Knauer Azura Assistant ASM 2.1L User Manual
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Knauer Azura Assistant ASM 2.1L User Manual

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Assistant ASM 2.1L
User Manual
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Summary of Contents for Knauer Azura Assistant ASM 2.1L

  • Page 1 Assistant ASM 2.1L User Manual HPLC...
  • Page 2 For latest version of the manual, check our website: http://www.knauer.net/knowledge.html Copyright: This document contains confidential information and may not be repro- duced without written content of KNAUER Wissenschaftliche Geräte GmbH. © KNAUER Wissenschaftliche Geräte GmbH 2017 All rights reserved. AZURA® is a registered trademark of...

  • Page 3: Table Of Contents

    Table of Contents Table of contents Product information ............Device overview.
  • Page 4 Table of Contents Troubleshooting............LAN .

  • Page 5: Product Information

    Product information Product information Note: Only use the device for applications that fall within the range of the intended use. Otherwise, the protective and safety equipment of the device could fail. Assistant ASM 2.1L The Assistant ASM 2.1L is a compact combination module which is used in analytical, preparative and continuous liquid chromatography.

  • Page 6: Detector And Flow Cells

    UVD 2.1S will be delivered with a test cell. For the use of the detector, a flow cell has to be installed. For further information, take a look into the UVD 2.1S user manual V6820: http://www.knauer.net/fileadmin/user_u- pload/produkte/files/Dokumente/detectors/azura/manuals/V6820_A- ZURA_UVD_2.1S_User-Manual_EN.pdf Flow cells Flow cells are available with different path lengths, connections and also for different maximum flow rates.

  • Page 7: Valve Drives And Valve Heads

    Ceramic 10 ml Valve drives and valve heads Prior to delivery the valve drive can be equipped with KNAUER multiposi- tion valves and 2-position valves. Connections and channels of 2-position valves are described by abbreviations (example 6P/3C=2-position valve with 6 ports and 3 channels). In case of multiposition valves the central port does not count.

  • Page 8: Degasser

    Device overview KNAUER Valves Ports Connection Material Pressure stability 2-position valve 1/16", 1/8" Stainless steel 300 bar 2-position valve 1/16" Stainless steel 400 bar 2-position valve 6, 8 1/16" Stainless steel 1000 bar 2-position valve 1/16", 1/8” PEEK 150 bar Multiposition valve 1/16", 1/8"...

  • Page 9: Configuration Of Modules

    Device overview Fig. 4 ASM 2.1L gas outlet on the front Configuration of modules Maximum number of same modules Three modules can be integrated in an assistant. The number of same device types is limited:  1x Degasser  1x Detector UVD 2.1S ...

  • Page 10: Three Modules

    Injection module 1. Multi valve fraction collector Scope of delivery Note: Only use original parts and accessories made by KNAUER or a com- pany authorized by KNAUER. Delivery ASM 2.1L with devices User manual ASM 2.1L plus user manuals of integrated micro...

  • Page 11: Safety For Users

    Only use a given PEEK fitting for one specific port and never re-use it for other ports. Always install new PEEK fittings on each separate port.  Follow KNAUER or manufacturer’s instructions on caring for the colums. More safety-relevant information is listed below: ...

  • Page 12: Signal Words

    Decontamination Report Devices without a completed Decontamination Report will not be repaired. If you would like to return a device to KNAUER, make sure to enclose a completed Decontamination Report with the device: http:// www.knauer.net/en/knowledge/downloads/service.html...

  • Page 13: Unpacking And Setup

    Phone +49 30 809727-111 +49 30 8015010 E-mail support@knauer.net You can make your requests in English and German. Location requirements Only if the requirements for ambient conditions of the operating environ- ment are met, can the intended use be ensured. Details on the operating conditions can be found in the Technical Data section.

  • Page 14: Connectors On The Rear Side

    Unpacking and setup Prerequisite Check packaging for damage caused during transportation. If necessary, put forward any claim for damages to the carrier. Tools Utility knife Bruising danger Damage to the device by carrying or lifting it on protruding housing parts. The device may fall and thus cause injuries.
  • Page 15 Unpacking and setup Connection Function EV 3 (Event 3) Relay contact The contact is on a floating basis. Its setting depends on the settings in the software. Steady-rate signal:  passive = open relay contact  active = closed relay contact Pulse: ...

  • Page 16: Integrator Output

    Initial startup Connection Function +24 V Event-controlled switching of 24 V against GND Max. current: 200 mA Reference point of the voltage at the signal inputs Integrator output The integrator output sends measuring signals from the detector.  non-bipolar  1 channel ...

  • Page 17: Leak Management

    Initial startup Leak management The leak management consists of the leak sensor and the drainage system (funnels, hoses, nozzles). The drainage system ensures that escaping liq- uids flow into a waste bottle. When leaks are registered by the leak sen- sor, the LED flashes red.

  • Page 18: Connecting A Device To A Computer To A Local Area Network (Lan)

    Connecting a device to a computer to a Local Area Network (LAN) Note: HPLC devices made by KNAUER work only with IP adresses which are assigned via IPv4. IPv6 is not supported. This section describes how to set up an HPLC system in a local area net- work (LAN) and how a network administrator can integrate this LAN into your company network.

  • Page 19: Configuring The Router

    Initial startup You will find patch cables for each device and the router in the accessories kit. To connect the router to a WAN, an additional patch cable is required, which is not supplied within the scope of delivery.  Prerequisite The computer has been switched off.

  • Page 20: Operation

    To control the device with chromatography software, it must be con- ware nected to the computer through the LAN interface. The list of supported documents is public in the software section on the KNAUER website: http://www.knauer.net/fileadmin/user_upload/produkte/files/Dokumente/ software/supported_instruments.pdf You will find a detailed description on the chromatography software in the software manual.

  • Page 21: Meaning Of The Degasser Leds

    The LAN connections between the modules and router are connected.  The LAN cable is connected to the workstation and router.  The chromatography software has been installed by KNAUER or a com- pany authorized by KNAUER.  The capillaries in the solvent bottles have a filter insert.

  • Page 22: Functionality Tests

    Installation Qualification The customer may request the Installation Qualification, which is free of (IQ) charge. In case of a request, the Technical Support of KNAUER or from a provider authorized by KNAUER performs this functionality test during the installation. The Installation Qualification is a standardized document that comes as part of the delivery and includes the following: ...

  • Page 23: Lan

    Troubleshooting Go through the following steps, in case no connection between the com- puter and the devices can be established. Check after each step if the problem is solved. If the problem cannot be located, call the Technical Support. 1. Check the status of the LAN connection in the Windows task bar: ...
  • Page 24 Exchange the check valves.  When the pump head seals are defec- tive, solvent enters the piston backflush- ing. Inform the Technical Support of KNAUER.  Exchange the pump head.  Pressure and flow rate Pump without pressure sensor: Pay...

  • Page 25: System Messages

    Inform the Technical Support of KNAUER. System messages If other system messages are displayed besides those listed below, please turn the device off and then on. Inform the Technical Support of KNAUER in case the system message repeats itself. The system messages are sorted alphabetically.
  • Page 26 Leak sensor not present Switch the device off and then on. If the leak sensor is still not present, contact the Technical Support of KNAUER. Leak was detected Switch off the device. Remove the leak and start the device afterwards.

  • Page 27: Maintenance And Care

    (see “Device overview” on page 5). Maintenance contract The following maintenance work on the device may only be performed by KNAUER or a company authorized by KNAUER and is covered by a sepa- rate maintenance contract:  Opening the device.

  • Page 28: Technical Data

    Note: For repeat orders of spare parts use the enclosed packing list. Con- tact the Technical Support in case there are any questions on spare parts or accessories. Further Information Further information on spare parts and accessories can be found online: www.knauer.net ASM 2.1L user manual V6815...
  • Page 29 A9853-3 columns with 20 mm ID Mounting bracket AZURA® L for Hypershear mixing A9853-8 chamber Mouting bracket AZURA® L for KNAUER flow cells A9853-5 Mouting bracket AZURA® L for KNAUER injection A9853 valves Mouting bracket AZURA® L for manual KNAUER multi-...

  • Page 30: Legal Information

    2001), old devices manufactured by KNAUER are marked as waste electri- cal and electronic equipment: 160214. WEEE Registration KNAUER as a company is registered by the WEEE number DE 34642789 in the German "Elektroaltgeräteregister" (EAR). The number belongs to category 8 and 9, which, among others, comprise laboratory equipment.

  • Page 31: Abbreviations And Terminology

    Abbreviations and terminology All wetted components of a device, e. g. flow cells of detectors or pump heads and pressure sensors for pumps, have to be flushed first with iso- propanol and then with water before being maintained, disassembled or disposed.
  • Page 32 Abbreviations and terminology Term Explanations Solvents Mobile phase (eluent) or carrier for liquid chromato- graphy ASM 2.1L user manual V6815...

  • Page 33: Index

    Index Index P 2.1S/P 4.1S UVD 2.1S abbreviations V 2.1S accessories Mobile Control ambient conditions mounting bracket analog port AVV marking operating environment care Compact HPLC setup packing list connectors PEEK contamination port (LAN) power disconnect decontamination plug disposal power cable power strip eluents power supply...
  • Page 34 Index valve warranty ASM 2.1L user manual V6815...
  • Page 35 KNAUER manuals online: www.knauer.net/knowledge Phone: KNAUER +49 30 809727-0 Fax: Wissenschaftliche Geräte GmbH +49 30 8015010 E-Mail: Hegauer Weg 38 info@knauer.net Internet: 14163 Berlin www.knauer.net © KNAUER 2017...

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