Related Manuals for Thermo Scientific Barnstead NANOpure DIamond D11901
Summary of Contents for Thermo Scientific Barnstead NANOpure DIamond D11901
- Page 1 Barnstead NANOpure DIamond ® ™ Analytical ultrapure water system Operation Manual Series 1367 Model No. Voltage D11901 100V - 240V LT1367X1 • 2/19/07...
-
Page 2: Table Of Contents
Table of Contents Safety Information ......................................3 Alert Signals ......................................3 Warnings........................................3 Introduction ........................................5 General Usage ......................................5 General Specifications ....................................6 Environmental Conditions..................................7 Declaration of Conformity ..................................7 Unpacking ........................................8 Installation ........................................9 Choosing a Site ....................................9 Other Accessories ....................................10 Bench Mounting ....................................10 Wall Mounting ......................................10 Installing the Control Panel in a Remote Location ..........................11 Water Connections ....................................12 Tubing Installation ....................................13... -
Page 3: Safety Information
Care should be taken Note when installing, operating or servicing Thermo Scientific Notes alert you to pertinent facts and products. The specific safety notes pertinent to this conditions. - Page 4 AFETY NFORMATION Avoid splashing cleaning solutions on clothing or skin. Ensure all piping connections are tight to avoid chemical leakage. Ensure adequate ventilation. Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets. Depressurize system prior to removing the cartridge pack.
-
Page 5: Introduction
Introduction Congratulations on your purchase of a Thermo Scientific Barnstead NANOpure DIamond Analytical ultrapure water system. This water purification system is designed to pro- vide high resistivity, reagent grade water that exceeds ASTM Type I, CAP and NCCLS Type I standards. It uses a four-stage deionization process combined with a 0.2... -
Page 6: General Specifications
General Specifications Dimensions and Clearance Requirements Dimensions 13.5” W x 19.5” H x 17.0” D (34.3 x 49.5 x 43.2 cm) Clearances Sides - 9” (22.9 cm) minimum for servicing. Above - 3” (7.6 cm) minimum for removal of the top cover. Front - 4.75”... -
Page 7: Environmental Conditions
ENERAL PECIFICATIONS Environmental Conditions Operating: 4°C - 40°C; 20% to 80% relative humidity, non-condensing. Installation Category II (over-voltage) in accordance with IEC 664. Pollution Degree 2 in accordance with IEC 664. Altitude limit: 3,500 meters. Storage: -25°C to 65°C; 10% to 85% relative humidity. Declaration of Conformity We hereby declare under our sole responsibility that this product conforms with the technical require-... -
Page 8: Unpacking
Unpacking Remove the unit from its shipping container. Remove all contents carefully. Ensure that the feed and drain tubing, cleaning cartridge, wall bracket, accessory parts bag and power cords (see list below) are removed from the packaging materials before discarding. Put the NANOpure DIamond Analytical on a bench. -
Page 9: Installation
Installation Choosing a Site Caution The NANOpure DIamond Analytical features a removable Wall composition, condition and control panel display which allows the system to be construction as well as fastener type mounted almost anywhere within the laboratory. Use the must be considered when mounting wall bracket for wall mounted systems as a template to this unit. -
Page 10: Other Accessories
NSTALLATION Other Accessories Optional accessories for this unit include a float switch, low pressure switch, N.I.S.T. Traceable Calibration Module, standard remote dispenser, Accu DIspense volu- metric remote dispenser, dispense overflow cutoff float and printer. If you purchased a float switch or low pres- Caution sure switch, refer to page 30 of this manual. -
Page 11: Installing The Control Panel In A Remote Location
NSTALLATION Note The removable control panel was not designed to be repeatedly removed from the unit, therefore, you may experience difficulty when attempting Installing the Control Panel in a to remove it. It is therefore Remote Location recommended that the control panel be permanently mounted in a remote For your convenience, the control panel can be removed location or remain intact with the unit. -
Page 12: Water Connections
NSTALLATION Caution Do not connect feed water until direct- ed to do so during “Initial Cleaning.” Water Connections Feed Water Connection Accu DIspense Locate the length of 3/8” O.D. tubing provided control cable with the unit with a quick disconnect insert on one end and a 3/8”... -
Page 13: Tubing Installation
NSTALLATION Tubing Installation To make tubing connections: Make sure the tubing is cut off reasonably COLLET square and that no plastic burrs or ridges are present. TYPICAL TUBING FITTING *Mark from end of tube the length of insertion. Tube size Insertion length 1/4 O.D. -
Page 14: Controls
Controls Main Power Switch The main power switch on the NANOpure DIamond Analytical is located on the lower back right side of the unit (as you face the front of the unit), directly above the power cord receptacle. Note Control Panel The removable control panel was not The NANOpure DIamond Analytical is controlled through designed to be repeatedly removed... - Page 15 ONTROLS of the unit as you face the unit) is ON, the switches on the control panel function as follows: START/STOP allows you to alternate the unit between the normal (recirculation) mode; when the display is showing purity, and the (Idle) mode. STANDBY allows you to put the unit into standby, recircu- lating water for 10 minutes/hour.
-
Page 16: Initial Operation
Initial Operation Part Application DIamond Kit Organic Free R/O & Distilled Feed D50280 Ultra-Low Organics, Type 1 Water, Reverse Osmosis or Distilled Water Feed DIamond Kit Organic Free Deionized Feed D50281 Ultra-Low Organics, Type 1 Water, Deionized Water Feed Warning DIamond Kit Type 1 R/O &... -
Page 17: Initial Rinse
NITIAL PERATION Initial Rinse Attach the feed water line to the unit by snap- ping the quick disconnect coupling into the quick disconnect body in the lower left back of the unit. Attach an atmospheric drain line [1/4” (.64 cm) ] tubing by pushing into the quick connect fitting on the lower left back of unit. -
Page 18: System Cleaning Procedure
NITIAL PERATION System Cleaning Procedure Your NANOpure DIamond Analytical has been shipped Warning with a cleaning syringe (Cat. No. CMX25). When the sys- Avoid splashing cleaning solution on tem is new or whenever a new cartridge pack is installed, clothing or skin. the system should be cleaned. - Page 19 NITIAL PERATION 13. Press the UP or DOWN arrow to select (YES) and press ENTER. Display will now read, “Unit Cleaning.” 14. Unit may now be left unattended until display reads, “Cleaning Complete: Press ENTER.” 15. After cleaning is complete the unit will return to the (Idle) mode.
-
Page 20: Normal Operation
Normal Operation Note Turn the system power ON by depressing the main On initial start-up, the purity meter power switch to the “I” position. may display “...MΩ-cm or uS/cm.” This is caused by air in the cell and should The system greeting display indicates the type of be replaced by a resistivity reading unit you own. -
Page 21: User Settings
User Settings Adjusting Display Brightness From the (Idle) mode, when the display reads, “NANOpure Diamond (Idle) xx:xx:xx xx/xx/xx,” press the UP or DOWN arrow until dis- play reads, “Advanced Menu?” Press ENTER. Press ENTER to proceed through the options until “Set Display Brightness” is displayed. Press the UP or DOWN arrow to choose “Yes.”... -
Page 22: Setting The Date And Time
ETTINGS Setting the Date and Time From the (Idle) mode, when the display reads, Note “NANOpure DIamond (Idle) xx:xx:xx Time values are displayed in 24 hr. xx/xx/xx,” press the UP or DOWN arrow until display military time. For example; 6:00p.m. = reads, “Advanced Menu?”... -
Page 23: Setting The Cell Constant
ETTINGS Setting the Cell Constant The actual temperature and cell constants are attached to the cell cable internal to the NANOpure DIamond unit. This data helps ensure that the purity displayed is as accurate as possible. The only time the user would need to enter this data is if the cell or main board is being replaced and/or updated. -
Page 24: Use Of Standby Mode
ETTINGS Use of Standby Mode Note At the end of the work day, place the NANOpure DIamond When in Standby mode, press Analytical in Standby mode for the night. To place the unit START/STOP to continue normal oper- in Standby mode: ation. -
Page 25: Resetting The Cleaning Timer
ETTINGS The second line of the display will show a “Below Set point” message once every 8 to 10 seconds when the measurement is below the set point. (The set point indica- tion is set at the factory at 10 MΩ-cm.) Resetting the Cleaning Timer From the (Idle) mode, when the display reads, “NANOpure DIamond (Idle) xx:xx:xx... -
Page 26: Setting Timed Dispensing
ETTINGS UP arrow: +0.25 up to 1 L, then 5 L, then incremental by 5 L. DOWN arrow: Decrement by 1 L until 1 L, then by 0.25 L. Maximum: 60 L Minimum: 0.25 L Setting Timed Dispensing From the normal recirculating mode, when the display is showing purity, press the UP or DOWN arrow until the display reads, “Auto Dispense Menu?”... -
Page 27: Performing A System Flush
ETTINGS Performing a System Flush From the normal recirculating mode, when the dis- play is showing purity, press the UP or DOWN arrow until the display reads, “System Flush?” Press ENTER. Press the UP or DOWN arrow to select “Short Flush?”... -
Page 28: Auto Standby
ETTINGS Auto Standby (Factory set to “NO”) Note This option allows for a convenient method for the user to If set to “YES”, unit will automatically ensure that the NANOpure DIamond Analytical unit will be enter Standby Mode only once per placed in Standby at a predetermined time each day. - Page 29 ETTINGS until “UNIT UNDER COUNTER” is displayed. Press the UP or DOWN arrow to choose “YES.” Press ENTER. Press BACK until you return to the (Idle) display.
-
Page 30: Accessories
Accessories Feedwater Float or Pressure Switch Accessories D8964 (float switch) and D2706 (pressure switch) are designed to protect the NANOpure DIamond Analytical pump by alerting the system of an inadequate feed water condition so that the pump can be shut down. If an inadequate feed water condition exists and the pump is shut down due to this condition, the display will read “Check Inlet.”... -
Page 31: Dispense Overflow Cutoff Float
CCESSORIES Dispense Overflow Cutoff Float Caution Accessory AY1367X1 (overflow float with 6 ft [2.83 meter] This accessory is not intended for cable) is designed as a user option to ensure automatic use with small containers as its dispensers (time or volumetric) do not overflow carboy weight could cause small, light- style containers. -
Page 32: Performing An Electronic Calibration Using The Optional N.i.s.t. Calibration Module
CCESSORIES Performing an Electronic Calibration Using the Optional N.I.S.T. Calibration Module If you purchased the optional N.I.S.T. calibration module (Catalog No. E896X5) you can perform a calibration of the NANOpure DIamond purity sensing electronics traceable to N.I.S.T. standards. Disconnect power cord from the unit. Unlatch and open the right door. -
Page 33: Manual Remote Dispenser And Accu Dispense Volumetric Remote Dispenser
CCESSORIES 12. Turn the main power switch to the OFF “O” position. Unplug the unit. 13. Remove the calibration module and reconnect the cell. 14. Reattach the cover plate and close and latch the door. 15. Reconnect the power cord. The calibration procedure is complete. -
Page 34: Computer/Printer Setup
Computer/Printer Setup Connecting NANOpure DIamond to Computer and Communicating Through the RS-232 Port Using Hyperterminal or Procomm Hyperterminal RS-232 Capture Instructions Connect the 9 pin serial cable (part no. WHX18) from the NANOpure DIamond RS-232 port to COM2: port or (COM1: port) on back of computer. - Page 35 OMPUTER RINTER ETUP you name in the c:/windows directory called cap- ture.txt and the file will be an ASCII text file. 11. You should see the data on the computer screen. 12. When you are finished storing data from the NANOpure DIamond, save your file.
-
Page 36: Connecting And Starting The Printer
OMPUTER RINTER ETUP 12. Type in 21 <Enter>, sets to COM2: or (Type in 20 <Enter>, sets to COM1:), depending on your computer. 13. Type in 24 <Enter>, saves settings. 14. Type ESC to exit setup menu. 15. Procomm is now ready to accept input from the NANOpure DIamond. -
Page 37: Printer Setup
OMPUTER RINTER ETUP 10. During normal Recirculation mode, a purity and temperature reading will be printed once every 12 minutes. Printer Setup Power Switch Located on the front of the printer (AY1137X1), this switch turns power to the printer ON and OFF. The POWER light will illuminate when the printer is ON. -
Page 38: Maintenance And Servicing
Maintenance and Servicing General Cleaning Instructions Warning Disconnect electrical service to the unit. Wipe exterior sur- • Avoid splashing mild detergent faces with lightly dampened cloth containing mild soap or weak acid on clothing or solution. skin • Ensure all piping connections Cell Cleaning are tight to avoid chemical leakage... -
Page 39: System Cleaning
AINTENANCE AND ERVICING System Cleaning Note It is best to perform cleaning procedures early in the The cleaning timer will display after six afternoon. After cleaning is complete (approximately 3.5 months, reminding you to clean the hours), place the unit into its normal (recirculation) mode unit. -
Page 40: System Depressurization
AINTENANCE AND ERVICING 14. Unit may now be left unattended until the display reads, “Cleaning Complete: Press ENTER.” 15. After cleaning is complete and the user presses “ENTER” the unit will return to the (Idle) mode. 16. Press the START/STOP switch to return the unit to the normal recirculating mode. -
Page 41: Cartridge Pack Replacement
AINTENANCE AND ERVICING Cartridge Pack Replacement Warning The frequency with which you will need to clean your unit Depressurize system prior to removing and replace your cartridge pack is dependent on your cartridge pack. feed water’s characteristics, your purity requirements and your usage. -
Page 42: 0.2 Micron Filter Replacement
AINTENANCE AND ERVICING Caution Do not overtighten the 0.2 micron filter or use excessive force in seating it. 0.2 Micron Filter Replacement The filter can be damaged by over- tightening or excessive force. Replace the 0.2 micron final filter whenever any of the fol- lowing conditions occur: the product water flow rate is reduced or bacteria break through. -
Page 43: Shutdown
AINTENANCE AND ERVICING Shutdown If the NANOpure DIamond Analytical is to be shut down for an extended period of time, the unit should be com- pletely drained and the cartridge pack removed to prevent the growth of bacteria. If the system has remained inac- tive and full of water for more than 96 hours, the unit should be drained, cleaned and new cartridge pack installed prior to use. -
Page 44: Troubleshooting
Troubleshooting Problem Possible Causes Solutions NANOpure DIamond completely No electrical power to NANOpure Ensure NANOpure DIamond power inactive (pump and display DIamond. cord is connected to a live power not operating.) source and completely plugged into electrical outlet as well as power entry module on the unit. - Page 45 ROUBLESHOOTING Problem Possible Causes Solutions Short cartridge pack life. Cartridge pack is beyond Check the expiration date. Cartridge expiration date. packs begin to lose capacity after being stored for 2 years from the date of manufacture. Replace the cartridge pack with an unexpired one. Poor quality feed water.
- Page 46 ROUBLESHOOTING Problem Possible Causes Solutions Display reads, “Meter PC board communication error. Turn the NANOpure DIamond OFF Board Problem.” (I/O Switch) and restart the unit. System electronics failure. Replace the resistivity meter board mounted on the inside of the right door. Water is leaking between the Wing head screws are not Tighten wing head screws on unit...
-
Page 47: Replacement Parts
Replacement Parts Recommended Spares Consumables Consumable parts are those required to support the day-to-day operation of this equipment. We establish two types of consumables; those items that must periodically be replaced to maintain performance (filters, resin cartridges, etc.) and other items of limited life (indicator lights, fuses, etc.) that you can expect to replace on a more or less random basis. - Page 48 EPLACEMENT ARTS Safety Stock For critical applications where performance with minimum downtime is required, we recommend that you maintain a local stock of those parts listed in the General Maintenance Parts and Safety Stock sections. Description Catalog No. Recommended Quantity Display SW1190X2 External Display cable (Remote Display Use)
-
Page 49: Flow Chart
Flow Chart ITLE IGHT power switch turned on Barnstead Tx.xx Style English Unit/Meter Initialization & Meter Calibration Check NANOpure DIamond (Idle) xx :xx :xx xx /xx /xx standby back key up or down enter key start_stop key pressed key pressed pressed keys pressed pressed... -
Page 50: Wiring Diagram
Wiring Diagram... -
Page 51: Ordering Procedures
Ordering Procedures Please refer to the Specification Plate for the complete model number, serial number, and series number when requesting service, replacement parts or in any corre- spondence concerning this unit. All parts listed herein may be ordered from the Thermo Scientific dealer from whom you purchased this unit or can be obtained promptly from the factory. -
Page 52: Two Year Limited Warranty
(ii) misuse (including use inconsistent with written operating instructions for the product), mishandling, contamination, overheating, modification or alteration of the product by any customer or third party or (iii) use of replacement parts that are obtained from a party who is not an authorized dealer of Thermo Scientific prod- ucts.