Thermo Scientific Nanopure Analytical 1367 Series Operating Manual And Parts List
Ultrapure water system
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Summary of Contents for Thermo Scientific Nanopure Analytical 1367 Series
- Page 1 Nanopure™ Analytical Ultrapure Water System Series 1367 Operating Manual and Parts List LT1367X1 Rev. 0 _________________________________________________________________________________ Part of Thermo Fisher Scientific...
- Page 2 Preface Models covered in this manual Model number Voltage D11901 (7143) 100V - 240V MANUAL NUMBER LT1367X1 (7007143) 6/9/10 Transfer to Marietta (was LT1367X1 3/4/10) ECR/ECN DATE DESCRIPTION Thermo Scientific Nanopure™ Analytical...
- Page 3 Thermo Fisher Scientific makes no representations or warranties with respect to this manual. In no event shall Thermo be held liable for any damages, direct or incidental, arising out of or related to the use of this manual. ©2010 Thermo Fisher Scientific. All rights reserved. Nanopure™ Analytical Thermo Scientific...
- Page 4 Always use the proper protective equipment (clothing, gloves, goggles, etc.) 4 Always dissipate extreme cold or heat and wear protective clothing. 4 Always follow good hygiene practices. 4 Each individual is responsible for his or her own safety. Thermo Scientific Nanopure™ Analytical...
- Page 5 We can also provide you with a quotation on our Extended Warranty for your Thermo Scientific products. Whatever Thermo Scientific products you need or use, we will be happy to discuss your applications. If you are experiencing technical problems, working together, we will help you locate the problem and, chances are, correct it yourself...over the telephone without a service...
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Page 6: Table Of Contents
Dispensing Water ........8-2 Thermo Scientific... - Page 7 Wiring Diagram ........14-5 Nanopure™ Analytical Thermo Scientific...
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Page 8: Safety Information
Water purification technology employs one or more of the following: chemicals, electrical devices, mercury vapor lamps, steam and heated vessels. Care should be taken when installing, operating or servicing Thermo Scientific products. The specific safety notes pertinent to this product are listed below. Warnings To avoid electrical shock, always: 1. - Page 9 6. Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets. 7. Depressurize system prior to removing the cartridge pack. 8. Refer servicing to qualified personnel. 9. A full cartridge pack may weigh about 20 lbs. Nanopure™ Analytical Thermo Scientific...
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Page 10: Introduction
Introduction Section 2 Congratulations on your purchase of a Thermo Scientific Nanopure Analytical ultrapure water system. This water purification system is designed to provide high resistivity, reagent grade water that exceeds ASTM Type I, ISO 3696 and CLSI-CLRW Type I standards. It uses a four-stage deionization process combined with a 0.2 micron filter to polish... -
Page 12: General Specifications
Accuracy: ......± 5% Repeatability: ......± 3% Thermo Scientific Nanopure™ Analytical... - Page 13 Measurement, Control and Laboratory Use; Part I: General Requirements per the provisions of the Electromagnetic Compatibility Directive 2004/108/EC, and per the provisions of the Low Voltage Directive 2006/95/EC. Copies of the Declaration of Conformity are available upon request. Nanopure™ Analytical Thermo Scientific...
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Page 14: Unpacking
Plug Adapter ..... . .CEX42 Power Cords Also required for installation: * Customer Supplied Fasteners to mount unit and remote display. Thermo Scientific Nanopure™ Analytical... -
Page 16: Installation
Routine maintenance of this unit may involve water spillage and subsequent electrical shock hazard if improperly located. Warning Do not use in the presence of flammable materials; fire or explosion may result. This device contains components which may ignite such materials. Thermo Scientific Nanopure™ Analytical... -
Page 17: Wall Mounting
7. Push the locking slides on each side of the wall bracket in as far as they will go. 8. Replace the locking screws. Note Please refer to the “General Specifications” section for clearance requirements. Nanopure™ Analytical Thermo Scientific... -
Page 18: Install Control Panel In A Remote Location
3. Replace the control panel with the blank panel provided with the unit to protect the electrical connector. Note The blank protective cover on the rear side panel display connector should remain in place when the display is not remotely located. Thermo Scientific Nanopure™ Analytical... - Page 19 Note A bracket is available that will allow you to mount the control panel on the bench. If bench mounting is desired, order bracket AY1367X2. Blank panel Wall Mount Bracket Figure 5-1. Control Panel Wall Mounting Nanopure™ Analytical Thermo Scientific...
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Page 20: Water Connections
Accudispense control cable Remote 1 Remote 2 Feed Water Inlet Atmospheric Drain Figure 5-2. Water Connections - Left Side of Unit Overflow Float Connection Figure 5-3. Water Connections - Right Side of Unit Thermo Scientific Nanopure™ Analytical... -
Page 21: Atmospheric Drain Connection
3. Wet the tube end with water and insert tube straight into fitting until it bottoms out on interior shoulder and insertion mark is no longer visible. 4. To remove tubing, push collet toward fitting body and pull on tubing. To reuse fitting, begin assembly at Step 1. Nanopure™ Analytical Thermo Scientific... -
Page 22: Electrical Connections
The Nanopure is not shipped with fuses installed in the fuse draw of the power module. Before connecting the power cord to the power module, install the proper fuses in the fuse holder. Refer to Figure 5-6. Fuse Holder Power Switch Power Cord Figure 5-6. Electrical Connections Thermo Scientific Nanopure™ Analytical... -
Page 24: Controls
LED is not illuminated: System is OFF or in (Idle) mode. • Solid Green LED: System is recirculating and operating normally. • Blinking Green LED: System is in Standby mode. • Red LED: System is alerting user to an operational error or maintenance issue. Thermo Scientific Nanopure™ Analytical... -
Page 25: Switches
Push to the left to deliver water manually until button is released. Note The unit MUST be in the normal recirculating mode (when the display is showing purity) in order to dispense water. Nanopure™ Analytical Thermo Scientific... -
Page 26: Initial Operation
3. Lift unit manifold upwards, insert cartridge pack and align the pack so that it mates with the unit manifold. 4. Lower unit manifold until it is flush with the top of the cartridge pack. Figure 7-1. Cartridge Pack Installation Thermo Scientific Nanopure™ Analytical... -
Page 27: Initial Rinse
Self Test. Passed.” Finally, the display will read “10 (±0.2) MΩ-cm.” This is a reading of the calibration reference value. 9. From the (Idle) mode, when the display reads, “Nanopure (Idle) xx:xx:xx xx/xx/xx,” press ENTER to run an air purge. Nanopure™ Analytical Thermo Scientific... -
Page 28: System Cleaning Procedure
7. Remove luer cap on system injection port, located on the right side of the cartridge pack manifold by turning counterclockwise. 8. Remove syringe luer cap and attach syringe to the system luer fitting. Figure 7-2. Injecting Cleaning Solution Thermo Scientific Nanopure™ Analytical... - Page 29 16. Press the START/STOP switch to return the unit to the normal recirculation mode. 17. Remove the new 0.2 micron filter and bell assembly (Figure 7-3) from the bag and insert it into the dispenser arm manifold. Gently turn it clockwise until it is fully seated. Nanopure™ Analytical Thermo Scientific...
- Page 30 15-20 liters through the cartridges and 0.2 micron filter may be necessary. Caution Never dispense water without first installing hose barb provided in parts bag or final filter supplied with cartridge pack. 0.2 Micron Filter Figure 7-3. Installing 0.2 Micron Filter Thermo Scientific Nanopure™ Analytical...
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Page 32: Normal Operation
Standby Mode. Note From the normal recirculating mode when the display is showing purity, press ENTER to show the current temperature. The temperature will display for about 5 seconds before returning to the normal recirculating mode. Thermo Scientific Nanopure™ Analytical... -
Page 33: Automatic Dispensing
Note Press any switch except ENTER to stop dispensing. Display will read, “Auto Dispense Interrupted by User.” Note If the Nanopure “Auto Dispense” feature is set to (TIME), a connected Accudispense accessory (if applicable) will not automatically dispense. Nanopure™ Analytical Thermo Scientific... -
Page 34: User Settings
BACK switch until the display reads “LANGUAGE.” 2. The currently selected language is displayed on line 2 of the display. 3. Press the UP or DOWN arrow to select the language desired. 4. Press ENTER. Thermo Scientific Nanopure™ Analytical... -
Page 35: Setting The Date And Time
11. Press the UP or DOWN arrow until you reach the desired minute value. Press ENTER. 12. Press BACK twice to return to the (Idle) mode. Note Time values are displayed in 24 hr. military time. For example; 6:00p.m. = 18:00:00 = hr./min./sec.) Nanopure™ Analytical Thermo Scientific... -
Page 36: Setting The Call Constant
14. If the cell constants displayed on line 1 of the display are correct, press the UP or DOWN arrow to select “Yes.” 15. Press ENTER. 16. Press BACK twice to return to the (Idle) mode. Thermo Scientific Nanopure™ Analytical... -
Page 37: Selecting The Set Point
3. Proceed through the options by pressing ENTER until “Adjust Set Point” is displayed. 4. Press the UP or DOWN arrow to choose “Yes.” 5. Press ENTER. 6. Press the UP or DOWN arrow until the desired value is displayed. 7. Press ENTER. Nanopure™ Analytical Thermo Scientific... -
Page 38: Setting Volumetric Dispensing
3. Display will read, “Dispense Method.” Press the UP or DOWN arrow to select VOLUMETRIC. 4. Press ENTER. Display will read, “Unit Volume Setting: xx Liters.” 5. Press the UP or DOWN arrow to set the desired volume value. Press ENTER. Thermo Scientific Nanopure™ Analytical... -
Page 39: Setting Timed Dispensing
2. Press the UP or DOWN arrow to select “Short Flush?” or “Extended Flush?” Press ENTER. 3. Display will read, “System Flushing: (xxx) Seconds or (xxx) Minutes Remaining.” Note Press the STOP/STOP switch to cancel the flush. Nanopure™ Analytical Thermo Scientific... -
Page 40: Auto Standby
Standby during weekends. 1. From the “Nanopure (Idle) xx:xx:xx xx/xx/xx” press the UP or DOWN arrow until display reads, “Advanced Menu.” 2. Press ENTER. 3. Press ENTER to proceed through the options until “AUTO STANDBY START” is displayed. Thermo Scientific Nanopure™ Analytical... -
Page 41: Unit Under Counter
3. Press ENTER to proceed through the options until “UNIT UNDER COUNTER” is displayed. 4. Press the UP or DOWN arrow to choose “YES.” 5. Press ENTER. 6. Press BACK until you return to the (Idle) display. Nanopure™ Analytical Thermo Scientific... -
Page 42: Accessories
Nanopure Analytical into the remaining opening of the PVC tee. 4. Route the cable from the float or low pressure switch to the top left of the Nanopure Analytical. Thermo Scientific Nanopure™ Analytical 10-1... -
Page 43: Dispense Overflow Cutoff Float
Figure 10-2. Dispense Overflow Cutoff Float 2. Position carboy to be filled and place float assembly on open neck of carboy. Position float assembly such that it will not interfere with product water stream being dispensed into carboy. 10-2 Nanopure™ Analytical Thermo Scientific... -
Page 44: Electronic Calibration W/ Optional Cal. Mod
7. From the (Idle) mode, Press the UP or DOWN arrow until the display reads, “N.I.S.T. Calibrate?” Press ENTER. 8. Display will show “Calibration Module Installed?” Press the UP or DOWN arrow to select (YES). 9. Press ENTER. Thermo Scientific Nanopure™ Analytical 10-3... -
Page 45: Remote Volumetric Dispenser
14. Reattach the cover plate and close and latch the door. 15. Reconnect the power cord. The calibration procedure is complete. Remote Volumetric Refer to the Operating Instructions for your manual or Accudispense Dispenser volumetric remote dispenser (LT1366X11). 10-4 Nanopure™ Analytical Thermo Scientific... -
Page 46: Computer/Printer Set-Up
10. To receive data to a file, select Transfer and capture text. Accepting default will put the file which you name in the c:/windows directory called capture.txt and the file will be an ASCII text file. 11. You should see the data on the computer screen. Thermo Scientific Nanopure™ Analytical 11-1... -
Page 47: Procomm
12. Type in 21 <Enter>, sets to COM2: or (Type in 20 <Enter>, sets to COM1:), depending on your computer. 13. Type in 24 <Enter>, saves settings. 14. Type ESC to exit setup menu. 15. Procomm is now ready to accept input from the Nanopure. 11-2 Nanopure™ Analytical Thermo Scientific... -
Page 48: Connecting And Starting The Printer
Located on the front of the printer (AY1137X1), this switch turns power to the printer ON and OFF. The POWER light will illuminate when the printer is ON. For additional setup and operation, refer to the instruction manual included with the printer. Thermo Scientific Nanopure™ Analytical 11-3... -
Page 50: Maintenance And Servicing
6. Thoroughly rinse the cell in deionized or distilled water following the detergent or acid cleaning. 7. After cleaning, check the o-ring; replace if necessary. 8. Reinstall the cell into the cell well and hand-tighten. 9. Reroute the cable and reconnect to J2 on circuit board. Thermo Scientific Nanopure™ Analytical 12-1... -
Page 51: System Cleaning
Manual mode.) From the (Idle) mode, press the UP or DOWN arrow until the display reads, “Clean Unit?” 2. Press ENTER. 3. Display will prompt, “Disconnected Inlet Water (NO).” 4. Disconnect feed water supply at the quick-disconnect inlet valve. 12-2 Nanopure™ Analytical Thermo Scientific... - Page 52 Complete: Press ENTER.” 15. After cleaning is complete and the user presses “ENTER”, the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculating mode. Thermo Scientific Nanopure™ Analytical 12-3...
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Page 53: Cartridge Pack Replacement
The simple-to-use cleaning syringe is available (Catalog Number CMX25). This is used to effect a complete cleaning. Warning Depressurize system prior to removing cartridge pack. Warning A full cartridge pack may weigh about 20 lbs. (9 kg). Figure 12-1. Cartridge Pack Replacement 12-4 Nanopure™ Analytical Thermo Scientific... -
Page 54: Micron Filter Replacement
Note If a newly installed 0.2 micron filter clogs rapidly after installation, the Nanopure Analytical may need to be cleaned to remove bacterial contaminants. See “System Cleaning.” 0.2 Micron Filter Figure 12-2. Replacing 0.2 Micron Final Filter Thermo Scientific Nanopure™ Analytical 12-5... -
Page 55: Shutdown
If the system has remained inactive and full of water for more than 96 hours, the unit should be drained, cleaned and new cartridge pack installed prior to use. 12-6 Nanopure™ Analytical Thermo Scientific... -
Page 56: Troubleshooting
Check the expiration date. Cartridge packs begin to lose capacity after Cartridge pack is beyond expiration Short cartridge pack life. being stored for 2 years from the date of manufacture. Replace the date. cartridge pack with an unexpired one. Thermo Scientific Nanopure™ Analytical 13-1... - Page 57 Reinstall cartridge pack as 4 posts must contain an o- indicated in “Cartridge Pack Replacement.” ring.) Water is leaking at atmos- Tubing not fully inserted. Insert tubing into connection until it bottoms out. pheric drain connection 13-2 Nanopure™ Analytical Thermo Scientific...
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Page 58: Replacement Parts
Main Fuse, 120 Volt - Slow Blow, 1.6 Amp, 250V FZX47 Main Fuse, 230 Volt - Type T Time Lag, 0.63 Amp, 250V FZX54 PTFE Tape, Roll 06078 Transformer Fuse, Type F Fast-Acting, 3.15 Amp, 250V AZ9027 Cleaning Solution CMX25 Thermo Scientific Nanopure™ Analytical 14-1... - Page 59 Power Supply PC Board TNX116 Calibration PC Board PC1190X2 Resistivity Meter PC Board PC896X2 Check Valve PMX214 Flow Sensor ME1190X1 Flush Solenoid RY1190X3 Cartridge Pack Manifold BK1190X3 Dispenser Manifold W/Solenoid BK1367X1 Dispense Switch SW1190X1 Cell O-ring GSX29 14-2 Nanopure™ Analytical Thermo Scientific...
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Page 60: Ordering Procedures
All parts listed herein may be ordered from the Thermo Scientific dealer from whom you purchased this unit or can be obtained promptly from the factory. -
Page 61: Flow Chart
Compensation? Remote Gun System flush? Date Format Auto Dispense Set Date Menu? Set Time Arrow Legend: Set Cell Constant Keypress Options Set Display Brightness Automatic Entry Adjust Set Menu Wrap-around Point Diagnostics menu? Operational Overview 14-4 Nanopure™ Analytical Thermo Scientific... -
Page 62: Wiring Diagram
Section 14 Replacement Parts Wiring Diagram Thermo Scientific Nanopure™ Analytical 14-5... - Page 64 Thermo Scientific 401 Millcreek Road Marietta, Ohio 45750 United States www.thermofisher.com...
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