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Summary of Contents for MRC ROVAP Series
- Page 1 High Throughput Vacuum Parallel Evaporator Instruction Manual This user manual needs to be read before operating this product Please follow the safety instructions provided in this manual Hagavish st. Israel 58817 Tel: 972 3 5595252, Fax: 972 3 5594529 mrc@mrclab.com MRC. 8.22...
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Page 2: Table Of Contents
Content ..........................2 ..........................3 ........................ 3 DANGER: For damage and danger caused by improper use is the sole responsibility of the user........................3 ......................3 ..........................4 2.3.1 Dangerous vapor........................4 2.3.2 High internal pressure......................5 2.3.3 Hot surfaces and liquid......................5 2.3.4 broken glass.......................... - Page 3 ........................20 .........................21 ........................21 ....................22 ....................22 ........................ 22 ......................23 ........................ 23 ..........................24 9.2.1 Method display interface....................26 9.2.1.1 Method setting interface....................27 9.2.2 Solvent Reference Interface....................28 9.2.3 Setting interface........................29 9.2.3.1 Basic setting interface..................... 30 9.2.3.2 Function setting interface....................30 9.2.3.3 User management interface..................31 9.2.3.4 Operation record interface....................32 9.2.3.5 Equipment information interface .................
- Page 4 Dear users, thank you for choosing MRC High Throughput Vacuum Parallel Evaporator. This equipment is mainly used in the field of organic analysis and testing,which rapidly concentrates the sample under reduced pressure. MRC RovaP High Throughput Vacuum Parallel Evaporator was developed and manufactured in accordance with the most advanced level of scientific and technological knowledge.
- Page 5 Please keep this instruction manual near the equipment Please pass this instruction manual to the next owner or user MRC Co., Ltd. will not assume any damage or malfunction caused by failure to comply with this operation manual please contact customer service department of MRC Co., Ltd if you have any questions after reading this instruction manual.
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Page 6: Danger: For Damage And Danger Caused By Improper Use Is The Sole Responsibility Of The User
Beware of broken glass causing injury! Beware of harmful gas poisoning! The RovaP series vacuum parallel evaporator is not allowed to be used as the following conditions ◆ Under an environment with explosion danger and explosion- proof equipment;... -
Page 7: Dangerous Vapor
2.3.1 Dangerous vapor Hazardous vapors may be generated during use of the equipment, which can lead to poisoning and life-threatening conditions. The RovaP series vacuum parallel evaporator must be equipped with a steam condensing unit; ◆ Do not inhale the vapor generated during use;... -
Page 8: High Internal Pressure
the equipment can only be used in a well-ventilated environment for that ◆ If steam escapes from the connection, check the corresponding seal and replace if necessary. 2.3.2 High internal pressure High internal pressure may be created in the vial or in the condenser through the evaporation of the liquid. -
Page 9: Retrofit
Technical changes to equipment or accessories can only be made with the prior written approval of Beijing MRC Co., Ltd. and only by authorized MRC Co., Ltd. technicians Notes : MRC Co., Ltd. will not be liable for damage caused by unauthorized equipment changes RovaP-4... -
Page 10: Storage And Transportation Environmental Requirements
Max. application altitude ≤2000 m Ambient conditions Indoor Ambient temperature 5℃-35℃ 80 % (when temperature less than 31 °C) Max.relative air humidity 40 °C ，Linearly down to 50 % Storage and transportation environmental requirements Ambient temperature -25℃-55℃ Max.relative air humidity 90 % @25℃... - Page 11 Sample heated by controlling water bath temperature to accelerate concentration of sample; Vacuum control Accelerates sample concentration by controlling the vacuum inside sample bottle. Meanwhile the equipment has function of vacuum gradient control, so that vacuum degree can gradually approaches target value, preventing the vacuum degree from rising too fast , resulting in the sample to boil Vacuum lock function If sample heating temperature is known, but vacuum parameters are unknown,...
- Page 12 4.2.1 Axonometric projection Fig.1 Axonometric projection 1 Vacuum adjustment knob; 2 LCD touch screen; 3 Water bath; 4 Sample bottle adapter; 5 Sample bottle; 6 on-off button 7 cover plate; 8 cover plate handle; 9 attracting magnet; 10 vacuum pump power socket; 11 heating reset button;...
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Page 13: Rear View
4.2.2 Rear view Fig.2 Rear view 1 Vacuum pump inlet port; 2 Condensing device gas input port; 3 USB memory interface; 4 Air inlet; 5 water flood pump... -
Page 14: Water Supply And Drainage Connection Diagram
4.2.3 Water supply and drainage connection diagram Fig.3 Water supply and drainage connection diagram 4.2.4 External electrical connection of equipment diagram Fig.4 External electrical connection of equipment diagram 1 Water bath heating control line; 2 Circulating water pump control line; 3 cover plate heating control line;... -
Page 15: Water Shortage Detection Component
4.2.5 Nameplate information AH.VPXX-XXXX-XXXX Fig.5 Nameplate information 4.3.1 Water shortage detection component Built-in water flow sensor. If water bath is short of water, the equipment will stop heating, and a water shortage alarm message will appear on touch screen; 4.3.2 Heater overheat protection component Built-in overheat protector. -
Page 16: Over-Current Protection Component
4.3.3 Over-current Protection component RovaP series vacuum parallel evaporator rear side with power fuse, specifications are: diameter of 5mm, length 20mm, fusing current≥15A Fig.7 Fuse position diagram ◆ Make sure that equipment is disassembled and that all parts of equipment have been packaged to prevent breakage, if possible, packed in original cardboard box. - Page 17 The load-bearing capacity of countertop should be ≥500Kg, otherwise vibrate violently during operation will damage to equipment. There have two models A and B of condensing system for RovaP series vacuum, installing which modes according to the specific configuration of equipment...
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Page 18: Installation Model A Condensing System
Fig.9 Model B condensing system diagram 6.2.1 Installation model A condensing system A solvent recovery instrument is selected to realize condensation recovery of solvent vapor. Solvent recovery instrument RovaP unit vacuum pump silencer bottle Fig.10 Model A Pneumatic Connection Diagram Pipeline connection RovaP unit, solvent recovery instrument, vacuum pump, and silencer bottle as shown in figure 10. -
Page 19: Installation Model B Condensing System
6.2.2 Installation model B condensing system A cooling circulator and a glass condenser are selected to realize the condensation recovery of solvent steam. Fig.11 Model B Pneumatic Connection Diagram 6.2.2.1 Installation of glass condenser ◆ glass condenser fixed Fig.12 Model B glass condenser installation diagram Install glass condenser assembly on the bottom bracket on the right side of the RovaP unit as above shown, and fasten all the screws... -
Page 20: Installation Of Cooling Circulator Pipeline
◆ Collection bottle fixed Fig. 13 Collection bottle installation diagram Install collection bottle on the glass condenser as above shown, and fix it with bottle clamps and collection bottle bases; 6.2.2.2 Installation of cooling circulator pipeline cooling liquid outlet cooling Liquid inlet Fig. -
Page 21: Installation Of Vacuum Pump Pipeline
6.2.2.3 installation of vacuum pump pipeline 冷却液入口 Fig. 15 Installation of vacuum pump air circuit diagram Pipeline connection between RovaP unit, glass condenser, vacuum pump, and silencer bottle as . fig.15 shown, the pipeline I.D : 8mm, Material: PTFE Note: Please be sure to connect as fig. 15 shown , and check carefully, if the connection is wrong, it will cause serious damage to the equipment! AC220V 16A Vacuum pump power socket... - Page 22 ◆ turn on power and start the host; ◆ Enter the setting menu, long press to fill the water bath; ◆ Stop fill water to water bath when water level reaches between H and L lines. Note: Pure water must be added to prevent limescale from clogging the circulation channel and causing damage to the equipment! 按照图示样品瓶插入样品瓶适配器内。...
- Page 23 After completing the equipment installation according to 6.1-6.5, check equipment performance in the following steps before use. ◆ Place in an empty sample bottle; ◆ Make the upper cover in the closed state; ◆ Turn on power supply of the host, vacuum pump and condensing system; ◆...
- Page 24 Note: After start button is activated, the handle of upper cover must be pressed down quickly to ensure that electromagnets at the left and right ends of the upper cover are in the suction state, otherwise the system vacuum will be abnormal. After equipment runs, the real-time temperature, vacuum degree and oscillation speed on the main interface will gradually approach the target value.
- Page 25 ◆ Turn on the power of cooling circulator or solvent recovery instrument, and start condensation system; ◆ Make sure that the condensate collection bottle is installed; Note: The condensing system should be turned on 10 minutes in advance, and temperature of condensing system should be more than 35℃ lower than the water bath temperature during operation, so that the solvent vapor can be well condensed and collected;...
- Page 26 ◆ When sample volume is close to target state, press ,then sample will stop Concentrating. ◆ When vacuum degree is close to atmospheric pressure, the electromagnet of the upper cover will be automatically released, and then open which and take out sample. Note: After the concentration work is over, please clean up the liquid in the collection bottle of the condensation system in time, otherwise the equipment will malfunction;...
- Page 27 ◆ 【Method】 Establishment ,preservation and loading of sample concentration methods ◆ 【Save】 The currently set parameters such as temperature, time, vacuum, and oscillation speed can be saved to method; ◆【Setting】 Language and vacuum degree can be chosen; Preheat mode can be turned on or off; User management is possible;...
- Page 28 automatically bounce. Click button again to restart vacuum pump, meanwhile, you need to press down cover plate to keep it in suction state, and then continue to concentrate sample; ◆【Suspend】 After clicking the button, the countdown pauses, sample stops oscillating, vacuum pump stops working, equipment will release vacuum, cover plate will automatically pop up, click button again, equipment will work again, time countdown continues, at this time, you need to press down cover...
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Page 29: Method Display Interface
9.2.1 Method display interface ◆ 【Storage area code】 there have 100 storage area codes, which can create and store 100 methods. When editing, loading and deleting methods, you need to select the corresponding storage area number first; ◆ 【New-built 】 The new method can be created, and system will automatically select vacant storage area code to edit and create the method ◆... -
Page 30: Method Setting Interface
9.2.1.1 Method setting interface ◆ 【Name】 Please enter the method name to be created; ◆ 【Creator】 Automatically created according to the user's name; ◆ 【Temp.】 According to requirements of analysis method, set heating temperature of water bath, temperature setting range: room temperature +5 °C to 85 °C; ◆... -
Page 31: Solvent Reference Interface
vacuum control is not required, only need input vacuum degree and duration time of the first stage, the minimum input value of the duration is 1min; Note: The data in stage1 must be input, otherwise equipment will not work properly; ◆... -
Page 32: Setting Interface
selected, vacuum parameters corresponding to solvent will be automatically exported to the working interface, and temperature will default to 40°C, shaking speed will default to 150rpm, and time will default to 100min. Note: The recommended parameters are for reference only and should be changed according to the actual situation to avoid experiment failure;... -
Page 33: Basic Setting Interface
◆ 【water pump 】 filling water into water bath ◆ 【Return】 Return to working interface. 9.2.3.1 Basic setting interface Select or cancel language and vacuum degree, and return to the previous interface after saving. 9.2.3.2 Function setting interface Select or cancel sample preheating function, and return to the previous interface after saving;... -
Page 34: User Management Interface
When sample preheating is selected and equipment starts to run,but vacuum pump will be restarted after a delay of 2 minutes, which can make sample preheat first then concentrate , avoiding sample explosive boiling due to unevenness heating; 9.2.3.3 User management interface User management is only for administrator . -
Page 35: Operation Record Interface
Change the selected user name and password, save and return to the previous interface; Note: After changing administrator password, be sure to save password properly, otherwise equipment cannot be used normally. If the administrator password is lost, please call service number of MRC Co., Ltd. ; 9.2.3.4 Operation record interface... -
Page 36: Equipment Information Interface
The key data during operation is recorded in operation record. Each time start button is clicked to run equipment, the system will record start time of operation, vacuum degree used, temperature of the water bath, oscillation speed, operation time, operator information, operation time and the fault code generated in the process which can trace experimental data;... -
Page 37: Cover Plate Temperature Setting Interface
9.2.3.6 Cover plate temperature setting interface RovaP series products supports cover plate heating, which can heat and evaporate solvent vapor entering cover chamber to prevent the solvent vapor from condensing in the upper cover chamber Equipment has the function of self-adapting the heating temperature of cover plate, and automatically adjusts heating temperature of cover to target value of current water bath temperature. -
Page 38: Software Alarm Information Description
Software alarm information description Problem Possible cause Solution Liquid level in water bath is too F ill water into the bath and keep the water line between H-L; First turn off main unit power , then turn There is residual gas in water bath circulation pipeline, which on the power again, enter the system and Water bath level is low... -
Page 39: Cleaning And Maintance
Compnent Substance Solution frequency before each trial Collection bottle Clean condensate in Remove collection bottle fixation and cleaning collection bottle collection bottle, and pour liquid in collection bottle into a dedicated waste liquid collection container; before each trial silencer bottle Clean condensate in Unscrew cap of silencer bottle and cleaning... -
Page 40: Other Instructions
Use supplied special tool to remove lock nut, remove compression washer and gasket, and replace the seal. When replacing a new bottle seal, the smooth surface of the seal covered with Teflon film must be installed towards the bottle mouth. 1 lock nut;... -
Page 41: Optional Items
RovaP series parallel evaporator can realize use of different volumes of sample bottles by replacing the upper cover plate and sample adapter. ◆ Replace cover plate Turn off power of equipment, making cover plate in a closed state, remove countersunk head screws on the left and right sides of cover plate, pull out the pins, take off cover plate and replace it. - Page 42 Profile Nmae Order No. Specifications 4-position sample RovaP-4-850 For 4-position, 850ml sample bottles; adapter 9-position sample RovaP-9-450 For 9-position, 450ml sample bottles; adapter 16-position sample RovaP-16-250 For 16-position, 250ml sample bottles; adapter 36-position sample RovaP-36-060 For 36-position,60ml sample bottles; adapter Ball mouth solvent P35QK2000H Ball Regular Mouth，volume 2000ml；...
- Page 43 Profile Nmae Order No. Specifications RovaP-4-HC-01 For cover plate APE4-850 sample adapter RovaP-9-HC-01 For cover plate APE9-450 sample adapter bottle seal RovaP-16-HC-01 For cover plate APE16-250 sample adapter RovaP-36-HC-01 For cover plate APE36-060 sample adapter F850-4PMMA For 4 pcs 850ml sample bottles F450-9PMMA For 4 pcs 450ml sample bottles sample bottle...
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