parameters were configured previously by one of the described methods. Figure 37 Using Stored (Principle) 1290 Infinity Quaternary Pump User Manual...
Page 272 In the Using Default mode, the parameters stored in the memory of the module are not N O T E cleared automatically. If not changed by the user, they are still available, when switching back to the mode Using Stored. 1290 Infinity Quaternary Pump User Manual...
Page 273: Dynamic Host Configuration Protocol (Dhcp)
2 It may be necessary to fully qualify the hostname with the DNS suffix, e.g. 0030d3177321.country.company.com. 3 The DHCP server may reject the hostname proposed by the card and assign a name following local naming conventions. 1290 Infinity Quaternary Pump User Manual...
Page 274: Setup (Dhcp)
Interface Card or Main Board). This MAC address is on a label on the card or at the rear of the main board, e.g. 0030d3177321. On the Local Controller the MAC address can be found under Details in the LAN section. Figure 40 LAN Setting on Instant Pilot 1290 Infinity Quaternary Pump User Manual...
Page 275 Lab Advisor, Firmware Update Tool) and use MAC address as host name, e.g. 0030d3177321. The LC system should become visible in the control software (see Note in section “General Information (DHCP)” on page 273). 1290 Infinity Quaternary Pump User Manual...
Page 276: Link Configuration Selection
SW 5 Link Configuration speed and duplex mode determined by auto-negotiation manually set to 10 Mbps, half-duplex manually set to 10 Mbps, full-duplex manually set to 100 Mbps, half-duplex manually set to 100 Mbps, full-duplex 1290 Infinity Quaternary Pump User Manual...
Page 277: Manual Configuration
Therefore, manual configuration can be done at any time. A power cycle is mandatory to make the stored parameters become the active parameters, given that the initialization mode selection switches are allowing Figure 41 Manual Configuration (Principle) 1290 Infinity Quaternary Pump User Manual...
Page 278: With Telnet
Handheld Controller, or the default IP address (see “Configuration Switch” on page 270). When the connection was established successfully, the module responds with the following: Figure 43 A connection to the module is made 1290 Infinity Quaternary Pump User Manual...
Page 279 Then press [Enter], where parameter refers to the configuration parameter you are defining, and value refers to the definitions you are assigning to that parameter. Each parameter entry is followed by a carriage return. 1290 Infinity Quaternary Pump User Manual...
Page 280 IP setting to Initialization mode is Using Stored active TCP/IP settings stored TCP/IP settings in non-volatile memory connected to PC with controller software (e.g. Agilent ChemStation), here not connected Figure 46 Telnet - Change IP settings 1290 Infinity Quaternary Pump User Manual...
Page 281 If the Initialization Mode Switch is changed now to “Using Stored” mode, the instrument N O T E will take the stored settings when the module is re-booted. In the example above it would be 134.40.27.99. 1290 Infinity Quaternary Pump User Manual...
Page 282: With The Instant Pilot (G4208A)
Figure 48 Instant Pilot - LAN Configuration 5 Press the Edit button (only visible if not in Edit mode), perform the required changes and press the Done button. 6 Leave the screen by clicking Exit. 1290 Infinity Quaternary Pump User Manual...
Page 283: Pc And User Interface Software Setup Setup
This procedure describes the change of the TCP/IP settings on your PC to match the module’s default parameters in a local configuration (see also “Initialization Mode Selection” on page 271). Figure 49 Changing the TCP/IP settings of the PC 1290 Infinity Quaternary Pump User Manual...
Page 284: User Interface Software Setup
LAN Configuration PC and User Interface Software Setup Setup User Interface Software Setup Install you user interface software according the provided User Interface Software Setup Guide. 1290 Infinity Quaternary Pump User Manual...
Page 285: Appendix
1290 Infinity Quaternary Pump User Manual Appendix General Safety Information General Safety Information Safety Standards General Before Applying Power Ground the Instrument Do Not Operate in an Explosive Atmosphere Do Not Remove the Instrument Cover Do Not Modify the Instrument...
Page 286: General Safety Information
Do not use this product in any manner not specified by the manufacturer. The protective features of this product may be impaired if it is used in a manner not specified in the operation instructions. 1290 Infinity Quaternary Pump User Manual...
Page 287: Before Applying Power
Verify that the voltage range and frequency of your power distribution matches to the power specification of the individual instrument. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. ➔...
Page 288: Do Not Operate In An Explosive Atmosphere
WA R N I N G Personal injury (for example electrical shock, intoxication) ➔ Instruments that appear damaged or defective should be made inoperative and secured against unintended operation until they can be repaired by qualified service personnel. 1290 Infinity Quaternary Pump User Manual...
Page 289: Solvents
For details, see the usage guideline for the solvent cabinet. A printed copy of the guideline N O T E has been shipped with the solvent cabinet, electronic copies are available in the Agilent Information Center or via the Internet. 1290 Infinity Quaternary Pump User Manual...
Page 290: Safety Symbols
European Community directives. The European Declaration of Conformity is available at: http://regulations.corporate.agilent.com/DoC/search.htm Manufacturing date. Power symbol indicates On/Off. The apparatus is not completely disconnected from the mains supply when the power switch is in the Off position 1290 Infinity Quaternary Pump User Manual...
Page 291 C AU T I O N alerts you to situations that could cause loss of data, or damage of equipment. ➔ Do not proceed beyond a caution until you have fully understood and met the indicated conditions. 1290 Infinity Quaternary Pump User Manual...
Page 292: Waste Electrical And Electronic Equipment (Wee) Directive
The affixed label indicates that you must not discard this electrical/electronic product in domestic household waste. Do not dispose of in domestic household waste N O T E To return unwanted products, contact your local Agilent office, or see http://www.agilent.com for more information. 1290 Infinity Quaternary Pump User Manual...
Page 293: Radio Interference
Appendix Radio Interference Radio Interference Cables supplied by Agilent Technologies are screened to provide optimized protection against radio interference. All cables are in compliance with safety or EMC regulations. Test and Measurement If test and measurement equipment is operated with unscreened cables, or...
Page 294: Sound Emission
This product has a sound pressure emission (at the operator position) < 70 dB. • Sound Pressure Lp < 70 dB (A) • At Operator Position • Normal Operation • According to ISO 7779:1988/EN 27779/1991 (Type Test) 1290 Infinity Quaternary Pump User Manual...
Page 295: Agilent Technologies On Internet
Appendix Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com 1290 Infinity Quaternary Pump User Manual...
Page 296 DHCP drive position limit remote general information drive timeout RS-232 setup fan failed cables dimensions flow rate limit exceeded analog 1290 Infinity Quaternary Pump User Manual...
Page 297 1290 Infinity Quaternary Pump User Manual...
Page 298 Optimization reading of multi purpose valve tag physical specifications failed power consideration reading the pump encoder tag failed non-operating altitude power consumption remote non-operating temperature cable power cords remove power switch 1290 Infinity Quaternary Pump User Manual...
Page 299 (MCGV) forced cold start specification 1290 Infinity Quaternary Pump User Manual...
Page 300 In This Book This manual contains technical reference information about the Agilent 1290 Infinity Quaternary Pump G4204A. The manual describes the following: • Introduction, • Site requirements and specifications, • installation, • configuration, • using and optimizing, • troubleshooting and diagnostic, •...

Agilent Technologies 1290 Infinity User Manual

Table of Contents

1 Introduction Features

2 Site Requirements and Specifications

3 Installing the Module

4 Using the Module

5 How to Optimize the Performance of Your Module

7 Error Information

9 Maintenance

10 Parts and Materials

11 Identifying Cables

12 Hardware Information

13 LAN Configuration

14 Appendix

Quick Links

Chapters

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Summary of Contents for Agilent Technologies 1290 Infinity