CEM MARS 6 iWave Manual
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CEM MARS 6 iWave Manual

Microwave accelerated reaction system
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MARS 6 iWave
Microwave Digestion System
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Summary of Contents for CEM MARS 6 iWave

  • Page 1 MARS 6 iWave Microwave Digestion System Manual...
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  • Page 3: Table Of Contents

    Contents Safety Users Safety Notations Create User Edit/Delete User Introduction Auto Login About the Instrument Password Configuration Important Safeguards Data Management Microwave Safeguards View, Print, and Export Data Instrument Safeguards Activity Log Compounds Unsuitable for Closed Vessel Microwave MARS 6 Screenshot Capture Digestion Calibrations Instrument Overview...
  • Page 4 Glossary Glossary Warranty Limited Warranty Information Technical Assistance Applications Support Technical Support Contact Information CEM Corporation Headquarters CEM International Subsidiaries CEM Authorized Dealers...

  • Page 5: Safety

    Safety Safety Notations This manual uses three safety alert words at points in the documentation where the user should be aware of potential hazards. The safety alerts are shown in color-coded boxes. The three words – NOTE, CAUTION, and WARNING – indicate differing levels of observation or action as described below: NOTE A NOTE is intended to provide emphasis on procedures that may be misinterpreted or overlooked, or to clarify confusing situations.

  • Page 6: Introduction

    CEM’s website at www.cem.com. The MARS 6 iWave® is designed to be operated as outlined in this manual. The iPrep®, EasyPrep™, MARSXpress™, and MARSXpress Plus vessel series are the only approved vessels for this system.

  • Page 7: Important Safeguards

    Important Safeguards General guidelines for safe operation of the MARS 6 iWave system are presented below and all specific safety messages are located throughout the manual. Proper precautions must be taken to avoid contact with acids or acid vapors. Protective gear should be worn as outlined in the user’s safety program for hazardous materials and the acid manufacturer’s safety data sheet.
  • Page 8 vessel microwave digestion because they are highly reactive with oxidizing acids and/or may become nitrated and potentially explosive. Absence of a particular chemical compound from this list does not imply microwave acid decomposition of such a sample is safe under all conditions. •...

  • Page 9: Instrument Overview

    Instrument Overview Front and Side View Item Description Touch Screen Display Shows menus, method parameters, etc. Includes 86 dB speakers Door Handle Permits ease of opening instrument door Internal Printer (optional) Permits printing of method parameters, graphs and/or method data Cooling Fan Draws room air past the electronics Communication Access...

  • Page 10: Back And Side View

    Back and Side View Item Description Power Cord Receptacle Receives the female end of the power cord Cavity Exhaust Outlet Exhausts fumes from the microwave cavity Cavity Exhaust Blower Directs air from the microwave cavity to the exhaust outlet at the rate of 3.6 m /minute (125 /minute) External Sensor Port...

  • Page 11: Cavity

    Cavity Fluoropolymer-coated microwave cavity. Item Description Door Seal Ensures tight fit between door and interior cavity of the MARS 6 to prevent microwave leakage Waveguide Covers Evenly distribute microwaves into instrument cavity Turntable Drive Lug Allows the turntable drive shaft to pass through the cavity floor and engage the Turntable Floor Mat Protects the Teflon Coating on the Floor of the Mars 6 Cavity...

  • Page 12: Software Overview

    Software Overview Software Icons Icon Description Icon Description Icon Description Add Stage Home Back Information Save Blower Import Screen Context Menu Delete iWave System Settings Done Temperature Edit Power Turntable Export Print Filter Remove Stage Software Overview...

  • Page 13: Home Screen

    One Touch® Methods, Classic Methods, and System Settings. • One Touch Methods are methods created and optimized by CEM for a variety of sample types in an effort to reduce method development time required of user. These methods cannot be edited, but they can be copied and the copy can be edited.

  • Page 14: System Settings

    System Settings The following is a basic review of each section of the System Settings to be used as a quick guide for locating software items and instrument functions. • Tools: Calibration and Diagnostic tools to ensure proper system functionality and software update when a new version is released •...
  • Page 15 Settings • General: Views system information, service records, and CEM information • System: Instrument settings for the audio and visual selections for the individual user • Localization: Regional adjustments, including language and the preferred date and time format • Date/Time: Location for setting the correct date and time •...
  • Page 16 Logout • Displays logout screen Software Overview...

  • Page 17: System Installation

    2. Carefully inspect the shipping carton, the instrument, and accessories for any damage that may have occurred during shipping. If the instrument or accessories have damage, contact the freight carrier to report the damage and file a damage report. Contact your CEM Representative for assistance. WARNING If any damage to the instrument is noted, do not attempt instrument operation.
  • Page 18 6. Lay the sides of the box flat and remove the foam from the top of the system. 7. Lift the system, from the sides, onto bench top near exhaust service (two people required). Do not place the system in a fume hood. 8.

  • Page 19: System Setup

    remove plastic & lifting device before using 9. Remove the box from inside of the system cavity. Write down the serial number located on the nameplate on the back left side of the system. 10. Retain all packing material for use if returning the instrument to the manufacturer for service. System Setup 1.
  • Page 20 4. Position the instrument so the door is facing forward and so there is open space to access the power switch. 5. Locate the power switch on the right side of the instrument, and position it in the ON position. 6.
  • Page 21 8.4. Scroll to the “Power” section and select “Line Voltage.” • 60 Hz - select 208 V or 230 V • 50 Hz - select 200 V, 220 V, or 240 V 8.5. Select “Ok” and the Save icon in the upper right corner of the screen. 9.
  • Page 22 - Save the new offset value and proceed with next step. • “Turntable is not aligned. Mechanical alignment is required for turntable offset of +/-XXX.” - DO NOT continue with installation/operation. Contact your CEM Represetative for assistance. 11. System Setup is complete.

  • Page 23: Perform A Digestion

    Perform a Digestion Detailed instructions for each vessel set are outlined in the vessel manual. Read and fully understand all documentation before operating the instrument. iPrep Vessel Series iPrep Vessel Series Manual - P/N 600856 EasyPrep Vessel Series EasyPrep Vessel Series Manual - P/N 600962 MARSXpress Vessel Series MARSXpress Vessel Series Manual - P/N 600968 MARSXpress Plus Vessel Series...

  • Page 24: Methods

    4. Select “Temperature” and enter the desired temperature. 5. Select “Sample Type” and choose the appropriate sample type from the list. • “Organic” is the recommend sample type for most samples. Contact CEM before selecting any other sample types. 6. Select “Hold Time” and enter in the appropriate hold time.

  • Page 25: Export Method

    3. Select “Yes” to delete the method(s) or “No” to return to the previous screen. Export Method Methods will be exported to a USB. 1. Install a USB on the right side of the MARS 6 instrument. 2. Select and hold (long touch) the method to be exported. 3.

  • Page 26: Import Method

    4.2. If “Single File” is selected, then an additional screen will appear and a bundle name will be required. Import Method 1. Install a USB containing the desired method(s) on the right side of the MARS 6 instrument. 2. From the Home Screen, select “Classic” or “One Touch.” 3.

  • Page 27: Users

    4. Scroll down until “Users” section appears. 5. Select “Add User.” 6. Enter the “User Name.” 7. Assign the User Group. • Administrators: Ability to create, edit, and delete any non-CEM method. • Users: Ability to create, edit, and delete their individual methods only. Users...

  • Page 28: Edit/Delete User

    • Basics: Ability to run methods only, no create, edit, or delete capability. NOTE Every system must maintain at least one Administrator. 8. Enter and confirm desired password. 9. Select “Add.” Additional users can be added at this time. Edit/Delete User Only an administrator can edit/delete a user.

  • Page 29: Password Configuration

    Password Configuration Determines password criteria for all users. Only an administrator can change the Auto Login to on/off. 1. Select the System Settings icon in the bottom right corner of the screen. 2. Select Settings. 3. Select Users. Scroll down to “Password Settings“ and toggle to “ON” or “OFF.” •...

  • Page 30: Data Management

    Data Management View, Print, and Export Data View data associated with a specific method. 1. Select the method with the data to view. 2. Select the Information icon. 3. The “Summary” will provide information about the method and the run data will be listed in the order they were run (newest first).

  • Page 31: Activity Log

    Activity Log The Activity Log can be filtered by date range and user. The results can be exported to a “.pdf” file or printed using the internal printer. 1. Select the System Settings icon in the bottom right corner of the screen. 2.
  • Page 32 3. Using the keyboard, select “Ctrl + O” (letter “O”) on the keyboard to save the screenshot to the USB. An on- screen notification will appear (software version ≥ 1.40). 4. Press “OK” to clear the notification. 5. Remove USB and plug into a computer. 6. The screenshot will be saved into the following folder: cem/mars6/screenshots. Data Management...

  • Page 33: Calibrations

    Calibrations Temperature Verification (iWave Sensors) The optional AutoCal calibration device is required for temperature verification. Read and fully understand the AutoCal manual (P/N 600835) before operation. 1. Plug the AutoCal into an electrical outlet close enough to the instrument for it to be placed on the instrument floor.

  • Page 34: Temperature Calibration (Iwave Sensors)

    6. Wait for a stable reading. 7. The temperature should read within ±3 ºC of the AutoCal temperature. If it is outside this range, perform the Temperature Calibration for iWave sensors. Temperature Calibration (iWave Sensors) The iWave temperature calibration procedure should only be performed if the verified temperature is ≥ ±4 ºC of the AutoCal temperature.

  • Page 35: Turntable Calibration

    5. Select Sensor. 6. Select “Inner” or “Outer” and “Ok.” 7. Select “Target” and enter a target temperature. A temperature of 175 ºC should be used for the iWave calibra- tion. 8. Select “Ok.” 9. Ensure that the “Ready” light on the AutoCal is illuminated and place the heating module so it is directly cen- tered 0.5"...
  • Page 36 • “Turntable is not aligned. It is recommended to save the turntable offset of +/-XXX. Do you wish to save?” - Save the new offset value to align the turntable. • “Turntable is not aligned. Mechanical alignment is required for turntable offset of +/-XXX.” - DO NOT continue operating the MARS 6 instrument. Contact your CEM Representative for assistance. Calibrations...

  • Page 37: Power Test

    • The power output from the secondary magnetron should be 800 W. If the measured power is below 712 W, the secondary magnetron is not producing adequate microwave power. • If one or both of the magnetrons is not producing sufficient wattage, contact CEM Corporation. NOTE In order to perform an IEC power test, specialized equipment is required.

  • Page 38: Printer (Optional)

    Printer (Optional) Internal Printer The optional internal thermal printer permits printing of method parameters, graphs, and/or method data at any time that the Print icon is displayed on the screen during method performance or when viewing method information and previous method performance data. Replace Printer Paper 1.

  • Page 39: Software Update

    The MARS 6 software/firmware should be updated when a revised version is released. The software/firmware can be obtained from CEM’s website www.cem.com. One user should be responsible for updating the software. 1. Using a computer, create a folder titled “CEM” on the USB.

  • Page 40: Routine Maintenance

    Routine Maintenance CEM suggests that you perform the routine maintenance on your instrument as outlined below, along with having a CEM Certified Technician to come check out your system once a year. WARNING Proper precautions must be taken to avoid contact with acids or acid vapors. Protective gear should be worn as outlined in the user’s safety program for hazardous materials and the acid manufacturer’s safety...

  • Page 41: Annually

    WARNING Acid can condense and collect inside the blower duct. Annually • Preventative Maintenance by CEM Certified Technician. Contact the CEM Service Department for assistance. As Needed • If installed, replace printer paper. Routine Maintenance...

  • Page 42: Troubleshooting

    Wipe iWave sensors with a lint free damp cloth. correctly Sensor needs calibration If AutoCal Calibration device is available, calibrate sensor as outlined in this manual. If AutoCal calibration device is not available, contact CEM Corporation. Troubleshooting...

  • Page 43: System Specifications

    System Specifications Location Requirements • A fume hood within 8' (2.5 m) of unit or adequate exhaust that pulls a minimum of 125 CFM at point of connection • Never install a MARS 6 inside a fume hood • Provides adequate space for sample handling •...
  • Page 44 • Overvoltage Category II • Pollution degree 2 Conforms to Globally Harmonized EN61010-1 Standard for Safety Requirements for Electric Equipment for Measurement, Control and Laboratory Use Part 1: General Requirements (CAN/CSA-C22.2 No. 1010.1-1992). This instrument complies with United States Code of Federal Regulations 21CFR Part 1030.10 (C) for microwave leakage.
  • Page 45 As of software version 1.49, all TempGuard parameters are preset to CEM factory settings.
  • Page 46 Limited Warranty Information What Is Covered: CEM Corporation warrants that the instrument will be free of any defect in parts or workmanship and will, at its option, replace or repair any defective part (excluding consumables) or instrument. For How Long: This warranty remains in effect for 365 days from date of delivery to the original purchaser.
  • Page 47 CEM Corporation hereby excludes and disclaims any warranty of merchantability or fitness for any particular purpose. No warranty, express or implied, extends beyond the face hereof. CEM Corporation shall not be liable for loss of use of instrument or other incidental or consequential costs, expenses or damages incurred by the purchaser or any other user.
  • Page 48 “Analytical Support”, or email CEM MARS 6 iWave applications support at analytical.support@cem.com. Technical Support CEM is proud to provide technical support for the MARS 6 iWave from a team of specially trained Service Technicians. For technical support in the US and Canada, call (800) 726-5551 or (704) 821-7015 and ask for “MARS 6 iWave Service”...
  • Page 49 Address: Via Dell Artigianato, 6/8 24055 Cologno Al Serio (BG) Italy Web Address: http://www.cemmicroonde Email: info.srl@cem.com Japan: CEM Japan K.K. Phone: +81-3-5793-8542 Fax: +81-3-5793-8543 Address: 2-18-10 Takanawa Minato-Ku Tokyo 108-0074 Japan Web Address: http://www.cemjapan.co.jp Email: info@cemjapan.co.jp UK: CEM Microwave Technology Ltd. Phone: +44-1-280-822873 Fax: +44-1-280-822342 Contact Information...
  • Page 50 Email: info.ireland@cem.com CEM Authorized Dealers For a complete list of authorized dealers of CEM products, including contact information, go to the CEM website (http://www.cem.com), select Contact, and then select your region to see a list of authorized dealers by country.
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  • Page 52 Copyright 2019 by CEM Corporation CEM, iPrep, iWave and One Touch are Part Number 600832 All Rights Reserved. This guide contains registered trademarks of CEM Corporation. September 23, 2019 proprietary information which shall not be EasyPrep, EasyPrep Plus, MARS 6, Rev.

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