Agilent Technologies 1290 Infinity II User Manual
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Agilent Technologies 1290 Infinity II User Manual

Agilent Technologies 1290 Infinity II User Manual

Infinitylab lc series ms flow modulator
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Summary of Contents for Agilent Technologies 1290 Infinity II

  • Page 1 Agilent InfinityLab LC Series 1290 Infinity II MS Flow Modulator User Manual Agilent Technologies...
  • Page 2 Notices Warranty © Agilent Technologies, Inc. 2017 receive no greater than Restricted Rights as defined in FAR 52.227-19(c)(1-2) (June No part of this manual may be reproduced The material contained in this docu- 1987). U.S. Government users will receive in any form or by any means (including ment is provided “as is,”...
  • Page 3 In This Guide… In This Guide… This manual covers the Agilent InfinityLab LC Series 1290 Infinity II MS Flow Modulator (G7170B) 1 Introduction This chapter gives an introduction to the module. 2 Site Requirements and Specifications This chapter provides information on environmental requirements, physical and performance specifications.
  • Page 4 In This Guide… 9 Identifying Cables This chapter provides information on cables used with the modules. 10 Hardware Information This chapter describes the module in more detail on hardware and electronics. 11 Appendix This chapter provides addition information on safety, legal and web. MS Flow Modulator User Manual...

  • Page 5: Table Of Contents

    Contents Contents 1 Introduction 1290 Infinity II MS Flow Modulator Features (G7170B) Leak and Waste (G7170B) Operating Principle 2 Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications 3 Installing the Module Unpacking the Module Installation of the MS Flow Modulator...
  • Page 6 10 Hardware Information Electrical Connections Interfaces Config Switch Settings of the Infinity Valve Drive 11 Appendix General Safety Information Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Radio Interference Sound Emission Agilent Technologies on Internet MS Flow Modulator User Manual...

  • Page 7: Introduction

    MS Flow Modulator User Manual Introduction 1290 Infinity II MS Flow Modulator Features (G7170B) Leak and Waste (G7170B) Operating Principle This chapter gives an introduction to the module. Agilent Technologies...

  • Page 8: 1290 Infinity Ii Ms Flow Modulator

    Introduction 1290 Infinity II MS Flow Modulator 1290 Infinity II MS Flow Modulator Based on technology in our InfinityLab Quick Change valves, the 1290 Infinity II MS Flow Modulator facilitates efficient flow control for mass-based fraction collection on all InfinityLab LC Purification Solutions. The Flow Modulator is a compact module suitable for flow rates up to 100 mL/min and supports split ratios between 40:1 and 400000:1 with split frequencies up to 2 Hz.

  • Page 9: Features (G7170B)

    Introduction Features (G7170B) Features (G7170B) Purification efficiency • Supports wide range of split modes from 40:1 up to 400000:1 depending on flow rate • Enables split frequencies of up to 2 Hz • Handles flow rates up to 100 mL/min Instrument efficiency •...

  • Page 10: Leak And Waste (G7170B)

    This example shows the leak and waste concept of the module, if installed to a leak tray and attached to another module. Alternatively, the module can be installed and integrated to the leak and waste concept of 1290 Infinity II Preparative Column Compartment.

  • Page 11: Operating Principle

    Introduction Operating Principle Operating Principle The flow modulator is a compact, active splitting device configured to deliver three different unique aliquots from a HPLC to a Single Quad Mass Spectroscopic Detector while maintaining uninterrupted flow. Aliquot Transfer Principle of aliquot transfer (see also Figure 2 on page 11): 1 In the Aliquot Fill position, HPLC effluent enters Port 1 where a portion of...
  • Page 12 Introduction Operating Principle Calculation of the Split Ratio • The MS Flow Modulator has 4 ports with 6 positions (2 x 3) • The user can choose the size of aliquots, from three aliquots • The valve will move the rotor between two of the same aliquots, backwards and forwards The user can change the gating frequency of the valve from 14 different modes...

  • Page 13: Site Requirements And Specifications

    MS Flow Modulator User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter provides information on environmental requirements, physical and performance specifications. Agilent Technologies...

  • Page 14: Site Requirements

    Site Requirements and Specifications Site Requirements Site Requirements A suitable environment is important to ensure optimal performance of the instrument. Power Considerations The module power supply has wide ranging capability. It accepts any line voltage in the range described in Table 1 on page 17.
  • Page 15 Never use the power cords that Agilent Technologies supplies with this instrument for any other equipment. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. Power cords WA R N I N G Solvents may damage electrical cables.
  • Page 16 Site Requirements and Specifications Site Requirements Condensation Condensation within the module C AU T I O N Condensation can damage the system electronics. ➔ Do not store, ship or use your module under conditions where temperature fluctuations could cause condensation within the module. ➔...

  • Page 17: Physical Specifications

    Site Requirements and Specifications Physical Specifications Physical Specifications Table 1 Physical Specifications Type Specification Comments Weight 2.2 kg (4.9 lbs) Dimensions 95 x 95 x 300 mm (height × width × depth) (3.7 x 3.7 x 11.8 inches) Line voltage 100 –...

  • Page 18: Performance Specifications

    Site Requirements and Specifications Performance Specifications Performance Specifications Table 2 Performance Specifications 1290 Infinity II MS Flow Modulator (G7170B) Feature Specification Comment External Leak Sensor controlled via ERI Flow rate 4 – 200 mL/min Maximum Pressure 69 bar (100 psi)

  • Page 19: Installing The Module

    Installation of the MS Flow Modulator Assembling and Installing the Leak Tray and Leak Sensor Mounting the MS Flow Modulator to an Instrument Mount the MS Flow Modulator to the 1290 Infinity II Preparative Column Compartment. Install the MS Flow Modulator...

  • Page 20: Unpacking The Module

    For parts identification please check the illustrated parts breakdown in the chapter Parts and Materials. Please report any missing or damaged parts to your local Agilent Technologies sales and service office. Accessory Kit The flow modulator is shipped with Accessory Kit (G9352-68100) (see “Accessory Kit for the Flow Modulator”...

  • Page 21: Installation Of The Ms Flow Modulator

    The MS Flow Modulator can be installed in different ways. • Mounted to another module The MS Flow Modulator fits on Infinity I rails or Infinity II clamps. N O T E • Inside the 1290 Infinity II Preparative Column Compartment MS Flow Modulator User Manual...

  • Page 22: Assembling And Installing The Leak Tray And Leak Sensor

    Installing the Module Installation of the MS Flow Modulator Assembling and Installing the Leak Tray and Leak Sensor Only connect or disconnect the leak sensor while the module is powered off. N O T E The module must be ‘powered off’ for at least 10 s to recognize any hardware changes correctly.

  • Page 23: Mounting The Ms Flow Modulator To An Instrument

    Installing the Module Installation of the MS Flow Modulator Mounting the MS Flow Modulator to an Instrument "Defective on arrival" problems C AU T I O N If there are signs of damage, please do not attempt to install the module. Inspection by Agilent is required to evaluate if the instrument is in good condition or damaged.

  • Page 24: Mount The Ms Flow Modulator To The 1290 Infinity Ii Preparative Column Compartment

    Installing the Module Installation of the MS Flow Modulator Mount the MS Flow Modulator to the 1290 Infinity II Preparative Column Compartment. Slide the MS Flow Modulator into a free slot of the 1290 Infinity II Preparative Column Compartment. Position the module correctly above the leak tray.

  • Page 25: Install The Ms Flow Modulator

    Modulator. Slide the flow modulator into a free slot inside the column compartment, see “Mount the MS Flow Modulator to the 1290 Infinity II Preparative Column Compartment.” on page 24. N O T E Use the finger tight 10-32 male threaded UHPFF fittings only, that are supplied with the splitter.
  • Page 26 Installing the Module Installation of the MS Flow Modulator Connect the power cable to the power connector at the Connect the CAN interface connection. rear of the module. Next Steps: Power on the flow modulator by switching the power button at the rear of the module. N O T E To power cycle the module (necessary for example after a valve head, or leak sensor installation), wait for at least 10 seconds before re-powering.

  • Page 27: Install The Valve Head And Connecting Capillaries

    Installing the Module Installation of the MS Flow Modulator Install the valve head and connecting capillaries The valve actuator contains sensitive optical parts, which need to be protected from C AU T I O N dust and other pollutions. Pollution of these parts can impair the accurate selection of valve ports and therefore bias measurement results.
  • Page 28 Installing the Module Installation of the MS Flow Modulator Insert the valve head into the valve shaft. When the outer pin is locked into the groove, manually screw the nut onto the valve head. N O T E If the outside pin does not fit into the outside groove, you have to turn the valve head until you feel that the two pins Fasten the nut with the 5043-1767 Valve Removal tool.
  • Page 29 Installing the Module Installation of the MS Flow Modulator Install all required capillary connections to the valve. Power on or power-cycle your module, so the valve head gets recognized during module initialization. MS Flow Modulator User Manual...
  • Page 30 Installing the Module Installation of the MS Flow Modulator MS Flow Modulator User Manual...

  • Page 31: Using The Module

    MS Flow Modulator User Manual Using the Module Overview Solvent Information Material Information Status Indicator Leak and Waste Handling Waste Concept Configure the Flow Modulator This chapter provides information on how to use the module. Agilent Technologies...

  • Page 32: Overview

    Using the Module Overview Overview The flow modulator is a compact, active splitting device capable of automated control. For details, see “Operating Principle” on page 11. The split ratio depends on the main flow rate, the rotor seal groove size (aliquot volume) and the frequency (aliquots gated to the MS): Use the controller software to establish the required split ratio, see “Configure...

  • Page 33: Solvent Information

    Using the Module Solvent Information Solvent Information Chemical Compatibility Chemical compatibility of the valve parts C AU T I O N Corrosion of stator seal and rotor seal. ➔ Do not use sulfuric acid and generally avoid the use of concentrated acids. ➔...
  • Page 34 Using the Module Solvent Information Solvent compatibility for stainless steel in standard LC systems Stainless steel is inert against many common solvents. It is stable in the presence of acids and bases in the pH range specified for standard HPLC (pH 1 –...

  • Page 35: Material Information

    Using the Module Solvent Information Material Information Materials in the flow path are carefully selected based on Agilent’s experiences in developing highest quality instruments for HPLC analysis over several decades. These materials exhibit excellent robustness under typical HPLC conditions. For any special condition, please consult the material information section or contact Agilent.
  • Page 36 Polyethylene (PE) Agilent uses UHMW (ultra-high molecular weight)-PE/PTFE blends for yellow piston and wash seals, which are used in 1290 Infinity pumps, 1290 Infinity II pumps, the G7104C and for normal phase applications in 1260 Infinity pumps. Polyethylene has a good stability for most common inorganic solvents including acids and bases in a pH range of 1 to 12.5.
  • Page 37 Using the Module Solvent Information Stainless Steel (ST) Stainless steel is inert against many common solvents. It is stable in the presence of acids and bases in a pH range of 1 to 12.5. It can be corroded by acids below pH 2.3. It can also corrode in following solvents: •...
  • Page 38 Using the Module Solvent Information significantly reduces corrosion rates. Titanium is sensitive to acidic metal chlorides like FeCl or CuCl . Titanium is subject to corrosion in anhydrous methanol, which can be avoided by adding a small amount of water (about 3 %).
  • Page 39 Using the Module Solvent Information Fluorinated polymers (PTFE, PFA, FEP, FFKM, PVDF) Fluorinated polymers like PTFE (polytetrafluorethylene), PFA (perfluoroalkoxy) and FEP (fluorinated ethylene propylene) are inert to almost all common acids, bases, and solvents. FFKM is perfluorinated rubber, which is also resistant to most chemicals. As an elastomer, it may swell in some organic solvents like halogenated hydrocarbons.

  • Page 40: Status Indicator

    Using the Module Status Indicator Status Indicator Status indicators 1 Idle 2 Run mode 3 Not-ready. Waiting for a specific pre-run condition to be reached or completed. 4 Error mode - interrupts the analysis and requires attention (for example a leak or defective internal components).

  • Page 41: Leak And Waste Handling

    Using the Module Leak and Waste Handling Leak and Waste Handling Toxic, flammable and hazardous solvents, samples and reagents WA R N I N G The handling of solvents, samples and reagents can hold health and safety risks. ➔ When working with these substances observe appropriate safety procedures (for example by wearing goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet supplied by the vendor, and follow good laboratory practice.

  • Page 42: Waste Concept

    Using the Module Leak and Waste Handling Waste Concept 1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports (5043-1221) for optimal and safe waste disposal. If you decide to use your own waste solution, make sure that the tubes don't immerse in the liquid.

  • Page 43: Configure The Flow Modulator

    Using the Module Configure the Flow Modulator Configure the Flow Modulator 1 Choose your module from the list of Modules, click on >. You can now configure your module. 2 Click Autoconfig to configure the module automatically. Click Configure, manually configure the module and click Ok to confirm the configuration.
  • Page 44 Using the Module Configure the Flow Modulator 3 To create a method, right click on the dashboard and select Method..4 Set the required parameters. The possible Split Modes are calculated automatically by the software. MS Flow Modulator User Manual...
  • Page 45 Using the Module Configure the Flow Modulator 5 Select the Split Mode. 6 Click Ok to save the method. MS Flow Modulator User Manual...
  • Page 46 Using the Module Configure the Flow Modulator MS Flow Modulator User Manual...

  • Page 47: Troubleshooting And Diagnostics

    MS Flow Modulator User Manual Troubleshooting and Diagnostics User Interfaces Agilent Lab Advisor Software Overview about the troubleshooting and diagnostic features. Agilent Technologies...

  • Page 48: User Interfaces

    Troubleshooting and Diagnostics User Interfaces User Interfaces • Depending on the user interface, the available tests and the screens/reports may vary. • Preferred tool should be Agilent Lab Advisor Software, see “Agilent Lab Advisor Software” on page 49. • The Agilent OpenLAB ChemStation C.01.03 and above do not include any maintenance/test functions.

  • Page 49: Agilent Lab Advisor Software

    Troubleshooting and Diagnostics Agilent Lab Advisor Software Agilent Lab Advisor Software The Agilent Lab Advisor Software is a standalone product that can be used with or without a chromatographic data system. Agilent Lab Advisor helps to manage the lab for high-quality chromatographic results by providing a detailed system overview of all connected analytical instruments with instrument status, Early Maintenance Feedback counters (EMF), instrument configuration information, and diagnostic tests.
  • Page 50 Troubleshooting and Diagnostics Agilent Lab Advisor Software MS Flow Modulator User Manual...

  • Page 51: Error Information

    Leak Module Specific Error Messages Initialization of Valve Failed Valve Switching Failed Valve Tag Violation This chapter describes the meaning of error messages, and provides information on probable causes and suggested actions how to recover from error conditions. Agilent Technologies...

  • Page 52: What Are Error Messages

    Error Information What Are Error Messages What Are Error Messages Error messages are displayed in the user interface when an electronic, mechanical, or hydraulic (flow path) failure occurs which requires attention before the analysis can be continued (for example, repair, or exchange of consumables is necessary).

  • Page 53: General Error Messages

    Error Information General Error Messages General Error Messages General error messages are generic to all Agilent series HPLC modules and may show up on other modules as well. Timeout Error ID: 0062 The timeout threshold was exceeded. Probable cause Suggested actions Check the logbook for the occurrence and The analysis was completed successfully, source of a not-ready condition.

  • Page 54: Shutdown

    Error Information General Error Messages Shutdown Error ID: 0063 An external instrument has generated a shutdown signal on the remote line. The module continually monitors the remote input connectors for status signals. A LOW signal input on pin 4 of the remote connector generates the error message.

  • Page 55: Remote Timeout

    Error Information General Error Messages Remote Timeout Error ID: 0070 A not-ready condition is still present on the remote input. When an analysis is started, the system expects all not-ready conditions (for example, a not-ready condition during detector balance) to switch to run conditions within one minute of starting the analysis.

  • Page 56: Leak Sensor Short

    Error Information General Error Messages Leak Sensor Short Error ID: 0082 The leak sensor in the module has failed (short circuit). The current through the leak sensor is dependent on temperature. A leak is detected when solvent cools the leak sensor, causing the leak sensor current to change within defined limits.

  • Page 57: Leak

    Error Information General Error Messages Leak Error ID: 0064 A leak was detected in the module. The signals from the two temperature sensors (leak sensor and board-mounted temperature-compensation sensor) are used by the leak algorithm to determine whether a leak is present. When a leak occurs, the leak sensor is cooled by the solvent.

  • Page 58: Module Specific Error Messages

    Error Information Module Specific Error Messages Module Specific Error Messages Initialization of Valve Failed Error ID: 24000 During the initialization process the motor of the valve drive moves to some special positions depending on the installed valve head. A failure in this process means either that the movement couldn’t be performed properly or it was not noticed correctly by the sensor.

  • Page 59: Valve Switching Failed

    Error Information Module Specific Error Messages Valve Switching Failed Error ID: 24001 The valve drive was not able to operate the valve head correctly. Either due to mechanical reasons or the movement couldn’t be detected correctly. Probable cause Suggested actions •...
  • Page 60 Error Information Module Specific Error Messages MS Flow Modulator User Manual...

  • Page 61: Maintenance

    Introduction to Maintenance Warnings and Cautions Cleaning the Module Replacing the Fuses of the Infinity Valve Drive Replace Rotor and Stator Replace Valve Heads Replacing the Module Firmware Module Specific Information This chapter describes the maintenance of the module. Agilent Technologies...

  • Page 62: Introduction To Maintenance

    Maintenance Introduction to Maintenance Introduction to Maintenance The module is designed for easy maintenance. Maintenance can be done from the front with module in place in the system. There are no serviceable parts inside. N O T E Do not open the module. MS Flow Modulator User Manual...

  • Page 63: Warnings And Cautions

    Maintenance Warnings and Cautions Warnings and Cautions Toxic, flammable and hazardous solvents, samples and reagents WA R N I N G The handling of solvents, samples and reagents can hold health and safety risks. ➔ When working with these substances observe appropriate safety procedures (for example by wearing goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet supplied by the vendor, and follow good laboratory practice.

  • Page 64: Cleaning The Module

    Maintenance Cleaning the Module Cleaning the Module To keep the module case clean, use a soft cloth slightly dampened with water, or a solution of water and mild detergent. Liquid dripping into the electronic compartment of your module can cause shock WA R N I N G hazard and damage the module ➔...

  • Page 65: Replacing The Fuses Of The Infinity Valve Drive

    Maintenance Replacing the Fuses of the Infinity Valve Drive Replacing the Fuses of the Infinity Valve Drive When If the flow module shows no reaction. Tools required Description Screwdriver Parts required Description 2110-1486 Fuse 2 AT250 V Electrical shock WA R N I N G ➔...
  • Page 66 Maintenance Replacing the Fuses of the Infinity Valve Drive To access the fuse drawer, gently lift the outer plastic Pull out the fuse drawer as shown. housing of the power inlet socket using a flat screwdriver. Replace the defect fuse(s). Slide in the fuse drawer and push till it fits tightly.

  • Page 67: Replace Rotor And Stator

    Maintenance Replace Rotor and Stator Replace Rotor and Stator Always replace rotor and stator as pair. N O T E Toxic, flammable and hazardous solvents, samples and reagents WA R N I N G The handling of solvents, samples and reagents can hold health and safety risks. ➔...
  • Page 68 Maintenance Replace Rotor and Stator With the hex key remove the screws from the stator. Remove the stator and stator seal from the stator ring (the stator seal usually remains on the stator). Remove the stator ring. Remove the rotor seal from the valve body. The rotor seal is mounted on three pins and can be pulled off.
  • Page 69 Maintenance Replace Rotor and Stator Replace the stator ring so the two short pins enter the Mount the new stator seal onto the stator. The pins on include three sets of replacement mating holes in the the assembly fit into the mating holes in the stator only body.

  • Page 70: Replace Valve Heads

    Maintenance Replace Valve Heads Replace Valve Heads Parts required Description InfinityLab MS Flow Modulator Valve 100 mL 5067-4292 Toxic, flammable and hazardous solvents, samples and reagents WA R N I N G The handling of solvents, samples and reagents can hold health and safety risks. ➔...
  • Page 71 Maintenance Replace Valve Heads Switch off the module. Remove all capillary connections from the valve head N O T E Use the provided Valve Removal tool if necessary. MS Flow Modulator User Manual...
  • Page 72 Maintenance Replace Valve Heads Unscrew the valve head. Insert the valve head into the valve shaft. If the outside pin does not fit into the outside groove, you have to turn the valve head until you feel that the two pins snap into the grooves.
  • Page 73 Maintenance Replace Valve Heads When the outer pin is locked into the groove, manually Install all required capillary connections to the valve. screw the nut onto the valve head. N O T E Fasten the nut with the 5043-1767 Valve Removal tool. Power on or power-cycle your module, so the valve head gets recognized during module initialization.

  • Page 74: Replacing The Module Firmware

    Maintenance Replacing the Module Firmware Replacing the Module Firmware When The installation of newer firmware might be necessary • if a newer version solves problems of older versions or • to keep all systems on the same (validated) revision. The installation of older firmware might be necessary •...

  • Page 75: Module Specific Information

    Maintenance Replacing the Module Firmware Module Specific Information Table 3 Module Specific Information (G7170B) Firmware Set B/C/D.07.20 Agilent OpenLab CDS A.02.02/C.01.07 SR3 HF1 LC drivers A.02.17 LabAdvisor B.02.10 MS Flow Modulator User Manual...
  • Page 76 Maintenance Replacing the Module Firmware MS Flow Modulator User Manual...

  • Page 77: Parts And Materials

    MS Flow Modulator User Manual Parts and Materials Accessory Kit for the Flow Modulator Optional Parts This chapter provides information on parts for maintenance. Agilent Technologies...

  • Page 78: Accessory Kit For The Flow Modulator

    Parts and Materials Accessory Kit for the Flow Modulator Accessory Kit for the Flow Modulator Accessory Kit (G9352-68100) Item Description 5043-0915 Fitting mounting tool 5043-1767 Valve Removal tool 5067-6821 Capillary ST, 0.12x100 SX/SX 5067-6820 Capillary ST, 0.25x80 SX/RLO 5067-5685 Clamp Guide Kit-IF-II 2110-1486 Fuse 2 AT250 V 5181-1519...
  • Page 79 Parts and Materials Accessory Kit for the Flow Modulator MS Flow Modulator User Manual...

  • Page 80: Optional Parts

    Parts and Materials Optional Parts Optional Parts Description InfinityLab MS Flow Modulator Valve 100 mL 5067-4292 Active Splitter Rebuild Kit (3 Stator/Rotor pairs) 1535-5215 1535-4045 Bearing ring 1535-4857 Stator screws 5067-1510 Rail assy for column organizer 5067-4634 Valve rail assembly G1369-60012 LAN Interface Card G9321-60013...

  • Page 81: Identifying Cables

    MS Flow Modulator User Manual Identifying Cables Cable Overview Analog Cables Remote Cables CAN/LAN Cables Agilent Module to PC This chapter provides information on cables used with the modules. Agilent Technologies...

  • Page 82: Cable Overview

    Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent 35900A A/D converter...
  • Page 83 Identifying Cables Cable Overview LAN cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) RS-232 cables (not for FUSION Description board) RS232-61601 RS-232 cable, 2.5 m Instrument to PC, 9-to-9 pin (female).

  • Page 84: Analog Cables

    Identifying Cables Analog Cables Analog Cables One end of these cables provides a BNC connector to be connected to Agilent modules. The other end depends on the instrument to which connection is being made. Agilent Module to 35900 A/D converters p/n 35900-60750 35900 Pin Agilent...
  • Page 85 Identifying Cables Analog Cables Agilent Module to BNC Connector p/n 8120-1840 Pin BNC Pin Agilent Signal Name module Shield Shield Analog - Center Center Analog + Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog +...

  • Page 86: Remote Cables

    Identifying Cables Remote Cables Remote Cables ERI (Enhanced Remote Interface) • 5188-8029 ERI to general purpose (D-Sub 15 pin male - open end) • 5188-8044 ERI to ERI (D_Sub 15 pin male - male) • 5188-8059 ERI-Extension-Cable 1.2 m (D-Sub15 pin male / female) p/n 5188-8029 Color code Enhanced...
  • Page 87 Identifying Cables Remote Cables • 5188-8045 ERI to APG (Connector D_Subminiature 15 pin (ERI), Connector D_Subminiature 9 pin (APG)) p/n 5188-8045 Pin (ERI) Signal Pin (APG) Active (TTL) Start Request Stop Ready High Power on High Future Shut Down Start Prepare Ground Cable Shielding...
  • Page 88 Ground Cable Shielding One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. MS Flow Modulator User Manual...
  • Page 89 Identifying Cables Remote Cables Agilent Module to Agilent 35900 A/D Converters p/n 5061-3378 Pin 35900 Pin Agilent Signal Name Active module (TTL) 1 - White 1 - White Digital ground 2 - Brown 2 - Brown Prepare run 3 - Gray 3 - Gray Start 4 - Blue...

  • Page 90: Can/Lan Cables

    Identifying Cables CAN/LAN Cables CAN/LAN Cables Both ends of this cable provide a modular plug to be connected to Agilent modules CAN or LAN connectors. CAN Cables Description 5181-1516 CAN cable, Agilent module to module, 0.5 m 5181-1519 CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203...

  • Page 91: Agilent Module To Pc

    Identifying Cables Agilent Module to PC Agilent Module to PC Description RS232-61601 RS-232 cable, 2.5 m Instrument to PC, 9-to-9 pin (female). This cable has special pin-out, and is not compatible with connecting printers and plotters. It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9.

  • Page 92: Usb

    Identifying Cables To connect a USB Flash Drive use a USB OTG cable with Mini-B plug and A socket. Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) MS Flow Modulator User Manual...

  • Page 93: Hardware Information

    Hardware Information Electrical Connections Serial Number Information (ALL) Front and Rear View of the Module Interfaces Overview Interfaces Config Switch Settings of the Infinity Valve Drive This chapter describes the module in more detail on hardware and electronics. Agilent Technologies...

  • Page 94: Electrical Connections

    There are no externally accessible fuses, because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations.

  • Page 95: Front And Rear View Of The Module

    Hardware Information Electrical Connections Front and Rear View of the Module Figure 3 Front view of the flow modulator Figure 4 Rear view of the flow modulator MS Flow Modulator User Manual...

  • Page 96: Interfaces

    Hardware Information Interfaces Interfaces The Agilent InfinityLab LC Series modules provide the following interfaces: Table 5 Agilent InfinityLab LC Series Interfaces Module RS-232 Analo Special (on-board) (A) / ERI (E) Pumps G7104A/C G7110B G7111A/B, G5654A G7112B G7120A G7161A/B Samplers G7129A/B/C G7167B/C, G5667A G7157A Detectors...
  • Page 97 Hardware Information Interfaces Table 5 Agilent InfinityLab LC Series Interfaces Module RS-232 Analo Special (on-board) (A) / ERI (E) Fraction Collectors G7159B G7166A Requires a host module with on-board LAN with minimum FW B.06.40 or C.06.40, or with additional G1369C LAN Card G1364E/F, G5664B THERMOSTAT for G1330B...

  • Page 98: Overview Interfaces

    Hardware Information Interfaces Overview Interfaces The CAN is inter-module communication interface. It is a 2-wire serial bus system supporting high speed data communication and real-time requirement. The modules have either an interface slot for an LAN card (e.g. Agilent G1369B/C LAN Interface) or they have an on-board LAN interface (e.g. detectors G1315C/D DAD and G1365C/D MWD).
  • Page 99 Hardware Information Interfaces The RS-232C is designed as DCE (data communication equipment) with a 9-pin male SUB-D type connector. The pins are defined as: Table 6 RS-232C Connection Table Direction Function Ground Figure 5 RS-232 Cable Analog Signal Output The analog signal output can be distributed to a recording device. For details refer to the description of the module’s main board.
  • Page 100 APG Remote The APG Remote connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. Remote control allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.
  • Page 101 Hardware Information Interfaces Table 7 Remote Signal Distribution Signal Description DGND Digital ground PREPARE (L) Request to prepare for analysis (for example, calibration, detector lamp on). Receiver is any module performing pre-analysis activities. START (L) Request to start run / timetable. Receiver is any module performing run-time controlled activities.

  • Page 102: Config Switch Settings Of The Infinity Valve Drive

    Hardware Information Config Switch Settings of the Infinity Valve Drive Config Switch Settings of the Infinity Valve Drive Configuration Switch Settings Figure 6 Config Switch Figure 7 Dipswitch 1 and 2 Table 8 Configuration Switch Settings Dipswitch 1 Dipswitch 2 Function ON (1) ON (1)
  • Page 103 Hardware Information Config Switch Settings of the Infinity Valve Drive Special Settings Boot-Resident Firmware update procedures may require this mode in case of firmware loading errors (main firmware part). If you use the following switch settings and power the instrument up again, the instrument firmware stays in the resident mode.
  • Page 104 Hardware Information Config Switch Settings of the Infinity Valve Drive MS Flow Modulator User Manual...

  • Page 105: Appendix

    Do Not Modify the Instrument In Case of Damage Solvents Safety Symbols Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Radio Interference Sound Emission Agilent Technologies on Internet This chapter provides addition information on safety, legal and web. Agilent Technologies...

  • Page 106: General Safety Information

    Appendix General Safety Information General Safety Information General Safety Information The following general safety precautions must be observed during all phases of operation, service, and repair of this instrument. Failure to comply with these precautions or with specific warnings elsewhere in this manual violates safety standards of design, manufacture, and intended use of the instrument.

  • Page 107: Before Applying Power

    Verify that the voltage range and frequency of your power distribution matches to the power specification of the individual instrument. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. ➔...

  • Page 108: Ground Solvent Lines

    Electrical shock, fire, explosion ➔ Never use solvent guiding tubes, capillaries, and fittings other than the ones supplied by Agilent Technologies for use in preparative systems. Do Not Operate in an Explosive Atmosphere Presence of flammable gases or fumes WA R N I N G Explosion hazard ➔...

  • Page 109: In Case Of Damage

    Appendix General Safety Information In Case of Damage Damage to the module WA R N I N G Personal injury (for example electrical shock, intoxication) ➔ Instruments that appear damaged or defective should be made inoperative and secured against unintended operation until they can be repaired by qualified service personnel.

  • Page 110: Solvents

    Appendix General Safety Information Solvents Toxic, flammable and hazardous solvents, samples and reagents WA R N I N G The handling of solvents, samples and reagents can hold health and safety risks. ➔ When working with these substances observe appropriate safety procedures (for example by wearing goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet supplied by the vendor, and follow good laboratory practice.

  • Page 111: Safety Symbols

    Appendix General Safety Information Safety Symbols Table 9 Symbols The apparatus is marked with this symbol when the user should refer to the instruction manual in order to protect risk of harm to the operator and to protect the apparatus against damage. Indicates dangerous voltages.
  • Page 112 Appendix General Safety Information Table 9 Symbols Magnetic field Magnets produce a far-reaching, strong magnetic field. They could damage TVs and laptops, computer hard drives, credit and ATM cards, data storage media, mechanical watches, hearing aids and speakers. Keep magnets at least 25 mm away from devices and objects that could be damaged by strong magnetic fields.

  • Page 113: Waste Electrical And Electronic Equipment (Weee) Directive (2002-96-Ec)

    Appendix Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Abstract The Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC), adopted by EU Commission on 13 February 2003, is introducing producer responsibility on all electric and electronic appliances starting with 13 August 2005.

  • Page 114: Radio Interference

    Appendix Radio Interference Radio Interference Cables supplied by Agilent Technologies are screened to provide optimized protection against radio interference. All cables are in compliance with safety or EMC regulations. Test and Measurement If test and measurement equipment is operated with unscreened cables, or...

  • Page 115: Sound Emission

    Appendix Sound Emission Sound Emission Manufacturer’s Declaration This statement is provided to comply with the requirements of the German Sound Emission Directive of 18 January 1991. This product has a sound pressure emission (at the operator position) < 70 dB. •...

  • Page 116: Agilent Technologies On Internet

    Appendix Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com MS Flow Modulator User Manual...
  • Page 117 Index Index error messages leak sensor short initialization of valve failed leak Agilent Lab Advisor software leak sensor open line frequency Agilent Lab Advisor leak sensor short line voltage Agilent leak lost CAN partner on internet lost CAN partner ambient non-operating temperature remote timeout ambient operating temperature shutdown...
  • Page 118 Index physical specifications power consideration unpacking power consumption power cords voltage range radio interference remote waste cables electrical and electronic repairs equipment replacing firmware WEEE directive RS-232C weight cable safety class I safety general information standards symbols serial number information shutdown site requirements power cords...
  • Page 119 Index MS Flow Modulator User Manual...
  • Page 120 In This Book This manual contains technical reference information about the Agilent InfinityLab LC Series 1290 Infinity II MS Flow Modulator (G7170B) The manual describes the following: • Introduction • Site Requirements and Specification • Installation • Using the Module •...

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