Endress+Hauser Analytik Jena PlasmaQuant MS Series Installation Manual page 4

Contents
4
6.3 Instrument Tool Box ........................................................................................ 47
6.4 Connecting the Argon ...................................................................................... 47
6.5 Connecting the Mains Power .......................................................................... 48
6.5.1 Connecting the Instrument to Mains Power .............................................. 49
6.6 Connecting the Exhaust Ducting ..................................................................... 51
6.7 Connecting the Leybold SV40 PFPE Rotary Pump ......................................... 51
6.8 Installing the ASpect MS Software ................................................................. 53
6.9 Connecting the PC and Loading the USB Driver ............................................ 60
6.10 Enabling the Service Diagnostics Software .................................................... 63
6.11 Connecting the Water Cooling System ........................................................... 64
7 Vacuum System Startup ............................................................................................ 68
8 ASpect MS Software Setup ....................................................................................... 69
9 Instrument Optimization .......................................................................................... 71
9.1 Starting and Warming Up the Instrument ..................................................... 71
9.2 Calibrations....................................................................................................... 73
9.3 Plasma Alignment ............................................................................................ 74
9.4 Resolution and Trim ........................................................................................ 75
9.5 Mass Calibration .............................................................................................. 77
9.6 Setting the Detector Voltage ........................................................................... 78
10 Method Optimization ........................................................................................... 80
10.1 Typical Optimization Parameters ................................................................... 80
10.2 Optimizing the Ion Optics ................................................................................ 83
10.2.1 How to Perform an Auto Optimization .................................................. 83
10.3 Method Optimization Troubleshooting .......................................................... 85
11 Performance ......................................................................................................... 86
11.1 Analytical Performance Specifications ........................................................... 86
11.1.1 Sensitivity ................................................................................................. 86
11.1.2 Background .............................................................................................. 87
11.1.3 Oxide Ratio .............................................................................................. 87
11.1.4 Doubly-Charged Ratio ............................................................................. 87
11.1.5 Precision (RSD %) ................................................................................... 88
11.1.6 Resolution ................................................................................................ 88
11.1.7 iCRC Check ............................................................................................... 88
11.1.8 Boost Check ............................................................................................. 89
11.2 Test Solutions ................................................................................................... 90
12 Appendix A - Routine Maintenance .................................................................... 92
PlasmaQuant MS Series