Endress+Hauser Analytik Jena PlasmaQuant MS Series Manuals

Endress+Hauser Analytik Jena PlasmaQuant MS Series Manuals

Manuals and User Guides for Endress+Hauser Analytik Jena PlasmaQuant MS Series. We have 2 Endress+Hauser Analytik Jena PlasmaQuant MS Series manuals available for free PDF download: Service Manual, Installation Manual

Endress+Hauser Analytik Jena PlasmaQuant MS Series Service Manual

Endress+Hauser Analytik Jena PlasmaQuant MS Series Service Manual (221 pages)

ICP MS

Brand: Endress+Hauser | Category: Laboratory Equipment | Size: 15 MB

Table of Contents

Table of Contents

3
- Service Manual
  1
- Plasmaquant MS Series ICP MS
  1
  - Table of Contents
    3
- Contents
  3
- Safety Practices and Hazards
  9
- Safety Messages and Symbols
  9
- Warning Symbols
  10
- Color Coding
  10
- Information Symbols
  11
- General Safety Hazards
  11
- Plasma
  11
- Table 1 - Information Symbols
  11
- Electricity
  12
- Compressed Gas
  13
- Heat, Ozone, Vapors, and Fumes
  14
- Hazardous Materials
  14
- Radio Frequency Radiation
  15
- Ultraviolet Radiation
  15
- ICP-MS Equipment Caution Notices
  15
- Regulatory Compliance
  16
- Federal Communications Commission Advisory (U.S. Only)
  16
- Spurious and Harmonic Radiation Compliance
  16
- CE Compliance
  17
- Maintaining Records
  17
- Before You Begin
  18
- Safety Requirements
  18
- Audience
  18
- Introduction
  18
- Additional Resources
  19
- Table 2 - Resources and Contact Information
  19
- Preventative Maintenance Overview
  20
- Sample Introduction
  22
- System Description
  22
- Theory of Operation
  23
- Nebulizer
  23
- Peristaltic Pump
  24
- Spray Chamber
  24
- Sheath Gas Accessory Port
  25
- Torch
  25
- Sample Introduction PCB
  26
- Safety and Operational Information
  26
- Specifications
  28
- Maintenance
  28
- Cleaning the Torch
  29
- Removing and Replacing the Nebulizer
  30
- Cleaning the Concentric Nebulizer
  30
- Removing and Replacing the Spray Chamber
  31
- Cleaning the Spray Chamber
  32
- Replacing the Peristaltic Pump Tubing
  32
- Removing the Peristaltic Pump Assembly
  33
- Gas Control System
  34
- System Description
  34
- Instrument Gas Control
  34
- Table 3 - Solenoid Valve Functions Within Gas Control Assembly
  36
- Icrc Gas Control
  38
- Theory of Operation
  41
- Instrument Gas Control
  41
- Table 4 - Sample Introduction PCB Diagnostic LED Identification
  43
- Icrc Gas Control
  45
- Safety and Operational Information
  45
- Specifications
  45
- Replacement/Maintenance
  46
- Table 5 - Instrument Gas Control Specifications
  46
- Cover Removal Procedures to Access the Gas Control Box
  47
- Removal of Sample Introduction PCB
  48
- Removing Sheath Gas, Nebulizer and Nitrox Mass Flow Controllers
  49
- Removing the Argon Inlet Manifold with RG1 and RG2 Attached
  50
- Removing Plasma/Auxiliary Gas Flow Manifold
  51
- Checking Plasma Gas Flows
  52
- Checking Auxiliary Gas Flows
  53
- Igniter Assembly
  54
- Checking Sheath Gas Flow (MFC2)
  54
- Checking Nebulizer Gas Flow (MFC1)
  55
- Adjusting Gate Valve
  55
- Removing and Maintaining the Icrc Box Assembly
  56
- Plasma Generation
  60
- System Description
  60
- Theory of Operation
  60
- Plasma Formation
  60
- Igniter Assembly
  61
- RF Generator Module
  62
- DC Power Supply Module
  64
- Translation Mechanism
  65
- Table 6 - Definition of Translator X, y and Z Planes
  65
- Table 7 - Example of Motor Steps Relative to Position (MM) for Depth Mechanism
  65
- Plasma Start-Up Procedure
  66
- Table 8 - Example of Motor Steps Relative to Position (MM) for Vertical Mechanism
  66
- Table 9 - Example of Motor Steps Relative to Position (MM) for Horizontal Mechanism
  66
- Safety and Operational Information
  67
- Specifications
  68
- Table 10 - RF Generating System Specifications
  69
- Maintaining Translator Platform
  69
- Repairing DC Power Supply
  69
- Repairing RF Generator
  69
- Maintenance
  69
- Replacing Torch
  70
- Removing and Replacing the RF Generator
  70
- Replacing, Aligning, and Adjusting the Plasma Coil
  72
- Removing RF Enclosure Filter Assembly
  80
- Removing Translator Platform
  81
- Removing the X-Axis Drive Mechanism
  83
- Removing the Y-Axis Drive Mechanism
  84
- Removing the Z-Axis Drive Mechanism
  85
- Replacing the DC Supply Module
  85
- Removing Igniter Assembly
  87
- Calibrating Translator Platform
  87
- System Description
  90
- Vacuum System
  90
- Theory of Operation
  93
- Vacuum System Start up
  93
- Table 11 - Vacuum Gauge Trip Points
  94
- Vacuum System Monitor Sequence
  95
- Vacuum System Shutdown Sequence
  96
- Vacuum Vent Device
  97
- The Thermocouple Gauge
  98
- The Penning Vacuum Gauge
  99
- Thermovac Transmitter (Gmain)
  100
- Turbo-Molecular Pumps Turbo1 and Turbo2
  102
- Safety and Operational Information
  103
- Specifications
  103
- Table 12 - Vacuum Chamber Specifications
  105
- Maintenance
  106
- Removing Turbo-Molecular Pumps 1 and 2
  106
- Removing Gate Valve Assembly and Gate Valve Piston Assembly
  107
- Checking and Changing Oil in Rotary Pumps
  109
- Maintaining Turbo-Molecular Pumps
  110
- Removing Thermocouple Gauge Head (G1)
  111
- Mass Spectrometer
  112
- Introduction
  112
- System Description
  112
- Theory of Operation
  113
- Ion Source
  113
- Interface Assembly
  114
- Ion Optics System
  117
- Mass Analyzer Assembly
  128
- Detector
  133
- Cone Specifications
  138
- Table 13 - Attenuation Factor Specifications
  138
- Safety Information and Operational Tips
  139
- Table 14- Ion Optics Elements and Their Effects on Sensitivity
  141
- Maintenance
  142
- Removal and Replacement Procedures
  144
- Cones
  144
- Detector Assembly
  147
- Mass Analyzer Assembly
  150
- Ion Lens System
  152
- System Description
  156
- Quadrupole Controller
  156
- Quadrupole DC Power Supplies
  157
- Quadrupole Controller Cooling
  158
- Control PCB
  158
- RF Modulator and Driver
  158
- RF Detection Circuitry
  158
- RF Output Transformer
  158
- RF Power Amplifier PCB
  159
- Connection Mass Analyzer
  159
- Theory of Operation
  159
- Power Supply
  160
- DC Control Circuit
  160
- RF Modulator
  161
- Error Detection
  161
- RF Servo-Loop
  161
- Safety and Operational Information
  162
- RF Detector
  162
- Error Generation
  162
- Specifications
  163
- Maintenance
  164
- Removing Quadrupole Controller
  164
- Quadrupole Control Drive Looms
  167
- Setting Rest Mass
  169
- Adjusting Resonation
  169
- System Description
  173
- Electronics System Functional Overview
  173
- Introduction
  173
- Electronics
  173
- Vacuum System Functionality
  174
- Plasma System Functionality
  176
- Ion Signal Control and Processing
  178
- Communication Functionality
  179
- Instrument Power Supplies
  180
- Instrument Interlocks and Sensors
  180
- Theory of Operation
  182
- System Control PCB
  182
- Amplifier/Discriminator PCB
  183
- Sample Introduction Interconnect PCB
  184
- Safety Information and Operational Tips
  188
- Table 15 - Thermistor Results and Possible Causes for Spray Chamber Fault Monitoring
  188
- Ion Optics High Voltage Power Supply
  189
- Power Supply
  189
- System Description
  189
- Introduction
  189
- Quadrupole Controller
  190
- Electrical Box Module
  190
- RF Generator
  191
- Utility Module
  191
- Theory of Operation
  192
- Ion Optics & Detector Supply PCB
  192
- Table 16 - Assignment of Bits Sent to the CPU Board
  195
- Testing and Servicing
  197
- Table 17 - Fundamental Properties of each Electrode
  197
- Testing at the Board Level
  198
- Table 18 - LED Summary on Ion Optics and HV Supply Board
  199
- Specifications
  202
- Troubleshooting
  203
- Schematics
  204
- Parts and Equipment
  205
- Tools, Test Equipment, Software and Documentation
  205
- Recommended Spare Parts List
  206
- Maintenance Forms and Checklists
  211
- Routine Maintenance Schedule
  211
- Operator Checklist
  213
- Preventative Maintenance Checklist
  214
- Figures
  217
Tables

221

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Endress+Hauser Analytik Jena PlasmaQuant MS Series Installation Manual

Endress+Hauser Analytik Jena PlasmaQuant MS Series Installation Manual (92 pages)

ICP MS

Brand: Endress+Hauser | Category: Laboratory Equipment | Size: 20 MB

Table of Contents

Installation Guide
1
Plasmaquant MS Series ICP MS
1
Table of Contents
3
Safety Practices and Hazards
5
Safety Messages and Symbols
5
Warning Symbols
6
Color Coding
6
Information Symbols
7
General Safety Hazards
7
Plasma
7
Electricity
8
Compressed Gas
9
Heat, Ozone, Vapors, and Fumes
10
Hazardous Materials
10
Radio Frequency Radiation
11
Ultraviolet Radiation
11
ICP-MS Equipment Caution Notices
11
Regulatory Compliance
12
Federal Communications Commission Advisory (U.S. Only)
12
Spurious and Harmonic Radiation Compliance
12
CE Compliance
13
Maintaining Records
13
Introduction
14
Installation Overview
15
System Interconnection
16
Unpacking the Instrument
17
Shipping Kit
18
Instrument Setup
20
Installing the Rotary Pump
20
Installing the Sample Introduction System
21
Installation of the Torch
22
Installation of the Nebulizer
24
Installation of the Spray Chamber
25
Installation of the Transfer Tube
26
Installation of the Peristaltic Pump Tubing
28
Installation of the ASPQ 3300 Autosampler
31
Installation of the CETAC ASX-560 Autosampler
35
Instrument Tool Box
47
Connecting the Argon
47
Connecting the Mains Power
48
Connecting the Instrument to Mains Power
49
Connecting the Exhaust Ducting
51
Connecting the Leybold SV40 PFPE Rotary Pump
51
Installing the Aspect MS Software
53
Connecting the PC and Loading the USB Driver
60
Enabling the Service Diagnostics Software
63
Connecting the Water Cooling System
64
Vacuum System Startup
68
Aspect MS Software Setup
69
Instrument Optimization
71
Starting and Warming up the Instrument
71
Calibrations
73
Plasma Alignment
74
Resolution and Trim
75
Mass Calibration
77
Setting the Detector Voltage
78
Method Optimization
80
Typical Optimization Parameters
80
Optimizing the Ion Optics
83
How to Perform an Auto Optimization
83
Method Optimization Troubleshooting
85
Performance
86
Analytical Performance Specifications
86
Sensitivity
86
Background
87
Oxide Ratio
87
Doubly-Charged Ratio
87
Precision (RSD %)
88
Resolution
88
Icrc Check
88
Boost Check
89
Test Solutions
90
Appendix A - Routine Maintenance
92

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