Chapter 3:  Use, Maintenance, & Diagnostics; Using The Dsc; Before You Begin - TA Instruments DSC Q Series Getting Started Manual

Differential scanning calorimeter
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Using the DSC

All of your DSC experiments will have the following general outline. In some cases, not all of these steps will
be performed. The majority of these steps are performed using the instrument control software. The instructions
needed to perform these actions can be found in the online help in the instrument control program; therefore,
they will not all be covered in detail here.
Calibrating the instrument
Selecting the pan type and material
Preparing the sample
Creating or choosing the test procedure and entering sample and instrument information through the TA
instrument control software
Setting the purge gas flow rate
Loading the sample and closing the cell lid
Starting the experiment.
To obtain accurate results, follow procedures carefully.

Before You Begin

Before you set up an experiment, ensure that the DSC and the controller have been installed properly. Make
sure you have:
Made all necessary cable connections from the DSC to the computer
Connected all gas lines
Powered up the unit
Connected any desired accessories
Connected the instrument with the controller
Become familiar with controller operations
Calibrated the DSC, if necessary.
DSC Q Series Getting Started Guide
Use, Maintenance, & Diagnostics
Chapter 3
47

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Q10Q1000Q20Q2000Q100Q200

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