Load The Checkout Method In The Hs - Agilent Technologies 7697A Installation And Startup Manual

Load the Checkout Method in the HS

Installation and First Startup
Using the HS front panel, load the checkout method.
Press [Load][Method].
1
Scroll to select Checkout, then press [Enter].
2
The checkout method will load. The HS will begin heating
and adjusting flows to the initial conditions.
Once the front display reads Ready, let he HS sampler
stabilize for 25 to 30 minutes before running the checkout
sample. This hold time ensures thermal stability and that
any residual moisture or other contaminants are swept from
the system.
For reference, Table 10
setpoints and configuration.
Table 10 Headspace checkout parameters
Configuration
Vial Gas type
Loop Volume (mL)
Advanced Functions
Extraction mode
Purge flow
Purge time
Temperature
Oven
Loop/Valve
Transfer line
Time
GC cycle time
Vial equib time
Pres equib time
Inject time
Vial
lists the headspace sampler checkout
He
1
Single
100.0
1.000
100.0 °C
110 °C
115 °C
4 min. (FID, NPD)
5 min. (µECD)
6.5 min. (MS, MSD)
7 min.
0.1 min.
0.5 min
2
First Startup
55