Agilent Technologies MSD 5977B Series Operating Manual page 48

2 Installing 8890 GC Columns
To Install a Capillary Column in the GC/MSD Interface Using a Standard Column Nut

 Procedure
Always wear clean gloves while handling any parts that go inside the GC or the
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analyzer chambers.
The analyzer, GC/MSD interface, and other components in the analyzer
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chamber operate at very high temperatures. Do not touch any part until you
are sure it is cool.
1 Condition the column.
Dangerous voltages exist inside the analyzer chamber, which can result in
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fatal injury. Do not open the analyzer chamber door for any reason. If access is
ever required, trained service personnel must first disconnect the instrument
from the building power source.
2 Vent the MSD and open the analyzer chamber. (See
The GC operates under high temperatures. Do not touch any GC parts unless
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you are certain they are cool.
3 If installed, remove the knurled tip seal retainer, interface tip seal, and spring
4 Slide an interface nut and conditioned ferrule onto the free end of the GC
5 Slide the column into the GC/MSD interface.
Do not break the column off inside the vacuum manifold. Pieces of column
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could fall or be pulled into the turbo pump and damage it.
6 Use the column cutter to score the column 2 cm from the end.
7 While holding the column against the column cutter with your thumb, break
8 Inspect the end for jagged edges or burrs. If the break is not clean and even,
9 Wipe the end with alcohol.
48
page 136 and"To Open the Analyzer Chamber"
can see the end of the GC/MSD interface.
from the end of the GC/MSD interface.
column. The tapered end of the ferrule must point towards the nut.
the column against the edge of the column cutter.
repeat steps 6 and 7.
(See"To Condition a Capillary Column"
5977B Series MSD Operating Manual
on page 41.)
"To Vent the MSD"
on page 176.) Be sure you
on