Hach LANGE TitraLab KF1000 Series User Manual
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- Basic user manual (176 pages) ,
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- Basic user manual (510 pages)
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Summary of Contents for Hach LANGE TitraLab KF1000 Series
- Page 1 DOC022.52.93082 ® TitraLab KF1000 series workstations User Manual 12/2014, Edition 1...
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Page 3: Table Of Contents
Table of Contents Section 1 Specifications ........................3 Section 2 General information ......................5 2.1 Safety information........................5 2.1.1 Use of hazard information....................5 2.1.2 Precautionary labels......................5 2.1.3 Certification......................... 6 2.2 Product overview.......................... 6 2.3 Instrument connections........................ 7 2.4 Product components........................8 Section 3 Installation .......................... - Page 4 Table of Contents 7.6.5 Other maintenance options....................32 7.7 Storage and transportation......................33 7.7.1 Prepare the instrument for short-term storage..............33 7.7.2 Prepare the instrument for long-term storage..............33 7.7.3 Prepare the instrument for shipment................. 33 Section 8 Troubleshooting ......................35 Section 9 Replacement parts and accessories ................
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Page 5: Section 1 Specifications
Section 1 Specifications Specifications are subject to change without notice. Specification Details Dimensions (W x D x H) 22 x 40 x 36 cm (8.7 x 15.7 x 14.2 in.) Weight 4 kg (8.8 lb) Power requirements 100–240 VAC, 50/60 Hz Altitude 2,000 m (6,562 ft) maximum Operating temperature... - Page 6 Specifications...
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Page 7: Section 2 General Information
Section 2 General information In no event will the manufacturer be liable for direct, indirect, special, incidental or consequential damages resulting from any defect or omission in this manual. The manufacturer reserves the right to make changes in this manual and the products it describes at any time, without notice or obligation. -
Page 8: Certification
General information This symbol indicates the presence of devices sensitive to Electro-static Discharge (ESD) and indicates that care must be taken to prevent damage with the equipment. Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August of 2005. -
Page 9: Instrument Connections
General information Figure 1 Product overview 1 Keypad 6 Beaker 11 Sensor holder 2 Display 7 Syringe protection cover 12 Pump 2 input/output (waste) 3 Sensor storage tubes 8 Syringe input/output 13 Pump 1 input/output (solvent) 4 USB port 9 Tube clips 14 Pump access cover 5 Sample stopper 10 Syringe... -
Page 10: Product Components
General information 2.4 Product components Make sure that all components have been received. Refer to the packing list in the box. If any items are missing or damaged, contact the manufacturer or a sales representative immediately. Figure 3 Contents of the instrument box 1 Instrument 3 Sensor storage tubes (3x) 5 Power cord... -
Page 11: Section 3 Installation
Section 3 Installation C A U T I O N Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document. 3.1 Installation guidelines • This instrument is for indoor use only. • The power supply connector on the rear panel must be easily accessible so the power can be disconnected quickly in case of emergency. - Page 12 Installation...
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Page 13: Install The Sensor Storage Tubes
Installation 3.4 Install the sensor storage tubes Put the three sensor storage tubes into the holder that is on the side of the instrument. Refer to Figure 1 on page 7. 3.5 Install the sensor holder accessories Add the stir bar to the beaker, and then attach the beaker to the sensor holder. Install the desiccant cartridge and the sample stopper. -
Page 14: Install The Sensor
Installation 3.8 Install the sensor 3.8.1 Connect the sensor Use a conical adapter to hold the sensor tightly in the sensor holder. Make sure the conical adapter is installed correctly. This makes sure of a secure water-tight fitting in the sensor holder and the tip of the sensor will be in the correct position in the beaker. -
Page 15: Install The Titrant And The Reagent
Installation 3.9 Install the titrant and the reagent C A U T I O N Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets (MSDS/SDS) for safety protocols. -
Page 16: Tidy The Work Area
Installation 3.10 Tidy the work area Attach the tubes to the instrument with the clips on the electrovalve and the sensor holder. Refer to the illustrated steps that follow. 3.11 Install accessories 3.11.1 Install an external pump This accessory (Item no. LZE142) is used to remove unwanted sample from the beaker. -
Page 17: Install An External Propellor
Installation 1. Remove any bends in the end of the tube from the inlet port on the pump. 2. Push the tube into a tube holder slot so it is correctly attached. 3. Make sure that the end of the tube is near the bottom of the beaker. 4. - Page 18 Installation...
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Page 19: Section 4 User Interface And Navigation
Section 4 User interface and navigation 4.1 Keypad Figure 6 shows the keypad and gives the key functions. Figure 6 Keypad 1 Power 4 Navigation keys 2 Printer 5 Home 3 Selection keys Description Power Sets the instrument power to on or off. Push the key for 2 seconds to set the power to off. Printer Sends data to an attached printer. - Page 20 User interface and navigation...
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Page 21: Section 5 Startup
Section 5 Startup C A U T I O N Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets (MSDS/SDS) for safety protocols. C A U T I O N Personal injury hazard. - Page 22 Startup 3. Choose an application to change from the installed list and then push Edit. 4. Push the arrow keys to scroll through the application parameters. The Edit key is only available when a parameter can be changed. Note: Push the left and right arrow keys to go to the previous or next parameter group. 5.
- Page 23 Startup Table 7 Titrant parameters Parameter Description Basic mode Expert mode Name Titrant name Titrant concentration Nominal titrant concentration Resolution Number of decimals to show for the nominal concentration Unit Titrant unit Real concentration Actual concentration of the titrant that is used in measurement calculation Resolution Number of decimals to show for the real concentration...
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Page 24: Install The Applications
Startup Table 8 KF titration parameters Parameter Description Basic mode Expert mode Active Specify if the method should be used during the analysis Stirring speed Stirring speed during the titration Measured parameter Parameter measured by the probe Delay Stirring time before the titration starts Injection autodetect Define if the calibration starts after the automatic detection of a sample injection... -
Page 25: Prepare The Instrument For Measurement
Startup 5.3 Prepare the instrument for measurement 1. From the main menu, select Purge, then push Start. All attached devices are listed. 2. Select All elements to purge all the attached devices, or select one device to purge. Push Select. Air is removed from the device and filled with liquid from the bottle. 3. - Page 26 Startup...
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Page 27: Section 6 Standard Operations
Section 6 Standard operations C A U T I O N Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document. C A U T I O N Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled. -
Page 28: Cell Management
Standard operations 14. Weigh the empty sample container and subtract this value from the weight of the sample in its container (refer to step 11). The result is the exact weight of the sample analyzed. Write down this value. 15. Push Start to start the moisture content analysis. Measurement data shows on the display. -
Page 29: Manage The Data Log
Standard operations 6.3 Manage the data log To select data to view, delete or export, specify data filters 1. From the main menu, select Data log. 2. Select an option, then push Select. Option Description View data log Views measurement data. Select individual lines of data to view more content. - Page 30 Standard operations...
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Page 31: Section 7 Maintenance
Section 7 Maintenance C A U T I O N Multiple hazards. Only qualified personnel must conduct the tasks described in this section of the document. N O T I C E Do not disassemble the instrument for maintenance. If the internal components must be cleaned or repaired, contact the manufacturer. -
Page 32: Regenerate The Molecular Sieve
Maintenance For other sensors, obey the cleaning instructions given in the documentation supplied with the sensor. 7.4 Regenerate the molecular sieve It is recommended to regenerate the molecular sieve weekly, but this will vary depending on the humidity of the laboratory. A humidity indicator, such as color changing silica gel crystal, can be used to show when regeneration is necessary. -
Page 33: Maintenance Menu
Maintenance 7.6 Maintenance menu Select Maintenance from the main menu. 7.6.1 Syringe activation Do a check of the syringe. Make sure the syringe fills and empties correctly. 1. From the maintenance menu, push Syringe activation. Option Description Fill Fills the syringe with titrant solution. The process stops automatically when the syringe is full. -
Page 34: Other Maintenance Options
Maintenance 7.6.5 Other maintenance options 1. Select an option, then push Select. Option Description Stirring activation Do a check of the magnetic stirrer. Push the up and down arrow keys to increase or decrease the stirring speed. Live measure This option is not available for all sensors. The option shows continuous measurement data with connected sensors to quickly check measurements. -
Page 35: Storage And Transportation
Maintenance Option Description Maintenance See the number of days remaining for maintenance tasks. After doing a summary task, push Reset to set the number of days remaining to the default value. Maintenance See the list of maintenance tasks. Push Edit to change the default schedule value. - Page 36 Maintenance...
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Page 37: Section 8 Troubleshooting
Section 8 Troubleshooting Refer to the following table for common problem messages or symptoms and possible causes. Error/Warning Description Stop requested The operator has pushed the stop button Measurement out of range The measurement is out of range Temperature out of range The temperature measurement is out of range Temperature unknown The temperature measurement cannot be determined... - Page 38 Troubleshooting...
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Page 39: Section 9 Replacement Parts And Accessories
Section 9 Replacement parts and accessories W A R N I N G Personal injury hazard. Use of non-approved parts may cause personal injury, damage to the instrument or equipment malfunction. The replacement parts in this section are approved by the manufacturer. Note: Product and Article numbers may vary for some selling regions. - Page 40 Replacement parts and accessories...
- Page 42 Tel. +49 (0) 2 11 52 88-320 SWITZERLAND Fax (970) 669-2932 Fax +49 (0) 2 11 52 88-210 Tel. +41 22 594 6400 orders@hach.com info@hach-lange.de Fax +41 22 594 6499 www.hach.com www.hach-lange.de © Hach Company/Hach Lange GmbH, 2014. All rights reserved. Printed in Germany.