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Thermo Scientific Manuals
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Prima PRO
User manual
Thermo Scientific Prima PRO User Manual
Mass spectrometers
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Contents
Table of Contents
Troubleshooting
Bookmarks
Table of Contents
Table of Contents
Chapter 1 Introduction
Chapter 2 Safety Information
Overview
Safety Conventions and Symbols
System Safety
Connecting the Instrument to the Electrical Supply
Repair & Maintenance
Changing the Rotary Pump Oil
Switching on the Rotary Pump
Rotary Pump Exhaust Outlet
Inlet System Exhaust
Gas Mixtures in the Inlet System
Protective Clothing
Hazardous Materials
Hazardous Area Systems
Fan Noise
Chapter 3 Site Requirements
Physical Installation
Cable Entries
Safe Area Systems
Hazardous Area Systems
Computer and Communications
Fibre Optic Communication
Hazardous Area Systems
Environment
General
Temperature
Humidity
Vibration
Particulate Contamination
Altitude
Inlet Gas Connections
Calibration Gases
Sample Gases
Exhaust Gas Connections
Power
Voltage and Frequency
Requirements
Over-Current Protection
Power Quality
Power Connection
Other Services
Safe Area Systems
Dry Gas Vent
Enclosure Purge
Hazardous Area Systems
Dry Gas Vent
Rotary Pump Purge
Compressed Air Requirements
Options
Pump Purge Gas
Rotary Oil Box Purge
Rotary Pump Ballast
Turbo Pump Bearing Purge
External I/O Unit
Chapter 4 Handling & Storage
Receiving the Instrument
Unpacking the Instrument
Storing the Instrument
Chapter 5 Installation & Interconnection
Introduction
Positioning the Instrument
Cable Connections
General Requirements
Safe Area Systems
Hazardous Area Systems
Power Connection
Safe Area Systems
Sentinel PRO Sample Pump Power Connection
Safe Area Systems
Hazardous Area Systems
Gas Connections
Computer System
Chapter 6 Commissioning
General
Procedure
Chapter 7 Startup & Shutdown
Startup
Procedure
Vacuum Gauge Trip Level
Checking Instrument Tuning and Mass Alignment
Emission
Peak Shape
Sensitivity
Detectors
Mass Alignment
Heaters
Shutdown
Introduction
Shutdown Procedure
Emergency Shutdown
Chapter 8 Status & Tuning Parameters
Instrument Status
Source Tab
Electron Energy
Emission
Filament Current
Filament Current Limit
Filament Integrity
In Current Limit
Ion Energy
Repeller Voltage
Source Current
Source Temperature
Trap Current
Analyser Tab
ASU Controller Status
Cabinet Temperature
Electronics Temperature
Magnet Controller Status
Mass Filter
Pressure Set Point
System Pressure
System Pressure Trip
Turbo Motor Current
Turbo Operating Hours
Turbo Speed
Turbo Speed Interlock
Vacuum
Vent Valve
Inlet
Pressure Raw
RMS Ambient Temperature
RMS Body Temp
RMS Controller Status
RMS Sample Flow Sensor
RMS Flow Zero
Sample Tube Temperature
Collector Tab
Faraday Deflector
Multiplier Deflector
Multiplier Voltage
Negative and Positive Quad Lens Voltages
Resolution
Power
Amplifier +24V
Analyser Supplies +24V
Instrument CPU 24V
Fan 24V
Inlet Probe Current
Magnet Supply Current
Magnet Sync AC
Power Controller Status
Turbo 24V
User IO 24V
Vent Valve 24V
Communications
Host Comms Quiet
User I/O 0 Comms Quiet
User I/O 1 Comms Quiet
User I/O 2 Comms Quiet
Chapter 9 Fault Diagnosis
Alarm Conditions
Leak Detection
Mass Spectrometer Faults
No Peaks
Poor Sensitivity
Poor Stability on Startup
Poor Results Following Calibration
Ion Source and Magnet Pole Pieces Assembly
Filament Failure
Chapter 10 Maintenance
Maintenance Schedule
Procedures
Rotary Pump Oil Level
Cleaning the Cooling Fans
Lubricating the Turbo Molecular Pump
Dismantling and Cleaning Procedures
Filament
Ion Source
Magnet Pole Piece Assembly
Fuses
Appendix A Hazardous Area Operation
Introduction
Installation
General Hazardous Area Work
Commissioning and Maintenance
Routine Checks
Hazardous Area - General
Area Classification
Gas Classification
Methods of Protection
Purge/Pressurisation
Flameproof (Europe) or Explosion Proof (North America
Increased Safety
Non-Electrical
Purge Operation
Purge Overview
Purge Operation Requirements
Parameter Measurement
Sample Containment System
Definition and Description
Parameters
Leakage Handling
Inspection and Testing
Enclosure Leak Testing
Purge Operation and Testing
All System Types
ATEX, Iecex and X-Purge Systems
Z-Purge Systems
Other Hazardous Area Considerations
Temperature
Over-Temperature Protection
Batteries
Dry Gas Vent
Rotary Vacuum Pump
General
Thermal Trip
Purge
Calibration Panels
Air Conditioner
Remote / Dual RMS
RMS and Instrument in Hazardous Area
RMS in Hazardous Area and Instrument in Safe Area
Sample Pump (Sentinel PRO Applications
Fibre Optic Communications
Service Replacement Items
Troubleshooting
Standards Conformance
Introduction to the Prima PRO Hardware
Main Components
Principle of Operation
Vacuum System
Ion Source
Filaments
Mass Analyser
Collector
Ion Detection
MCP Detector Assembly
MCP Operation
Faraday Detector
Introduction of a Gas Sample
Mass Spectrometer Parameters
Sensitivity
Resolution
Cracking Patterns
Ion Types
Molecular Ion
Isotope Ions
Fragment Ions
Multiple-Charged Ions
Rearrangement and Recombination Peaks
Definitions
Appendix C Technical Description: Inlet
Rapid Multi-Stream Sampler (RMS
Introduction
Safety
Inlet Specification
Inlet Operation
General Description
Connection to the Mass Spectrometer
Seals
Inlet Selection
Calibration Gas Control
Gas Connection
Exhaust Connection
Heating
Main Body Heater
Sample Tube Heater
Flow Sensor
Digital Inputs
Vginet
Inlet Testing
Functional Testing
Cross Port Leakage
External Leakage
Maintenance
Routine Maintenance
Sample Tube Removal
Inlet Ports
Cleaning Procedure
Inlet Options
Remote Mounting
Dual RMS
Solenoid Inlet
Introduction
Inlet Operation
Valve Operation
Capillary Connection
Heating
Inlet Controller
General
Valve Drives
Manifold Heater
Microcapillary Block Heater
Flow Sensor
Digital Inputs
Vginet
Testing
Capillary Testing
Valve Function
Cross Seat Leakage
External Leakage
Maintenance
Calibration Inlet
Sample Inlet
Cleaning Procedure
Appendix D Local I/O
Introduction
Serial I/O
Serial Link Type Selection
Indicators
Fibre Optic Serial Connection
Supplying Power to the External I/O Circuit
Indicators
Analogue I/O
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Prima PRO / Sentinel PRO
Mass Spectrometers
User Guide
P/N 209-230-510
Revision 10
Part of Thermo Fisher Scientific
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