D
Preparing the High Mass Range Calibration Solution
Supplies
80
Orbitrap Tribrid Series Getting Started Guide
Table 12. Required chemicals
Description
Acetic acid, glacial
Acetonitrile (ACN)
Ammonium hydroxide, 28–30%
Enfuvirtide, 100 mg
Methanol
Water
a
American Chemical Society
IMPORTANT
• Do not filter solvents. Filtering solvents can introduce contamination.
• Do not use plastic pipettes to prepare these solutions. Plastic products can release
phthalates that can interfere with the analyses.
Table 13. Required equipment
Description
Bottle, glass, 100 mL
Bottle, glass, 500 mL
Cylinder, glass, 100 mL
Cylinder, glass, 250 mL
a
Gloves, nitrile
(Fisher Scientific
19-120-2947 or
Pipet tips, 100 μL
Pipetter, 100–1000 μL
Sonicator
Spatula, stainless steel
Syringes, glass, 500 μL
Vial, scintillation, glass, 20 mL
Vortex mixer
Weighing container
Weight scale
a
Multiple sizes are available.
Grade
Optima LC/MS
Optima UHPLC/MS
a
Certified ACS
Plus
–
Optima UHPLC/MS
Optima UHPLC/MS
Unity Lab Services
23827)
Part number
A113
A956
A669
HAZMAT-01-00083
A458
W8-1
Quantity
1
1
1
1
–
3
1
1
1
3
1
1
1
1
Thermo Scientific