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Table of Contents
Related Manuals for Metrohm Combustion-IC-System
Summary of Contents for Metrohm Combustion-IC-System
- Page 1 Combustion-IC-System Manual – Short Instructions 8.920.8003EN / 2018-08-31...
- Page 3 Metrohm AG CH-9100 Herisau Switzerland +41 71 353 85 85 info@metrohm.com www.metrohm.com Combustion-IC-System Manual – Short Instructions 8.920.8003EN / 2018-08-31...
- Page 4 Disclaimer Deficiencies arising from circumstances that are not the responsibility of Metrohm, such as improper storage or improper use, etc., are expressly excluded from the warranty. Unauthorized modifications to the product (e.g. conversions or attachments) exclude any liability on the part of the manufacturer for resulting damage and its consequences.
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Page 5: Table Of Contents
................. 18 3.6.3 Connecting the Combustion Oven (TEI) inlet ......20 3.6.4 Connecting the Combustion Oven (TEI) outlet ......21 3.6.5 Connecting the 930 Compact IC Flex ........21 Connecting the LPG/GSS Module ........23 4 Start-up Index Combustion-IC-System ￭￭￭￭￭￭￭￭... - Page 6 Connecting the 6-port valve ............14 Figure 9 Combustion tube – Inlet ..............17 Figure 10 Combustion tube – Outlet ............... 18 Figure 11 Combustion tube – Inlet ..............20 Figure 12 Combustion Oven (TEI) – Outlet ............21 ￭￭￭￭￭￭￭￭ Combustion-IC-System...
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Page 7: About These Short Instructions
Combustion IC system and information on installing the 920 Absorber Module and its interfaces to the Combus- tion-IC-System. You can download the detailed manual for the 920 Absorber Module as a PDF file from the Internet (https://www.metrohm.com). Combustion-IC-System ￭￭￭￭￭￭￭￭... -
Page 8: Introduction
Combustion IC is particularly suited for deter- mining the following elements: Figure 1 Detectable elements An additional instrument is required for the determination of gaseous samples: the LPG/GSS Module (AJ) (2.136.0720) or the GLS Sampler CIC (TEI) (2.0136.0630). ￭￭￭￭￭￭￭￭ Combustion-IC-System... -
Page 9: System Description
The entire process is controlled and monitored using MagIC Net software. The analysis data is saved in the software's database. 2.1.3 Sequence of a determination A determination in the Combustion IC system runs according to the fol- lowing diagram: Combustion-IC-System ￭￭￭￭￭￭￭￭... -
Page 10: Figure 3 Sequence Of The Determination
Absorption solution: Combustion gases dissolved in the absorber ￭ solution. The determination is controlled entirely by MagIC Net. You can find a detailed description of the sequence in the online help for MagIC Net under the title "Combustion sequence". ￭￭￭￭￭￭￭￭ Combustion-IC-System... -
Page 11: Intended Use
The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010. WARNING Only personnel qualified by Metrohm are authorized to carry out service work on electronic components. WARNING Never open the housing of the instrument. The instrument could be damaged by this. -
Page 12: Tubing And Capillary Connections
Avoid applying excessive force to tubing con- nections. Damaged tubing ends lead to leakage. Appropriate tools can be used to loosen connections. Check the connections regularly for leakage. If the instrument is used mainly in unattended operation, then weekly inspections are manda- tory. ￭￭￭￭￭￭￭￭ Combustion-IC-System... -
Page 13: Flammable Solvents And Chemicals
The correct disposal of your old instrument will help to prevent negative effects on the environment and public health. More details about the disposal of your old instrument can be obtained from your local authorities, from waste disposal companies or from your local dealer. Combustion-IC-System ￭￭￭￭￭￭￭￭... -
Page 14: Overview
3.1 Overview ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation Overview Components of the Combustion-IC-System Depending on the application, the Combustion-IC-System consists of the following instruments: Type of sample Instruments Manufacturer solid/liquid samples only Combustion Module with Auto Boat Drive (ABD) Analytik Jena ￭ (2.136.0700) optional: sampler (MMS 5000) ￭... -
Page 15: Figure 4 Capillaries And Tubings In Use - Overview
1/8 OD / 1/16 ID / 1.5 m | Combus- Connection between the 10-port valve and tion Oven (TEI): PTFE capillary 1/8 OD / the waste container. 1/16 ID / 5 m Connection between the absorber tube and the Combustion Module (AJ) / Combustion Oven (TEI). Combustion-IC-System ￭￭￭￭￭￭￭￭... - Page 16 Table 1 Recommended color codes for the flow paths Liquid Colored sleeve Ultrapure water blue ￭￭￭￭￭￭￭￭ Combustion-IC-System...
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Page 17: Dosino For Ultrapure Water
Slip the colored sleeve over the capillary and secure it to the desired spot by heating it, for example by using a hairdryer. Dosino for ultrapure water 3.2.1 Connecting the ports – Overview Figure 5 Connect the Dosino for ultrapure water Combustion-IC-System ￭￭￭￭￭￭￭￭... -
Page 18: Dosino For The Absorber Solution
Combustion oven inlet (see chapter 3.6.1, page 16) You can find detailed instructions in the manual for the 920 Absorber Module. Dosino for the absorber solution 3.3.1 Connecting the ports – Overview Figure 6 Connect the Dosino for the absorber solution ￭￭￭￭￭￭￭￭ Combustion-IC-System... -
Page 19: 10-Port-Valve
The transfer tubing and capillaries for all of the liquids being used are con- nected to the 10-port valve. Connecting the 10-port valve Connect the ports of the 10-port valve according to the following figure: NOTICE We recommend connecting the central port first. Figure 7 Connecting the 10-port valve Combustion-IC-System ￭￭￭￭￭￭￭￭... -
Page 20: 6-Port Valve
Connect the ports of the 6-port valve according to the following figure: 6.1803.160 6.1831.040 6.2744.010 6.2744.010 6.1825.290 6.2744.010 6.2744.010 6.1803.030 6.1803.030 Figure 8 Connecting the 6-port valve Next steps Connect … to capillary/ tubing at port … Waste container ￭￭￭￭￭￭￭￭ Combustion-IC-System... -
Page 21: Connecting The 920 Absorber Module To The Remaining Components
The thicker capillary installed at the inlet of the absorber tube is routed ￭ out at the rear. The other end of the capillary is already connected to the oven outlet. Combustion-IC-System ￭￭￭￭￭￭￭￭... -
Page 22: Connecting The Combustion Module (Aj) Inlet: Water Infeed
2 Shortening the capillary Shorten the capillary using the capillary cutter so that it can be con- nected to the combustion tube's inlet easily. 3 Connecting the capillary Three connections are located at the combustion tube's inlet: ￭￭￭￭￭￭￭￭ Combustion-IC-System... -
Page 23: Figure 9 Combustion Tube - Inlet
Combustion Module operating instructions). Carefully attach the FAST connector to the connector (9-1). ￭ You can find information on connecting the flame sensor, the oxygen infeed and the ABD in the Combustion Module (AJ) operating instructions. Combustion-IC-System ￭￭￭￭￭￭￭￭... -
Page 24: Connecting The Combustion Module (Aj) Outlet: Absorber Solution
For feeding the absorber solution in and colored sleeve (4- removing the combustion gases. Peltier cooler Combustion gases connector For cooling the combustion gases at the Connector for the PTFE capillary, 1/8 / 1/16 combustion tube's outlet. ID / 1.5 m (6.1803.130) (4- ￭￭￭￭￭￭￭￭ Combustion-IC-System... - Page 25 3 Connecting the capillary Plug the capillary into a straight FAST connector (6.7304.010) (see ￭ Chapter "Replacing tubing connections" in the Combustion Mod- ule operating instructions). Carefully attach the FAST connector to the CIC T connector's out- ￭ let (10-1). Combustion-IC-System ￭￭￭￭￭￭￭￭...
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Page 26: Connecting The Combustion Oven (Tei) Inlet
Connecting the Combustion Oven (TEI) inlet Figure 11 Combustion tube – Inlet Argon infeed Oxygen infeed Connection for the argon infeed. Connection for the oxygen infeed. Oxygen infeed Water infeed inlet Connection for the oxygen infeed. Connector for the ultrapure water supply. ￭￭￭￭￭￭￭￭ Combustion-IC-System... -
Page 27: Connecting The Combustion Oven (Tei) Outlet
Combustion Module (AJ): A capillary is routed out on the left side of the 920 Absorber Module. Combustion Oven (TEI): A capillary is routed out on the right side of the 920 Absorber Module. This capillary is connected to the injection valve of the 930 Compact IC Flex. Combustion-IC-System ￭￭￭￭￭￭￭￭... - Page 28 Shorten the end of the capillary using the capillary cutter so that it ￭ can be connected to the injection valve of the 930 Compact IC Flex easily. Connect the end of the capillary to port 1 of the injection valve ￭ (see manual for 930 Compact IC Flex). ￭￭￭￭￭￭￭￭ Combustion-IC-System...
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Page 29: Connecting The Lpg/Gss Module
￭ Connecting the LPG/GSS Module to the combustion tube Prerequisites The Combustion Module and the LPG/GSS Module have to be ￭ switched off. Accessories Oven coupling for LPG/GSS (6.730.4030) ￭ 1 Disassemble the individual components of the adapter. Combustion-IC-System ￭￭￭￭￭￭￭￭... - Page 30 Protective sleeve FAST connector Plastic sleeve Injection needle 2 Attach the FAST connector to the inlet of the combustion tube. 3 Attach the plastic sleeve to the FAST connector. 4 Insert the injection needle into the FAST connector. ￭￭￭￭￭￭￭￭ Combustion-IC-System...
- Page 31 ￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭ 3 Installation Connector for argon Connector for sample 5 Screw the argon supply tubing to Inlet 1. 6 Screw the sample supply tubing to Inlet 2. Combustion-IC-System ￭￭￭￭￭￭￭￭...
- Page 32 Switch on the Combustion Module (AJ): the Combustion Module ￭ (AJ) and the MMS 5000 sampler (AJ) or the LPG/GSS Module (AJ), if present. Switch on the Combustion-IC-System. ￭ Switch on the ion chromatograph. ￭ MagIC Net detects all of the instruments and asks if they are to be saved to the device table.
- Page 33 Switch on the ion chromatograph and the 920 Absorber Module. ￭ MagIC Net detects both instruments and asks if they are to be saved to the device table. Confirm all of the prompts with [Yes]. ￭ Combustion-IC-System ￭￭￭￭￭￭￭￭...
- Page 34 The IC instrument is ready to measure as soon as equilibration has finished. 5 Start the equilibration of the Combustion Oven (TEI) and the Liquid Autosampler CIC (TEI), Solid Autosampler CIC (TEI) or the GLS Sam- pler CIC (TEI), if present, in the TEIS software. ￭￭￭￭￭￭￭￭ Combustion-IC-System...
- Page 35 Safety instructions ...... 5 Combustion IC Service ........5 Definition ......2 Electrostatic charge ....6 Detectable substances ..2 Supply voltage ......6 System description ...... 3 Combustion Module Connect ......15 Installation 6-port valve ......14 Combustion-IC-System ￭￭￭￭￭￭￭￭...
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