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Agilent Technologies 1290 Infinity User Manual

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1290 Infinity TCC User Manual
8
Maintenance
Cleaning the Column Compartment
Changing Column Identification Tags
Adding Heater Devices
Installing the capillaries
Correcting Leaks
Replacing Valve Heads
Preparing the Column Compartment for Transportation
Replacing the Module Firmware
This chapter describes the maintenance tasks for the TCC. If the instrument
needs repair please contact your Agilent service representative.
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Agilent Technologies
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  • Page 1 1290 Infinity TCC User Manual Maintenance Introduction to Maintenance and Repair Cautions and Warnings Overview of Maintenance Cleaning the Column Compartment Changing Column Identification Tags Adding Heater Devices Installing the capillaries Correcting Leaks Replacing Head Parts of Column Switching Valve...

  • Page 2: Introduction To Maintenance And Repair

    There are no serviceable parts inside. N O T E Do not open the module. 1290 Infinity TCC User Manual...

  • Page 3: Cautions And Warnings

    Repair work at the module can lead to personal injuries, e.g. shock hazard, when the cover is opened. ➔ Do not remove the cover of the module. ➔ Only certified persons are authorized to carry out repairs inside the module. 1290 Infinity TCC User Manual...
  • Page 4 For bio-inert applications, always use dedicated bio-inert parts, which can be identified by the bio-inert symbol or other markers described in this manual. ➔ Do not mix bio-inert and non-inert modules or parts in a bio-inert system. 1290 Infinity TCC User Manual...

  • Page 5: Table Of Contents

    If the valve performance shows page 136 indication of leakage or wear “Preparing the Column If the TCC shall be transported Compartment for Transportation” on page 140 “Replacing the Module If required Firmware” on page 143 1290 Infinity TCC User Manual...

  • Page 6: Cleaning The Column Compartment

    Liquid dripping into the electronic compartment of your module can cause shock WA R N I N G hazard and damage the module ➔ Do not use an excessively damp cloth during cleaning. ➔ Drain all solvent lines before opening any connections in the flow path. 1290 Infinity TCC User Manual...

  • Page 7: Changing Column Identification Tags"

    2 The tag needs to be placed differently, depending on whether the column is installed at the left or right heat exchanger, see Figure 26 on page 118 and Figure 27 on page 118. The Agilent logo should always be at front. 1290 Infinity TCC User Manual...
  • Page 8 Column-Identification Tag for Right Heat Exchanger 3 For columns with small diameter, a cable tie wrap should be used to fix the column identification tag to the column. Assure that the tie wrap does not block the front cover. 1290 Infinity TCC User Manual...

  • Page 9: Adding Heater Devices

    Adding Heater Devices Adding Heater Devices The additional heater devices can be arranged in the G1316C in various locations depending on the application needs. Some examples are shown below. Figure 28 Arrangements of Heater and Cooling Devices 1290 Infinity TCC User Manual...
  • Page 10 If the column identification system is required, fix the heater devices in the upper or lower locations or fix them right/left of the current location. The heater devices are mounted on a carrier that can be fitted to the left and/or right heat exchangers. 1290 Infinity TCC User Manual...
  • Page 11 ( Column clip set, 8 colors (5042-9918)) for more convenient installation; mark the nuts of the capillaries attached to the columns as well with color code tags (small rings) to easily follow the flow paths in your system. 1290 Infinity TCC User Manual...
  • Page 12 For the G1316C, additional heat exchanger devices can be installed on the carrier Carrier for heat exchanger (G1316-89200) using 3 screws ( Screw 2.5 mm hex (0515-1052), included to part number for carrier) as shown in figure below. Figure 30 Installing the low dispersion heat exchangers 1290 Infinity TCC User Manual...
  • Page 13 Do not overtighten the fitting at installation. Finger tighten the nut into the port until snug. Then use the wrench and apply about 1/4 of a revolution. (Torque ~ 1.0 – 1.2 Nm) Figure 31 Fitting type depends on column type 1290 Infinity TCC User Manual...

  • Page 14: Installing The Capillaries

    G4232B 2pos/10port valve Preparations Identify the required capillaries in your capillary kits (“Capillary kit PN 5067-4646” on page 158) Use outmost care to avoid any void volumes caused by poor connections. N O T E 1290 Infinity TCC User Manual...
  • Page 15 6 Starting from position one through six (ten, respectively), fasten the fittings on the heat exchanger. 7 Fasten all fittings on attached modules (autosampler, detector, additional pumps). Fit all unused valve ports with a plastic plug. 8 Push the valves into the rear positions. 1290 Infinity TCC User Manual...
  • Page 16 9 Place the capillaries that go to another module or waste into the capillary guides to prevent squeezing them when closing the front cover. 10 Stow any excess lengths of the capillaries. 11 Perform a final leak-check. 1290 Infinity TCC User Manual...
  • Page 17 Flow direction from top to bottom needs switch of connected capillaries at ports 5 and 2. Also column inlet connections needed to be switched with outlet connections. Port 4 to 3 and 6 to 1.) 1290 Infinity TCC User Manual...
  • Page 18 Low dispersion heat exchanger or build-in 3 µL/6 µL heat exchanger and 90 mm length capillary to column Pos.1: Connection between ports 1-6 , 4-5, 2-3 , active column 1 = left (enrichment column) Pos. 2: Connection between ports 1-2, 3-4, 5-6 active column 2 = right (analytical colum) 1290 Infinity TCC User Manual...
  • Page 19 Low dispersion heat exchanger or build-in 3 µL/6 µL heat exchanger and 90 mm length capillary to column Pos.1: Connection between ports 1-6 , 4-5, 2-3 , active column 1 = left (Pre-column) Pos. 2: Connection between Ports 1-2, 3-4, 5-6 active column 2 = right (analytical column) 1290 Infinity TCC User Manual...
  • Page 20 Pos.1: Connection between ports 1-10 , 2-3, 4-5, 6-7, 8-9 active column 1 = left / regemerating column = right Pos. 2: Connection between ports 1-2, 3-4, 5-6, 7-8, 9-10 active column 2 = right / regenerating column = left 1290 Infinity TCC User Manual...

  • Page 21: Correcting Leaks

    132 may vary. 1 Remove the front cover. 2 Use a pipette and tissue to dry the leak sensor area. 3 Observe the capillary connections and the column switching valve for leaks and correct, if required. 1290 Infinity TCC User Manual...
  • Page 22 Maintenance Correcting Leaks 4 Re-install the front cover. Figure 36 Possible Leak Areas 1290 Infinity TCC User Manual...

  • Page 23: Replacing Head Parts Of Column Switching Valve

    Stator face assembly Stator ring (available for service only) Rotor seal Bearing ring (P/N 1534-4045) Spanner nut (P/N 5068-0106, available for service only) When If valve leaks. Tools required Description Wrench, 1/4 inch Hexagonal key, 9/64 inch 1290 Infinity TCC User Manual...
  • Page 24 5 Remove the rotor seal (and isolation seal if damaged or contaminated). 6 Install the new isolation seal (if required). Ensure the metal spring inside the ring faces towards the valve body. 7 Install the new rotor seal. 1290 Infinity TCC User Manual...
  • Page 25 For example do not use 400 bar valve in a TCC or Flex Cube in combination with a 600 bar pump. 12 Perform a Pressure Test to ensure the valve is pressure tight. 1290 Infinity TCC User Manual...

  • Page 26: Replacing Valve Heads

    When using multiple column compartments as part of a method development solution, make sure that the high pressure valve head is connected to the autosampler and the low pressure valve head is connected to the detector. 1290 Infinity TCC User Manual...
  • Page 27 Selection of valve port positions can fail, if the instrument does not know the properties of the installed valve. To have the valve correctly recognized by the Agilent Infinity Valve Drive you must have the N O T E valve drive powered off for at least 10 seconds. 1290 Infinity TCC User Manual...
  • Page 28 Screw the valve head onto the valve drive using the union lobe fits to the groove (see also “Installing the Valve nut (see also “Installing the Valve Heads” on page 50. Heads” on page 50). 1290 Infinity TCC User Manual...
  • Page 29 Maintenance Replacing Valve Heads Install all required capillary connections to the valve Push the valve head until it snaps in and stays in the rear head. position. Switch on the module. 1290 Infinity TCC User Manual...

  • Page 30: Preparing The Column Compartment For Transportation

    Transportation Lock Kit (G1316-67001 ) can be re-ordered. Damage to Internal Parts C A U T I O N Mechanical shocks for example when being transported by car or shipped by post. ➔ Install a lock (Transportation Lock Kit). 1290 Infinity TCC User Manual...
  • Page 31 Preparing the Column Compartment for Transportation Remove the valve head as described in “Replacing Valve Replace the valve head by the transportation valve head. Heads” on page 136. Bring the transportation valve head to the outer position. 1290 Infinity TCC User Manual...
  • Page 32 Lock plate (G1316-03701) to the heat exchangers in the the Transportation valve head (G1316-40002) in the outer positions of the plate. central position of the plate. Put the spring washer (not shown) between the screw and the lock plate. 1290 Infinity TCC User Manual...

  • Page 33: Replacing The Module Firmware

    Initial firmware A.06.10 (main and resident) Compatible with All other modules must have firmware revision A.06.1x or B.06.1x or 1100/1200 series above (main and resident). Otherwise the communication will not work. modules Conversion to / emulation 1290 Infinity TCC User Manual...
  • Page 34 Maintenance Replacing the Module Firmware 1290 Infinity TCC User Manual...
  • Page 35 1290 Infinity TCC User Manual Parts and Materials for Maintenance Plastic Parts Leak Parts Heater and Cooling Devices Valve Options Overview Accessory Kits Standard Accessory Kit Low Dispersion Capillary Kit for G1316C Accessories This chapter provides information on parts for maintenance.
  • Page 36 Parts and Materials for Maintenance Plastic Parts Plastic Parts Item Description G1316-68754 Front cover 5042-9964 Name plate for Agilent 1290 series Figure 38 Plastic Parts 1290 Infinity TCC User Manual...
  • Page 37 Parts and Materials for Maintenance Leak Parts Leak Parts Item Description G1316-67000 Leak tube kit includes following items: Funnel holder G1316C, tubing-flex polyethylene, leak funnel G1316-42303 Capillary guide Figure 39 Leak Parts 1290 Infinity TCC User Manual...
  • Page 38 Heater long-down ( 0.12 mm i.d., 1.6 µL internal volume) (G1316-80003) Part of Capillary kit (5067-4646). For fittings see Table 23 on page 150. Heat Exchanger Long Down 0.075 mm (nom. 1.0 µL) (G1316-80013) Column clip set, 8 colors (5042-9918) 1290 Infinity TCC User Manual...
  • Page 39 Heater and Cooling Devices Table 22 Heater Devices Item Description Carrier for heat exchanger TCC SL Plus (G1316-89200) Fitting holder assembly (G1316-68706) Bio-Inert Solvent Heating Devices ( 9 µL internal volume, 600 bar max pressure) (G5616-60050) 1290 Infinity TCC User Manual...
  • Page 40 Table 23 TCC Heater Fittings Item Description Plastic fittings (0100-1259) Very high pressure removable fitting (5067-4738) Fitting screw long Ferrule back Ferrule front included in kit Fitting screw long (5065-4454) Figure 40 TCC Heater Fittings 1290 Infinity TCC User Manual...
  • Page 41 Parts and Materials for Maintenance Heater and Cooling Devices Figure 41 Heater Devices for G1316C 1290 Infinity TCC User Manual...
  • Page 42 Valve Head Parts (example shows a 5067-4159 valve head) Stator screws Stator head assembly Stator face assembly Stator ring (available for service only) Rotor seal Bearing ring (P/N 1534-4045) Spanner nut (P/N 5068-0106, available for service only) 1290 Infinity TCC User Manual...
  • Page 43 2 Pos/10 Port, 1200 bar (Vespel) 5067-4145 0101-1415 5068-0165 5068-0019 2 Pos/10Port, 600 bar (PEEK) 5067-4146 5068-0076 5068-0077 5068-0089 6 Column Selector, 600 bar (PEEK) 5067-4142 5068-0067 5067-0077 5068-0089 6 Column Selector, 1200 bar (Vespel) 1290 Infinity TCC User Manual...
  • Page 44 5068-0095 5068-0059 n.a. 2 Pos/10Port, 600 bar, bio-inert (PEEK) 5067-4134 5068-0045 5068-0044 5068-0093 5068-0059 n.a. 4 Column Selector, 600 bar, bio-inert (PEEK) 5067-4159 0101-1288 5068-0097 0101-1288 5068-0059 n.a. 12 Pos/13Port, Selector, 200 bar, (PEEK) bio-inert 1290 Infinity TCC User Manual...
  • Page 45 CAN cable, Agilent module to module, 0.5 m G1316-01202 (2x) Column clamp G1316-87300 Capillary, 0.17 x 90 mm 1/16 in male/male G1316-87321 Capillary column-heat exchanger 105 mm lg, 0.17 mm i.d. G1316-87323 Capillary column-heat exchanger 170 mm lg, 0.17 mm i.d. 1290 Infinity TCC User Manual...
  • Page 46 Flexible tubing, 280 mm G1156-22401 Fitting Screw long G1316-68706 Fitting holder assy, includes following items: Fitting fork, fitting clip, screws (pack of 4) G1316-89200 Carrier for heat exchanger G1316-80003 Heater long-down (0.12 mm i.d., 1.6 µL internal volume) 1290 Infinity TCC User Manual...
  • Page 47 RRHT pH Method Development Kit, 2.1 mm i.d. 5190-1433 RRHT Selectivity Method Development Kit, 4.6 mm i.d. 5190-1434 RRHT pH Method Development Kit, 4.6 mm i.d. 5190-1435 Rapid Resolution Selectivity Method Development Kit 5190-1436 Rapid Resolution pH Method Development Kit 1290 Infinity TCC User Manual...
  • Page 48 Heat Exchanger Long-Up, 1.6 µL G1316-80003 Heat Exchanger Long-Down, 1.6 µL G1316-89200 (2x) Carrier for heat exchanger TCC SL Plus G1316-68706 (2x) Fitting holder assembly 5042-9918 Column clip set, eight colors 0100-1259 (4x) Plastic fitting 1290 Infinity TCC User Manual...
  • Page 49 Heat Exchanger Long-Up, 1.6 µL G1316-80003 Heat Exchanger Long-Down, 1.6 µL G1316-89200 (2x) Carrier for heat exchanger TCC SL Plus G1316-68706 (2x) Fitting holder assembly 0100-1259 (4x) Plastic fitting 5042-9918 Column clip set, eight colors 1290 Infinity TCC User Manual...
  • Page 50 Capillary ST 0.17 mm x 120 mm SX/SX valve to valve (bypass) 5067-4721 Capillary ST 0.17 mm x 200 mm S/SX valve to detector 0890-1713 Tube PTFE, 2 m valve to waste 5042-9918 Column clip set, eight colors 1290 Infinity TCC User Manual...
  • Page 51 Chip-LC G1316-80002 (2x) Heat Exchanger Long-Up, 1.6 µL G1316-80003 (2x) Heat Exchanger Long-Down, 1.6 µL G1316-89200 (2x) Carrier for heat exchanger TCC SL Plus G1316-68706 Fitting holder assembly 5042-9918 Column clip set, eight colors 1290 Infinity TCC User Manual...
  • Page 52 You will need this kit to prepare the TCC for transportation. Transportation Lock Kit (G1316-67001 ) Description G1316-03701 Lock plate 2680-0128 Screw M4 0515-0897 Screw M3x8 (pack of 4) Spring Washer G1316-40002 Transportation valve head 1290 Infinity TCC User Manual...
  • Page 53 1290 Infinity TCC User Manual Identifying Cables Cable Overview Analog cables Remote Cables BCD Cables CAN Cable RS-232 Cable Kit Agilent Module to Printer This chapter summarizes information on all cables. Agilent Technologies...
  • Page 54 Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent module to 3394/6 integrators...
  • Page 55 It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity TCC User Manual...
  • Page 56 Pin Agilent Signal Name module Not connected Shield Analog - Center Analog + Agilent Module to BNC Connector p/n 8120-1840 Pin BNC Pin Agilent Signal Name module Shield Shield Analog - Center Center Analog + 1290 Infinity TCC User Manual...
  • Page 57 Identifying Cables Analog cables Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog + 1290 Infinity TCC User Manual...
  • Page 58 Identifying Cables Remote Cables Remote Cables One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. Agilent Module to 3396A Integrators...
  • Page 59 3 - Gray Start 4 - Blue Shut down 5 - Pink connected 6 - Yellow Power on High 7 - Red Ready High 8 - Green Stop 9 - Black Start request 13, 15 connected 1290 Infinity TCC User Manual...
  • Page 60 01046-60201 Wire Color Pin Agilent Signal Name Active module (TTL) White Digital ground Brown Prepare run Gray Start Blue Shut down Pink connected Yellow Power on High Ready High Green Stop Black Start request 1290 Infinity TCC User Manual...
  • Page 61 BCD 4 Black BCD 0 Orange BCD 3 BCD 2 Brown BCD 1 Gray Digital ground Gray Gray/pink BCD 11 Red/blue BCD 10 White/green BCD 9 Brown/green BCD 8 not connected not connected + 5 V 1290 Infinity TCC User Manual...
  • Page 62 Agilent Module to 3396 Integrators p/n 03396-60560 Pin 3396 Pin Agilent Signal Name BCD Digit module BCD 5 BCD 7 BCD 6 BCD 4 BCD0 BCD 3 BCD 2 BCD 1 Digital ground + 5 V 1290 Infinity TCC User Manual...
  • Page 63 CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) 1290 Infinity TCC User Manual...
  • Page 64 It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity TCC User Manual...
  • Page 65 Agilent Module to Printer Agilent Module to Printer Description 5181-1529 Cable Printer Serial & Parallel, is a SUB-D 9 pin female vs. Centronics connector on the other end (NOT FOR FW UPDATE). For use with G1323 Control Module. 1290 Infinity TCC User Manual...
  • Page 66 Identifying Cables Agilent Module to Printer 1290 Infinity TCC User Manual...

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