Performance Check: Intelligent Remote Module Type; Baseline (Abs 0 Line) Flatness - Jasco V-530 Hardware/Function Manual

Uv/vis spectrophotometer
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4.4

Performance Check: Intelligent Remote Module Type

A performance check should be
instrument performance. If the instrument is not operating properly, conduct checks
and take corrective action after referring to the troubleshooting chart in Section 5. After
taking corrective action, run the performance check again to verify that the instrument
has been restored to normal.
Note:
This section provides a simple description of operating procedures. For
details, refer to the Operations manual.
Baseline flatness
Wavelength repeatability
Wavelength accuracy

4.4.1 Baseline (Abs 0 line) Flatness

This check should be performed more than one hour after turning the instrument on.
(1) Select [Spectrum] from the main menu and measure the baseline of the entire
region after setting the following parameters. (Refer to Section 5-4 of the
Operations manual.)
This data is stored in the baseline memory.
Note:
This data is used for correcting the baseline spectrum (0 Abs line) to be
measured in (2) below.
(2) Set the following parameter and measure the baseline spectrum (0 Abs line) with
the sample chamber empty. (Refer to Section 5-3 of the Operations manual.) A
measurement example is shown in Fig 4.1.
V-530 measurement parameters
Phtmtrc mode
Response
Start WL
End WL
Data interval
Scan. speed
No. of Cycles
Lower scale
Upper scale
run
Response
Scanning speed
Abs
Medium
1000 nm
200 nm
1.0 nm
200 nm/min
1
-0.005 or more
+0.005 Abs
approx. once a month to ensure the
Refer to Section 4.4.1
Refer to Section 4.4.2
Refer to Section 4.4.3
Medium
100 nm/min
V-550/560/570
parameters
Phtmtrc mode
Response
Band width
Start WL
End WL
Data interval
Scan. speed
No. of Cycles1
Lower scale
Upper scale
24
normal
measurement
Abs
Medium
10 nm
850 nm
200 nm
1.0 nm
200 nm/min
-0.005 or more
+0.005 Abs

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