Temperature Calibration - CEM EDGE system Manual

Energized dispersive guided extraction
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Once the tool/Q-Cup looks aligned, select "Coarse," and then select the Z-axis "up" arrow once and then
down once. The tool/cup should move freely without hitting any sides. If this is not a smooth transition, retry
calibrating the drop-off position before pressing ok.
16. Once the position is calibrated, press "OK" to proceed to the next step.
17. Remove the tool/cup from the system before calibrating the waste position; No tool/Q-Cup is used for calibrat-
ing the waste.
18. Select "Estimate."
19. Move the autosampler using "Fine" and "Ultrafine" in small increments only. Move the autosampler until the
needle is at least ¾ into the waste port.
20. Select "OK" to save calibration values.

Temperature Calibration

This should be performed yearly by a CEM Service Engineer. Contact CEM Corporation before calibrating
temperature.
WARNING
Do not place hands or objects in the actuator (vessel chamber) area unless instructed to do so.
NOTE
Before starting, water should be plumbed into one of the solvent lines. A thermometer will be needed to
record the temperature during calibration.
1. Select the System Menu icon
2. Select Tools.
3. Select Calibration.
in the bottom right corner of the screen.
Calibrations
47

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