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Agilent Technologies 1290 Infinity II User Manual

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Agilent InfinityLab LC Series
1290 Infinity II
High Speed Pump
User Manual
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  • Page 1 Agilent InfinityLab LC Series 1290 Infinity II High Speed Pump User Manual Agilent Technologies...
  • Page 2 (June 1987) or any equivalent agency regu- lation or contract clause. Use, duplication or disclosure of Software is subject to Agi- lent Technologies’ standard commercial license terms, and non-DOD Departments and Agencies of the U.S. Government will 1290 Infinity II High Speed Pump User Manual...
  • Page 3 In This Guide… In This Guide… This manual covers the Agilent 1290 Infinity II High Speed Pump (G7120A). 1 Introduction This chapter gives an introduction to the pump and an instrument overview. 2 Site Requirements and Specifications This chapter provides information on environmental requirements, physical and performance specifications.
  • Page 4 This chapter describes the pump in more detail on hardware and electronics. 11 LAN Configuration This chapter provides information on connecting the module to the Agilent ChemStation PC. 12 Appendix This chapter provides addition information on safety, legal and web. 1290 Infinity II High Speed Pump User Manual...

  • Page 5: Table Of Contents

    Status Indicators Best Practices Purging the Pump Solvent Information Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Algae Growth in HPLC Systems Setting up the Pump with the Instrument Control Interface Agilent Local Control Modules...
  • Page 6 Install the Pump Head Assembly Replace the Outlet Valve Replace the Purge Valve Head Replace Parts of the High Pressure Filter Assembly Replace the Module Firmware Prepare the Pump Module for Transport 1290 Infinity II High Speed Pump User Manual...
  • Page 7 11 LAN Configuration What You Have to Do First TCP/IP parameter configuration Configuration Switch Initialization mode selection Dynamic Host Configuration Protocol (DHCP) Link configuration selection Manual Configuration PC and User Interface Software Setup Setup 1290 Infinity II High Speed Pump User Manual...
  • Page 8 Contents 12 Appendix General Safety Information Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Radio Interference Sound Emission Agilent Technologies on Internet 1290 Infinity II High Speed Pump User Manual...

  • Page 9: Introduction

    1290 Infinity II High Speed Pump User Manual Introduction Product Description Pump Principle Leak and Waste Handling Leak Sensor Waste Concept This chapter gives an introduction to the pump and an instrument overview. Agilent Technologies...

  • Page 10: Product Description

    A low-delay-volume mixer allows you to run fast gradients for narrow-bore applications for high laboratory efficiency. The new 1290 Infinity II LC power range has a high instrument efficiency, allowing you to run any HPLC and UHPLC method. The full ISET range enables you to transfer existing methods from different instruments, including current Agilent systems as well as instruments from other manufacturers.

  • Page 11: Pump Principle

    The pump automatically compensates for pressure- and flow instabilities caused by the complex relationship between solvent compressibility and system pressure. The only user interaction is selecting the appropriate solvent or solvent mixture per channel from a drop-down list. 1290 Infinity II High Speed Pump User Manual...
  • Page 12 Introduction Pump Principle Figure 2 The hydraulic path 1290 Infinity II High Speed Pump User Manual...

  • Page 13: Leak And Waste Handling

    • from the Multisampler needle wash port • from the Sample Cooler or Sample Thermostat (condensate) • from the pump's Seal Wash Sensor (if applicable) • from the pump's Purge Valve or Multipurpose Valve 1290 Infinity II High Speed Pump User Manual...
  • Page 14 Introduction Leak and Waste Handling Figure 3 Infinity II Leak Waste Concept (Flex Bench installation) 1290 Infinity II High Speed Pump User Manual...
  • Page 15 Introduction Leak and Waste Handling Figure 4 Infinity II Single Stack Leak Waste Concept (bench installation) 1290 Infinity II High Speed Pump User Manual...

  • Page 16: Leak Sensor

    C AU T I O N The solvent DMF (dimethyl formamide) leads to corrosion of the leak sensor. The material of the leak sensor, PVDF (polyvinylidene fluoride), is incompatible with DMF. ➔ Do not use DMF. 1290 Infinity II High Speed Pump User Manual...

  • Page 17: Waste Concept

    1 Agilent recommends using the 6 L waste can with 1 Stay Safe cap GL45 with 4 ports (5043-1221) for optimal and safe waste disposal. If you decide to use your own waste solution, make sure that the tubes don't immerse in the liquid. 1290 Infinity II High Speed Pump User Manual...
  • Page 18 Introduction Leak and Waste Handling 1290 Infinity II High Speed Pump User Manual...

  • Page 19: Site Requirements And Specifications

    1290 Infinity II High Speed Pump User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter provides information on environmental requirements, physical and performance specifications. Agilent Technologies...

  • Page 20: Site Requirements

    ➔ Make sure the power connector of the instrument can be easily reached and unplugged. ➔ Provide sufficient space behind the power socket of the instrument to unplug the cable. 1290 Infinity II High Speed Pump User Manual...

  • Page 21: Site Requirements

    Never use the power cords that Agilent Technologies supplies with this instrument for any other equipment. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. Absence of ground connection WA R N I N G The absence of ground connection can lead to electric shock or short circuit.
  • Page 22 ➔ If your module was shipped in cold weather, leave it in its box and allow it to warm slowly to room temperature to avoid condensation. 1290 Infinity II High Speed Pump User Manual...

  • Page 23: Physical Specifications

    Up to 4600 m (15092 ft) For storing the module Safety standards: Installation category II, Pollution degree 2 For indoor use only. IEC, EN, CSA, UL ISM Classification ISM Group 1 Class B According to CISPR 11 1290 Infinity II High Speed Pump User Manual...

  • Page 24: Performance Specifications

    Site Requirements and Specifications Performance Specifications Performance Specifications Table 2 Agilent 1290 Infinity II High Speed Pump (G7120A) Performance Specifications Feature Specification Hydraulic system Two dual pistons in series, pumps with proprietary servo-controlled variable stroke design and smooth motion control.
  • Page 25 Site Requirements and Specifications Performance Specifications Table 2 Agilent 1290 Infinity II High Speed Pump (G7120A) Performance Specifications Feature Specification Integrated degassing Included unit Number of channels: 2 Internal volume per channel: 1.5 mL Materials in contact with solvent: TFE/PDD Copolymer, FEP, PEEK, PPS.
  • Page 26 Site Requirements and Specifications Performance Specifications 1290 Infinity II High Speed Pump User Manual...

  • Page 27: Using The Pump

    Setting up the Pump with the Instrument Control Interface Overview Instrument Configuration The Pump User Interface (Dashboard Panel) Control Settings Method Parameter Settings Agilent Local Control Modules This chapter explains the operational parameters of the Agilent 1290 Infinity II High Speed Pump. Agilent Technologies...

  • Page 28: Magnets

    Using the Pump Magnets Magnets This stack exemplarily shows the magnets' positions in the modules. 1290 Infinity II High Speed Pump User Manual...

  • Page 29: Turn On/Off

    Using the Pump Turn on/off Turn on/off Power switch: On Turn instrument On/Off with the control software. Power switch: Off 1290 Infinity II High Speed Pump User Manual...
  • Page 30 Using the Pump Turn on/off 1290 Infinity II High Speed Pump User Manual...

  • Page 31: Status Indicators

    5. Resident mode (blinking) - for example during update of main firmware. 6. Bootloader mode (fast blinking). Try to re-boot the module or try a cold-start. Then try a firmware update. 1290 Infinity II High Speed Pump User Manual...

  • Page 32: Best Practices

    • Purge each channel with fresh solvent at 2.5 – 3 mL/min for 5 min. • Equilibrate your system with composition of your application for 15 min. Use conditioning for 1290 Infinity II Pumps and G7104C. Weekly tasks • Change seal wash solvent (10 % / 90 % isopropanol/water) and bottle.

  • Page 33: Power Up / Shut-Down The Pump

    • Equilibrate your system with composition of your application for 15 min. Use conditioning for 1290 Infinity II Pumps and G7104C. Long-term shut-down of the system • Flush system with water to remove buffer.

  • Page 34: How To Deal With Solvents

    • Label bottles correctly with bottle content, and filling date / expiry date. • Use solvent inlet filters. • Reduce risk of algae growth: use brown bottles for aqueous solvents, avoid direct sunlight. 1290 Infinity II High Speed Pump User Manual...

  • Page 35: Purging The Pump

    The pump should never be used for priming/purging empty tubings (never let the pump N O T E run dry). Use a syringe to draw enough solvent for completely filling the tubings to the pump inlet before continuing to prime with the pump. 1290 Infinity II High Speed Pump User Manual...
  • Page 36 6 Observe the pressure fluctuations. The system is air free as soon as the pressure is stable. 7 Change solvents and column according to the analytical conditions and purge the system to change solvents. 1290 Infinity II High Speed Pump User Manual...

  • Page 37: Solvent Information

    • Avoid or minimize the use of solvents that may corrode parts in the flow path. Consider specifications for the pH range given for different materials like flow cells, valve materials etc. and recommendations in subsequent sections. 1290 Infinity II High Speed Pump User Manual...
  • Page 38 UHMW-PE, SST Pressure sensor Automatic purge valve Polyimide, SST, DLC Ultra clean tubings are available for the use with high-end MS detectors. They are also compatible to THF. Jet Weaver, Heat Exchanger 1290 Infinity II High Speed Pump User Manual...
  • Page 39 THF, DMSO, strong acids (nitric acid > 10 %, sulphuric acid > 10 %, sulfonic acids, trichloroacetic acid), halogenes or aequous halogene solutions, phenol and derivatives (cresols, salicylic acid etc.). 1290 Infinity II High Speed Pump User Manual...
  • Page 40 Polyethylene (PE) Agilent uses UHMW (ultra-high molecular weight)-PE/PTFE blends for yellow piston and wash seals, which are used in 1290 Infinity pumps, 1290 Infinity II pumps, the G7104C and for normal phase applications in 1260 Infinity pumps. Polyethylene has a good stability for most common inorganic solvents including acids and bases in a pH range of 1 to 12.5.
  • Page 41 (about pH 0.1) at room temperature is about 13 μm/year. At room temperature, titanium is resistant to concentrations of about 5 % sulfuric acid (about pH 0.3). Addition of nitric acid to hydrochloric or sulfuric acids 1290 Infinity II High Speed Pump User Manual...
  • Page 42 Zirconium Oxide is inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. Platinum/Iridium Platinum/Iridium is inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. 1290 Infinity II High Speed Pump User Manual...
  • Page 43 Sapphire, Ruby and Al -based ceramics Sapphire, ruby and ceramics based on aluminum oxide Al are inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. 1290 Infinity II High Speed Pump User Manual...

  • Page 44: Solvent Recommendation For Agilent 1290 Infinity And 1290 Infinity Ii And 1260 Infinity Ii Flexible Pumps

    Using the Pump Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps While the Agilent 1290 Infinity, 1290 Infinity II, and 1260 Infinity II Flexible Pumps guarantee a high performance with a wide variety of solvents, other solvents may cause harm to the pump or to the (U)HPLC system.

  • Page 45: Normal Phase Applications

    Using the Pump Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Normal Phase Applications Valves for Normal Phase Applications Current passive inlet valves and outlet ball valves used with Agilent Infinity and Infinity II pumps do not work well while running nonpolar solvents for normal phase applications (for example, hexane and heptane).

  • Page 46: Solvent Handling

    Using the Pump Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Table 4 Recommended valves for normal phase applications Binary or High Speed Pumps Quaternary or Flexible Pumps Inlet valves 1290 Infinity Inlet Valve Type N...
  • Page 47 Using the Pump Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Handling of Buffers The following recommendations should be observed when using buffer solutions: • Buffers and aqueous solutions are possible sources of algae contamination, for avoiding related problems, please read “Algae Growth in HPLC...
  • Page 48 Using the Pump Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps Handling of Acetonitrile Acetonitrile is a solvent that is frequently used in reversed-phase chromatography. Despite of its common use, it can be a source of issues if not handled correctly.

  • Page 49: Algae Growth In Hplc Systems

    • Use the amber solvent bottle ( Solvent bottle, amber, 1000 mL (9301-6526)) supplied with the instrument for your aqueous mobile phase. • If possible add a few mg/L sodium azide or a few percent organic solvent to the aqueous mobile phase. 1290 Infinity II High Speed Pump User Manual...

  • Page 50: Setting Up The Pump With The Instrument Control Interface

    • Communication • Options Communication: The parameters in this dialog box are detected automatically during autoconfiguration. • Device name, • Type ID, • Serial number, • Firmware revision, • Button Connection settings 1290 Infinity II High Speed Pump User Manual...
  • Page 51 See “Importing Solvent Calibration Tables” on page 70. Please refer to the online help of your user interface for more detailed information. 1290 Infinity II High Speed Pump User Manual...

  • Page 52: The Pump User Interface (Dashboard Panel)

    The pressure setpoints. The red line shows the current maximum pressure limit; the green area shows the current pressure (also shown as text). The current solvent flow rate (in mL/min) is displayed above the pressure display. 1290 Infinity II High Speed Pump User Manual...
  • Page 53 Prepare Pump Allows you to control the Purge, Condition or the Prime function. Seal Wash Purge Allows you to refill the Seal Wash lines once the Seal Wash solvent has been changed 1290 Infinity II High Speed Pump User Manual...
  • Page 54 Conditioning may be necessary if the pump may contain air, for example after running out of solvent, after a long period of standby or after service or repair. 1290 Infinity II High Speed Pump User Manual...

  • Page 55: Control Settings

    Method Parameter Settings The Binary Pump method setup parameters are in eight sections: • Flow • Solvents A and B • Stoptime • Posttime • Pressure Limits • Timetable • Advanced • External Contacts 1290 Infinity II High Speed Pump User Manual...
  • Page 56 5 mL/min , the damage by pumping air. maximum pressure ramps down to 800 bar (11600 psi). Min: any value between 0 and the upper pressure limit setting. Timetable “Timetable Settings” on page 59 1290 Infinity II High Speed Pump User Manual...
  • Page 57 The External Contacts section enables you to set up the switching of the external contacts. N O T E The External Contacts section is present only when a BCD/external contacts board is installed. 1290 Infinity II High Speed Pump User Manual...
  • Page 58 You can set a limit on the rate of change of the solvent flow to protect your Gradient 1000.000 mL/min/min analytical column. You can set individual values for Flow ramp up and Flow in steps of ramp down. 0.001 mL/min/min Default value: 100.000 mL/min/min 1290 Infinity II High Speed Pump User Manual...
  • Page 59 • Change Solvent Composition - You can only use solvents, which have been enabled in the solvents section. • Function centric view - This checkbox allows you displaying parameter changes instead of a time table. 1290 Infinity II High Speed Pump User Manual...

  • Page 60: Agilent Local Control Modules

    • Preconfigured tablet with all required software already installed (included in the full package). • Centerpiece of the solution is a USB dongle that activates the complete intelligence of the InfinityLab LC Companion on the instrument stack. 1290 Infinity II High Speed Pump User Manual...
  • Page 61 • GLP – System logbook and module log-books record errors, unusual events and maintenance activities for GLP traceability. 1290 Infinity II High Speed Pump User Manual...
  • Page 62 Using the Pump Agilent Local Control Modules 1290 Infinity II High Speed Pump User Manual...

  • Page 63: Optimizing Performance

    1290 Infinity II High Speed Pump User Manual Optimizing Performance Delay Volume and Extra-Column Volume Delay Volume How to Configure the Optimum Delay Volume How to Achieve Higher Resolution Using Solvent Calibration Tables This chapter gives hints on how to optimize the performance or use additional devices.

  • Page 64: Delay Volume And Extra-Column Volume

    The delay volume in a system includes the volume in the pump from the point of mixing, connections between pump and autosampler, volume of the flow path through the autosampler and connections between autosampler and column. 1290 Infinity II High Speed Pump User Manual...

  • Page 65: How To Configure The Optimum Delay Volume

    127. The delay volume is increased by approximately 31 μL and the baseline performance with additives like TFA will be improved. The configuration of the Jet Weaver is logged automatically by an attached RFID tag. 1290 Infinity II High Speed Pump User Manual...
  • Page 66 The 380 μL Jet Weaver strongly improves mixing and therefore reduces baseline noise and improves sensitivity in detection. Patented Agilent microfluidic technology offers high mixing performance at a low internal volume of 380 μL. 1290 Infinity II High Speed Pump User Manual...

  • Page 67: How To Achieve Higher Resolution

    The resolution equation shows that the next most significant term is the plate count or efficiency, N, and this can be optimized in a number of ways. N is inversely proportional to the particle size and directly proportional to the 1290 Infinity II High Speed Pump User Manual...
  • Page 68 • F = flow (ml/min), • V = column delay volume, • Δ%B = change in fraction of solvent B during the gradient, • S = constant (ca. 4-5 for small molecules). 1290 Infinity II High Speed Pump User Manual...
  • Page 69 40 °C) can generate higher peak capacity than a longer STM column by virtue of running it faster. (Refer to Petersson et al., J.Sep.Sci, 31, 2346-2357, 2008, Maximizing peak capacity and separation speed in liquid chromatography). 1290 Infinity II High Speed Pump User Manual...

  • Page 70: Using Solvent Calibration Tables

    5 Navigate to the location of the solvent calibration table and click Open. The new solvent will now appear in the Solvent Type Catalogs. The imported solvent is now available for selection as a solvent type in the pump's method parameters. 1290 Infinity II High Speed Pump User Manual...

  • Page 71: Troubleshooting And Diagnostics

    1290 Infinity II High Speed Pump User Manual Troubleshooting and Diagnostics User Interfaces Agilent Lab Advisor Software Pump Leak Rate Test Troubleshooting the Pump Leak Rate Test System Pressure Test Overview about the troubleshooting and diagnostic features. Agilent Technologies...

  • Page 72: User Interfaces

    Advisor Software” on page 73. • The Agilent OpenLAB ChemStation C.01.03 and above do not include any maintenance/test functions. • Screenshots used within these procedures are based on the Agilent Lab Advisor Software. 1290 Infinity II High Speed Pump User Manual...

  • Page 73: Agilent Lab Advisor Software

    The tests and diagnostic features that are provided by the Agilent Lab Advisor software may differ from the descriptions in this manual. For details, refer to the Agilent Lab Advisor software help files. 1290 Infinity II High Speed Pump User Manual...

  • Page 74: Pump Leak Rate Test

    • The allowed leak limit for the primary piston is ≤30 μL/min A report can be displayed, saved or printed by opening it with the Print Result button at the lower right of the screen. 1290 Infinity II High Speed Pump User Manual...
  • Page 75 If the test does not pass, check the system for leaks or call a local Agilent representative. Figure 6 on page 75 and Figure 7 on page 76 show a typical test run. Figure 6 Static (secondary) Leak Test 1290 Infinity II High Speed Pump User Manual...
  • Page 76 Troubleshooting and Diagnostics Pump Leak Rate Test Figure 7 Dynamic (primary) Leak Test 1290 Infinity II High Speed Pump User Manual...

  • Page 77: Troubleshooting The Pump Leak Rate Test

    • Leak in Inlet Valve • Check for moving air bubbles in tubing directly to the Inlet Valve • Purge the lines with water to remove dirt • Knock at the valve, clean or replace it 1290 Infinity II High Speed Pump User Manual...
  • Page 78 Remove the SW tubes from the support ring and check for leaks • Replace the piston seals and clean the pistons • Ensure that seals are lubricated when pushed in • Use abrasive mesh >5000 grit 1290 Infinity II High Speed Pump User Manual...

  • Page 79: System Pressure Test

    If the test does not pass, check the system for leaks or call a local Agilent representative. Figure 8 on page 80 shows a typical test run. 1290 Infinity II High Speed Pump User Manual...
  • Page 80 Troubleshooting and Diagnostics System Pressure Test Figure 8 System Pressure Test 1290 Infinity II High Speed Pump User Manual...

  • Page 81: Error Information

    1290 Infinity II High Speed Pump User Manual Error Information What Are Error Messages General Error Messages Timeout Shutdown Remote Timeout Lost CAN Partner Leak Sensor Short Leak Sensor Open Compensation Sensor Open Compensation Sensor Short Fan Failed Leak Open Cover...
  • Page 82 Seal wash pump was missing when tried to turn on Invalid degasser pressure signal This chapter describes the meaning of error messages, and provides information on probable causes and suggested actions how to recover from error conditions. 1290 Infinity II High Speed Pump User Manual...

  • Page 83: What Are Error Messages

    In all cases, error propagation is done via the CAN bus or via an APG/ERI remote cable (see documentation for the APG/ERI interface). 1290 Infinity II High Speed Pump User Manual...

  • Page 84: General Error Messages

    Check the logbook for the occurrence and A not-ready condition was present during a source of a not-ready condition. Restart the sequence or multiple-injection run for a analysis where required. period longer than the timeout threshold. 1290 Infinity II High Speed Pump User Manual...

  • Page 85: Shutdown

    Check the vacuum degasser for an error The degasser failed to generate sufficient condition. Refer to the Service Manual for the vacuum for solvent degassing. degasser or the pump that has the degasser built-in. 1290 Infinity II High Speed Pump User Manual...

  • Page 86: Remote Timeout

    Exchange the remote cable. Defective remote cable. Check the instrument for defects (refer to the Defective components in the instrument instrument’s documentation). showing the not-ready condition. 1290 Infinity II High Speed Pump User Manual...

  • Page 87: Lost Can Partner

    Exchange the CAN cable. Defective CAN cable. Switch off the system. Restart the system, and Defective main board in another module. determine which module or modules are not recognized by the system. 1290 Infinity II High Speed Pump User Manual...

  • Page 88: Leak Sensor Short

    Please contact your Agilent service Leak sensor incorrectly routed, being representative. pinched by a metal component. Please contact your Agilent service Power switch assembly defective representative. Please contact your Agilent service Cable or contact problem. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 89: Leak Sensor Open

    Please contact your Agilent service Defective leak sensor. representative. Please contact your Agilent service Leak sensor incorrectly routed, being representative. pinched by a metal component. Please contact your Agilent service Power switch assembly defective representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 90: Compensation Sensor Open

    Probable cause Suggested actions Please contact your Agilent service Defective power switch assembly representative. Please contact your Agilent service Loose connection between the power representative. switch board and the main board 1290 Infinity II High Speed Pump User Manual...

  • Page 91: Fan Failed

    Probable cause Suggested actions Please contact your Agilent service Fan cable disconnected. representative. Please contact your Agilent service Defective fan. representative. Please contact your Agilent service Defective main board. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 92: Leak

    Loose or leaking purge valve, inlet valve, or If there are still signs of a leak, exchange the outlet valve. appropriate seal (purge valve, inlet valve, outlet valve). Exchange the pump seals. Defective pump seals. 1290 Infinity II High Speed Pump User Manual...

  • Page 93: Open Cover

    Probable cause Suggested actions Please contact your Agilent service The top foam was removed during representative. operation. Please contact your Agilent service Foam not activating the sensor. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 94: Pump Error Messages

    • Parameter: None Probable cause Suggested actions Check for leaks. Leak Check bottle filling. Bottle empty Check solvent. Wrong solvent (viscosity) Check flow rate and lower pressure limit. Inappropriate setting Replace column. Column degradation 1290 Infinity II High Speed Pump User Manual...

  • Page 95: Target Pressure Not Reached For Binary Pump Degasser

    Please contact your Agilent service Leak in degasser chamber or degasser representative. tubing. Please contact your Agilent service Defect vacuum pump. representative. Block unused degasser channels. Degasser chamber empty or connected to air. 1290 Infinity II High Speed Pump User Manual...

  • Page 96: Solvent Counter Exceeded Limit

    • Parameter: None Probable cause Suggested actions Empty waste container. The waste container is full. • Reset waste counter. Inappropriate setting for waste counter. • Adjust waste counter limit. 1290 Infinity II High Speed Pump User Manual...

  • Page 97: Flow Rate Limit Exceeded

    The binary pump has been shut down by the control software or control module during an analysis. • Parameter: 0 for off, 1 for standby. Probable cause Suggested actions Restart pump. Pump has been shut down. 1290 Infinity II High Speed Pump User Manual...

  • Page 98: Reading The Pump Encoder Tag Failed

    • Parameter: 1 – 4 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Defect connection between encoder and representative. main board. Please contact your Agilent service Defect tag Defect connection between tag representative. and encoder. 1290 Infinity II High Speed Pump User Manual...

  • Page 99: Pump Drive Blocked Or Encoder Failed

    Please contact your Agilent service Wrong/missing connection of pump drive representative. to main board. Drive Encoder failed Error ID: 22408 Drive encoder failed during pump drive calibration. Probable cause Suggested actions Contact Agilent support. Internal error. 1290 Infinity II High Speed Pump User Manual...

  • Page 100: Drive Current Too High

    Drive is blocked mechanically, fails during initialization. • Parameter: 1 – 4 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Blockage of pump drive Drive motor defect. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 101: Overcurrent Of Pump Drive

    Probable cause Suggested actions Replace the solvent selection valve. Valve defect. Deliver underrun Error ID: 22413 Internal error. • Parameter: None Probable cause Suggested actions Please contact your Agilent service Internal error. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 102: Defect Connection Between Main Board And Pump Drive Encoder

    Pump drive encoder defect Error ID: 22415 Defect pump drive encoder. • Parameter: 1 – 4 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Defect encoder. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 103: Purge Valve Failed

    Check cable connection. Reading of purge valve tag failed. Replace purge valve head. Purge valve head tag defect or empty. Please contact your Agilent service Purge valve tag reader is defect. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 104: Pump Drive Encoder Rollover

    Error ID: 22426 Insufficient power of drive encoder LED. • Parameter: 1 – 4 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 105: Drive Encoder Error

    Writing the purge valve tag failed. • Parameter: None Probable cause Suggested actions Replace purge valve head. Purge valve head tag defect. Please contact your Agilent service Purge valve tag reader is defect. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 106: Current Of Primary Pump Drive Too High

    Blockage of flow path between secondary pump head and pressure sensor, e.g. of the • Please contact your Agilent service heat exchanger. representative. Please contact your Agilent service Secondary pump drive is defect. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 107: Unknown Purge Valve Type

    The pump drive failed during calibration. • Parameter: 1 – 4 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive motor defect or mechanically representative. blocked. 1290 Infinity II High Speed Pump User Manual...

  • Page 108: Pump Drive Stroke Blocked

    • Parameter: 1 – 4 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Wiper shifted representative. Please contact your Agilent service Pump drive spindle is defect. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 109: Pressure Sensor Calibration Wrong Or Missing

    Suggested actions Check cable connection. Defect cable connection to seal wash pump. Please contact your Agilent service Defect seal wash pump motor. representative. Please contact your Agilent service Defective main board. representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 110: Invalid Degasser Pressure Signal

    Error ID: 29253 The degasser pressure signal is invalid. Probable cause Suggested actions Please contact your Agilent service Degasser might be disconnected representative. Please contact your Agilent service Pressure sensor might be defective representative. 1290 Infinity II High Speed Pump User Manual...

  • Page 111: Maintenance

    1290 Infinity II High Speed Pump User Manual Maintenance Introduction to Maintenance Warnings and Cautions Overview of Maintenance Cleaning the Module Install Fittings and Capillaries Remove and Install Doors Replace the Shutoff Valve Panel Replace the Pressure Sensor Replace the Solvent Selection Valve (SSV)

  • Page 112: Introduction To Maintenance

    Figure 9 on page 112 shows the main user accessible assemblies of the Agilent 1290 Infinity II High Speed Pump. These parts can be accessed from the front (simple repairs) and don’t require to remove the pump from the system stack.
  • Page 113 A “typical” application can be characterized as follows: • pressure range 100 – 800 bar, • flow rates 0.5 – 3.5 mL/min, • typical solvents used in reversed phase LC. 1290 Infinity II High Speed Pump User Manual...

  • Page 114: Warnings And Cautions

    Agilent product user guides, or use of the products in violation of applicable laws, rules or regulations. ➔ Use your Agilent products only in the manner described in the Agilent product user guides. 1290 Infinity II High Speed Pump User Manual...
  • Page 115 ➔ If you connect external equipment to the instrument, make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment. 1290 Infinity II High Speed Pump User Manual...

  • Page 116: Overview Of Maintenance

    Maintenance Overview of Maintenance Overview of Maintenance The following pages describe maintenance (simple repairs) of the module that can be carried out without opening the main cover. 1290 Infinity II High Speed Pump User Manual...

  • Page 117: Cleaning The Module

    WA R N I N G hazard and damage the module ➔ Do not use an excessively damp cloth during cleaning. ➔ Drain all solvent lines before opening any connections in the flow path. 1290 Infinity II High Speed Pump User Manual...

  • Page 118: Install Fittings And Capillaries

    The lifetime of a fitting depends on how firmly it has been tightened; firm tightening N O T E reduces the lifetime. If fitting has been overtightened, replace it. 1 Install fittings and capillaries. 2 Tighten fittings and capillaries. 1290 Infinity II High Speed Pump User Manual...

  • Page 119: Remove And Install Doors

    The figures shown in this procedure exemplarily show the Infinity II Multisampler module. N O T E The principle of how to remove and/or install doors works in the same way for all Infinity II modules. 1290 Infinity II High Speed Pump User Manual...
  • Page 120 Press the release buttons and pull the front door out. For the Installation of the front door. Insert the hinges into their guides and move the door in until the release buttons click into their final position. 1290 Infinity II High Speed Pump User Manual...

  • Page 121: Replace The Shutoff Valve Panel

    Unscrew tubing connections between shutoff valves, If a single valve shall be replaced, it can be pulled to the solvent bottles and the solvent selection valve. front for removing it from its mounting. 1290 Infinity II High Speed Pump User Manual...
  • Page 122 Maintenance Replace the Shutoff Valve Panel Remove the shutoff valve panel by pulling it downwards. After replacing the panel or after completion of other maintenance, re-install the panel and all flow connections. 1290 Infinity II High Speed Pump User Manual...

  • Page 123: Replace The Pressure Sensor

    In case the cable to the sensor shall be replaced as well, please contact your Agilent service representative. Remove capillary connections between the pressure Remove the screws that fix the pressure sensor to the sensor and purge valve. chassis. 1290 Infinity II High Speed Pump User Manual...
  • Page 124 Fix the pressure sensor to the instrument chassis. Connect the capillaries from the valve to the pressure sensor: connect port 3 to the pressure sensor inlet and port 2 to the outlet. 1290 Infinity II High Speed Pump User Manual...

  • Page 125: Replace The Solvent Selection Valve (Ssv)

    SSV and the degassing unit inlets. Push down the SSV panel for removing it. Remove the connector by pushing up the small clip at the bottom of the connector. 1290 Infinity II High Speed Pump User Manual...
  • Page 126 Replace the Solvent Selection Valve (SSV) Install a new SSV by inserting the connector and clipping the SSV panel to the module top panel. Then re-install all tubing connections, open shut-off valve and purge valve. 1290 Infinity II High Speed Pump User Manual...

  • Page 127: Change Configuration Or Replace The Jet Weaver

    ¼ inch wrench 3 mm hex key Parts required Description G4220-60027 Jet Weaver 35 µL/100 µL G4220-60012 Jet Weaver 380 µL (OPTIONAL) G4220-87000 Capillary ST 0.17 mm x 300 mm Valve to Jet Weaver 1290 Infinity II High Speed Pump User Manual...
  • Page 128 (G4220-60012)) is recommended for applications which are challenging with respect to mixing noise (e.g. TFA applications) and has just one side. Remove the Jet Weaver. Install new Jet Weaver or flip the Jet Weaver for backside. 1290 Infinity II High Speed Pump User Manual...
  • Page 129 The inlet at the left side of the Jet Weaver is connected to the central port of the pump valve by a capillary (length 300 mm, 0.17 mm i.d.). The outlet at the right side is connected to the autosampler. 1290 Infinity II High Speed Pump User Manual...

  • Page 130: Replace The Seal Wash Pump

    Insert the pump clips to the holes in the pump housing. Fix the seal wash tubings to the peristaltic pump inlet (1) and from the peristaltic pump outlet to the primary pump head inlet (2). 1290 Infinity II High Speed Pump User Manual...

  • Page 131: Replace The Inlet Valve

    For best performance and life time and for avoiding leaks, use a torque wrench set to N O T E approx. 10 Nm for fixing the inlet valve. Close the shut off valves to avoid solvent leaks. Unscrew the tubing at the inlet valve. 1290 Infinity II High Speed Pump User Manual...
  • Page 132 Install inlet valve and tighten it at approx. 10 Nm with a remove it. torque wrench (14 mm). Attach the inlet tubing at the inlet valve. Open the shut off valves and purge the system to remove air. 1290 Infinity II High Speed Pump User Manual...

  • Page 133: Release A Stuck Inlet Valve

    Remove the capillary connection from the outlet of the Unscrew the tubing at the inlet valve. secondary pump head. Attach a Luer lock syringe with adapter to the tubing and Reconnect tubing to inlet valve. fill it with solvent. 1290 Infinity II High Speed Pump User Manual...
  • Page 134 High Pressure Filter Assembly. Detach the syringe and reconnect the tubing into the Reinstall the capillary connection to the High Pressure degassing unit. Filter Assembly. Purge the system to remove air. 1290 Infinity II High Speed Pump User Manual...

  • Page 135: Remove The Pump Head Assembly

    In Lab Advisor go to Service & Diagnostics > Open the doors. Remove/Install Pump Head and follow instructions given on the screen. Close all shut-off valves. Remove the seal wash tubes. 1290 Infinity II High Speed Pump User Manual...
  • Page 136 Loosen the high pressure filter. Keep the filter installed Open the four screws holding the pump heads. to the pump head assembly. N O T E Open the screws step by step, not screw by screw. 1290 Infinity II High Speed Pump User Manual...
  • Page 137 Maintenance Remove the Pump Head Assembly Remove the complete pump head assembly by holding Remove the seal wash tubing interconnecting the two both heads and pulling it to the front. pump heads. 1290 Infinity II High Speed Pump User Manual...

  • Page 138: Pump Head Maintenance (Tool Free)

    Pump Head Maintenance (Tool Free) Pump Head Maintenance (Tool Free) Infinity II Flexible Pumps (G7104A/C) and 1290 Infinity II High Speed Pumps (G7120A) are equipped with Long Life Pump Heads. Long Life Pump Heads offer a significantly increased lifetime of pistons and seals compared to other pump heads.

  • Page 139: Disassemble Longlife Pump Heads

    N O T E A gold seal between outlet valve and heat exchanger capillary is used for a tight connection. 1290 Infinity II High Speed Pump User Manual...
  • Page 140 Binary/High Speed Pumps only: Remove the high primary pump head. pressure filter from the secondary pump head. N O T E Clean the valves by sonication, if appropriate. A good cleaning solution is 50 % isopropanol in water. 1290 Infinity II High Speed Pump User Manual...
  • Page 141 Remove the piston by pressing it out of the seal holder from the pump chambers. with a finger. Remove the seal holder from the spring housing. Screw the pin of the seal handling device into the piston seal. 1290 Infinity II High Speed Pump User Manual...
  • Page 142 The side with the backup ring has a bigger diameter and a sharp edge to hold the piston seal. The other side has no sharp edge and holds the smaller wash seal. 1290 Infinity II High Speed Pump User Manual...
  • Page 143 Maintenance Pump Head Maintenance (Tool Free) Repeat for the other seal holder. Clean the piston with abrasive paper. Rinse pump heads and pistons with isopropanol. 1290 Infinity II High Speed Pump User Manual...

  • Page 144: Replace The Heat Exchanger

    ➔ The heat exchanger does not need to be removed for pump head maintenance. Remove the 19 mm screw at the front of the secondary Remove the front plate. pump head. 1290 Infinity II High Speed Pump User Manual...
  • Page 145 If removed, first insert the spacer fitting. Then insert the Use the 19 mm screw for fixing the front plate. new heat exchanger to the opening in the pump head and lift it over the pins. Insert and fix the screw. 1290 Infinity II High Speed Pump User Manual...

  • Page 146: Assemble Longlife Pump Heads

    Pump Head Holder 5067-6197 Seal Handling Device Isopropanol Parts required Description 0905-1719 PE Seal 0905-1175 Wash seal (PTFE) Seals must be exchanged in both primary and secondary pump heads. N O T E 1290 Infinity II High Speed Pump User Manual...
  • Page 147 Seal Handling Device. The metal spring of the piston seal must be visible. Take care that the Seal Handling Device is seating flush Repeat for the other pump chamber. and press the seal into the pump chamber. 1290 Infinity II High Speed Pump User Manual...
  • Page 148 Repeat for the other seal holder. and press the wash seal into the seal holder. N O T E The Seal Handling Device has a cavity to fit over the pins of the seal wash tubings. 1290 Infinity II High Speed Pump User Manual...
  • Page 149 Mind the correct orientation: The backup ring must Both spring housings are identical, there is no risk face upwards and the seal holder must sit correcly. when mixing them, but make sure that the seal holder is oriented correctly. 1290 Infinity II High Speed Pump User Manual...
  • Page 150 Mount the pump head to the module. Do not fix the to approx. 5 Nm in a crosswise manner. screws at this stage! N O T E When the wrench clicks, the set torque is reached. Do not overtighten the screws. 1290 Infinity II High Speed Pump User Manual...
  • Page 151 Counter the outlet valve and tighten the lock screw of Attach the seal wash tubing interconnecting the two the heat exchanger capillary with a torque wrench set to pump heads. approx. 3 Nm. 1290 Infinity II High Speed Pump User Manual...
  • Page 152 Maintenance Pump Head Maintenance (Tool Free) Insert the screws that later fix the pump head assembly to the module housing. 1290 Infinity II High Speed Pump User Manual...

  • Page 153: Install The Pump Head Assembly

    Install the new pump head assembly by tightening the screws step by step. Apply approx. 5 Nm using a torque hex key, which is included to the 1290 Infinity Service Kit p/n 5067-4699. 1290 Infinity II High Speed Pump User Manual...
  • Page 154 4, channel B (right pump head assembly) to port 1 of the purge valve. Replace the seal wash tubes. Open the shut-off valves. Close the doors. Perform a Pump Leak Rate Test. 1290 Infinity II High Speed Pump User Manual...

  • Page 155: Replace The Outlet Valve

    (2). N O T E A gold seal between outlet valve and heat exchanger capillary is used for a tight connection. 1290 Infinity II High Speed Pump User Manual...
  • Page 156 Place the cap on the Outlet Valve. Mount the pump head assembly to the module, reconnect all hydraulic connections, and power up the pump. Open the shut off valves and purge the system to remove air. 1290 Infinity II High Speed Pump User Manual...

  • Page 157: Replace The Purge Valve Head

    The valve drive contains sensitive optical parts. Pollution of these parts can impair the accurate selection of valve ports and therefore bias measurement results. ➔ Protect the optical parts from dust and other pollutions. 1290 Infinity II High Speed Pump User Manual...
  • Page 158 Remove the head of the purge valve by pulling it to the Put the new valve head onto the valve drive such that front. the lobe fits to the groove. Screw the valve head onto the valve drive using the union nut. 1290 Infinity II High Speed Pump User Manual...
  • Page 159 Port 3: Pressure sensor, in • Port 4: Channel A • Ports 5 and 8: Waste capillaries, channels A and B • Port 9: Central port, connected to the Jet Weaver inlet 1290 Infinity II High Speed Pump User Manual...

  • Page 160: Replace Parts Of The High Pressure Filter Assembly

    This procedure describes replacements for channel A (left pump head assembly) and can N O T E be applied accordingly to channel B. In both cases, maintenance is done only at the secondary pump head outlet, which hosts the filter frit. 1290 Infinity II High Speed Pump User Manual...
  • Page 161 Re-install the filter assembly using the torque wrench note the correct orientation of the filter frit. (14 mm hex bit) set to approx. 16 Nm. Reconnect the capillary from the purge valve to the high pressure filter assembly. 1290 Infinity II High Speed Pump User Manual...

  • Page 162: Replace The Module Firmware

    Agilent web. http://www.agilent.com/en-us/firmwareDownload?whid=69761 2 For loading the firmware into the module follow the instructions in the documentation. Module Specific Information There is no specific information for this module. 1290 Infinity II High Speed Pump User Manual...

  • Page 163: Prepare The Pump Module For Transport

    For shipping the module, insert the Protective Foam to protected the module from mechanical damage. ➔ Be careful not to damage tubing or capillary connections while inserting the module in the Protective Foam. 1290 Infinity II High Speed Pump User Manual...
  • Page 164 Switch the solvent selection valve if applicable. 3 Remove tubing and capillary connections to other modules and the solvent cabinet. Remove tubing plugs. 1290 Infinity II High Speed Pump User Manual...
  • Page 165 4 Remove the shutoff valve panel by pulling it downwards. 5 You may keep internal tubing and capillary connections. 6 Remove cable connections to other modules. Remove the module from the stack. 1290 Infinity II High Speed Pump User Manual...
  • Page 166 7 Carefully insert the Protective Foam to the front part of the instrument. Do not damage any tubing or capillary connections. 8 Close the front cover. 9 For transport or shipment, put the module and accessory kit to the original shipment box. 1290 Infinity II High Speed Pump User Manual...

  • Page 167: Parts And Materials For Maintenance

    1290 Infinity II High Speed Pump User Manual Parts and Materials for Maintenance Overview of Maintenance Parts Flow Connections Pump Heads Pump Head Assembly Parts Primary Pump Head Parts Secondary Pump Head Parts Purge Valve Cover Parts Accessory Kit HPLC System Tool Kit This chapter provides information on parts for maintenance.

  • Page 168: Overview Of Maintenance Parts

    Parts and Materials for Maintenance Overview of Maintenance Parts Overview of Maintenance Parts Figure 11 Overview of main assemblies 1290 Infinity II High Speed Pump User Manual...
  • Page 169 SSV Valve Assembly 5065-4445 Peristaltic pump with Pharmed tubing G7104-60001 Pressure sensor 1300 bar 5067-4236 Purge valve head G4220-60350 Long Life Pump Head Channel A G4220-60360 Long Life Pump Head Channel B 1290 Infinity II High Speed Pump User Manual...

  • Page 170: Flow Connections

    Parts and Materials for Maintenance Flow Connections Flow Connections Figure 12 Flow connections of the High Speed Pump 1290 Infinity II High Speed Pump User Manual...
  • Page 171 (tubes from SSV to shutoff valve or degassing unit to MCGV) G7120-60017 Bottle Head Assembly Ultra Clean Tubing (bottle heads and tubing to shutoff panel / degasser) 5067-5760 Solvent Cabinet Kit (not shown) 1290 Infinity II High Speed Pump User Manual...

  • Page 172: Pump Heads

    For parts information on other pump head types, please refer to Agilent 1290 Infinity II Easy Maintenance Pump Head Technical Note (01200-90120) and to Agilent 1290 Infinity Pump Head Maintenance Technical Note (G4220-90122). Pump Head Assembly Parts 1290 Infinity II High Speed Pump User Manual...
  • Page 173 Outlet valve (primary pump head) 5042-9966 Cap Outlet Valve G4280-60026 High Pressure Filter Assembly (secondary pump head) G4220-81013 Heat Exchanger Channel A (secondary pump head only) G4220-40001 Link Plate 0960-2971 RF Transponder 1290 Infinity II High Speed Pump User Manual...
  • Page 174 Outlet valve (primary pump head) 5042-9966 Cap Outlet Valve G4280-60026 High Pressure Filter Assembly (secondary pump head) G4220-81012 Heat Exchanger Channel B (secondary pump head only) G4220-40001 Link Plate 0960-2971 RF Transponder 1290 Infinity II High Speed Pump User Manual...

  • Page 175: Primary Pump Head Parts

    Description 5067-5975 Plunger Assy ZrO 0515-6154 Screw-Socket-HD-Cap Hex-Recess M5X0.8 40 G4220-60046 Preload-Support Assembly LL 0905-1175 Wash seal (PTFE) G4220-60616 Seal Holder Integrated Assembly EM/LL 0905-1719 PE Seal G4220-60533 Body Head Primary EM/LL 1290 Infinity II High Speed Pump User Manual...

  • Page 176: Secondary Pump Head Parts

    Wash seal (PTFE) G4220-60616 Seal Holder Integrated Assembly EM/LL 0905-1719 PE Seal G4220-25513 Body Head Secondary EM/LL G4220-20001 Spacer Fitting G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20000 G4220-20003 Pump Head Screw 1290 Infinity II High Speed Pump User Manual...

  • Page 177: Purge Valve

    Parts and Materials for Maintenance Purge Valve Purge Valve Item Description 5067-4236 Purge valve head 1535-4857 Stator screws 5068-0004 Purge Valve Stator 5068-0201 Purge Valve Rotor Seal, PEEK, 1300 bar 1535-4045 Bearing ring 1290 Infinity II High Speed Pump User Manual...

  • Page 178: Cover Parts

    5067-5908 Top Cover G4224-60200 Side Cover Right 200 G4224-60201 Side Cover Left 200 5043-0856 Leak Adapter (not shown) 5067-5767 Door assy 200 left IF II 5067-5768 Door assy 200 right IF II 1290 Infinity II High Speed Pump User Manual...

  • Page 179: Accessory Kit

    5500-1217 Capillary ST 0.17 mm x 900 mm SI/SX ps-ps G7120-60005 Valve Holder left assembly INF II 01200-90091 1290 Infinity Pump Quick Reference Sheet 5067-6197 Seal Handling Device 5043-1400 Pump Head Holder 1290 Infinity II High Speed Pump User Manual...

  • Page 180: Hplc System Tool Kit

    Parts and Materials for Maintenance HPLC System Tool Kit HPLC System Tool Kit 1290 Infinity II High Speed Pump User Manual...

  • Page 181: Identifying Cables

    1290 Infinity II High Speed Pump User Manual Identifying Cables Cable Overview Analog Cables Remote Cables CAN/LAN Cables Agilent Module to PC This chapter provides information on cables used with the modules. Agilent Technologies...

  • Page 182: Cable Overview

    Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent 35900A A/D converter...
  • Page 183 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m USB cables Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) 1290 Infinity II High Speed Pump User Manual...

  • Page 184: Analog Cables

    The other end depends on the instrument to which connection is being made. Agilent Module to 35900 A/D converters p/n 35900-60750 35900 Pin Agilent Signal Name module Not connected Shield Analog - Center Analog + 1290 Infinity II High Speed Pump User Manual...
  • Page 185 Pin Agilent Signal Name module Shield Shield Analog - Center Center Analog + Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog + 1290 Infinity II High Speed Pump User Manual...

  • Page 186: Remote Cables

    High grey NOT USED pink SHUT DOWN blue START PREPARE black 1wire DATA violet DGND grey-pink +5V ERI out red-blue PGND white-green PGND brown-green +24V ERI out white-yellow +24V ERI out yellow-brown 1290 Infinity II High Speed Pump User Manual...
  • Page 187 • 5188-8045 ERI to APG (Connector D_Subminiature 15 pin (ERI), Connector D_Subminiature 9 pin (APG)) p/n 5188-8045 Pin (ERI) Signal Pin (APG) Active (TTL) Start Request Stop Ready High Power on High Future Shut Down Start Prepare Ground Cable Shielding 1290 Infinity II High Speed Pump User Manual...
  • Page 188 Ground Cable Shielding One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. 1290 Infinity II High Speed Pump User Manual...
  • Page 189 Wire Color Pin Agilent Signal Name Active module (TTL) White Digital ground Brown Prepare run Gray Start Blue Shut down Pink connected Yellow Power on High Ready High Green Stop Black Start request 1290 Infinity II High Speed Pump User Manual...

  • Page 190: Can/Lan Cables

    CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) 1290 Infinity II High Speed Pump User Manual...

  • Page 191: Agilent Module To Pc

    It is also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity II High Speed Pump User Manual...

  • Page 192: Usb

    To connect a USB Flash Drive use a USB OTG cable with Mini-B plug and A socket. Description 5188-8050 USB A M-USB Mini B 3 m (PC-Module) 5188-8049 USB A F-USB Mini B M OTG (Module to Flash Drive) 1290 Infinity II High Speed Pump User Manual...

  • Page 193: Hardware Information

    1290 Infinity II High Speed Pump User Manual Hardware Information Firmware Description Electrical Connections Serial Number Information Rear View of the Module Interfaces Overview Interfaces USB (Universal Serial Bus) Setting the 8-bit Configuration Switch Special Settings Early Maintenance Feedback Instrument Layout This chapter describes the pump in more detail on hardware and electronics.

  • Page 194: Firmware Description

    • run synchronization through APG/ERI remote, • error handling, • diagnostic functions, • or module specific functions like • internal events such as lamp control, filter movements, • raw data collection and conversion to absorbance. 1290 Infinity II High Speed Pump User Manual...
  • Page 195 Update of main system can be done in the resident system only. Update of the resident N O T E system can be done in the main system only. Main and resident firmware must be from the same set. Figure 13 Firmware Update Mechanism 1290 Infinity II High Speed Pump User Manual...
  • Page 196 All this specific information is described in the documentation provided with the firmware update tools. The firmware update tools, firmware and documentation are available from the Agilent web. • http://www.agilent.com/en-us/firmwareDownload?whid=69761 1290 Infinity II High Speed Pump User Manual...

  • Page 197: Electrical Connections

    There are no externally accessible fuses, because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations.

  • Page 198: Serial Number Information

    (there can be more than one code for the same module) 00000 Serial number Rear View of the Module Figure 14 Rear view of the High Speed Pump 1290 Infinity II High Speed Pump User Manual...

  • Page 199: Interfaces

    Agilent InfinityLab LC Series Interfaces Module RS-232 Analog APG (A) Special (on-board) / ERI (E) Pumps G7104A/C G7110B G7111A/B, G5654A G7112B G7120A G7161A/B Samplers G7129A/B/C G7167B/C, G5667A G7157A Detectors G7114A/B G7115A G7117A/B/C G7121A/B G7162A/B G7165A 1290 Infinity II High Speed Pump User Manual...
  • Page 200 • RS-232C as interface to a computer • USB (Universal Series Bus) as interface to a computer • REMOTE connector as interface to other Agilent products • Analog output connector(s) for signal output 1290 Infinity II High Speed Pump User Manual...

  • Page 201: Overview Interfaces

    “USB (Universal Serial Bus)” on page 203. Analog Signal Output The analog signal output can be distributed to a recording device. For details refer to the description of the module’s main board. 1290 Infinity II High Speed Pump User Manual...
  • Page 202 Remote (ERI) The ERI (Enhanced Remote Interface) connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. It allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.

  • Page 203: Usb (Universal Serial Bus)

    The line has a limited output of 0.5 A (1.7 A as of August 2011) and is self resetting. USB (Universal Serial Bus) USB (Universal Serial Bus) - replaces RS232, supports: • a PC with control software (for example Agilent Lab Advisor) • USB Flash Disk 1290 Infinity II High Speed Pump User Manual...

  • Page 204: Setting The 8-Bit Configuration Switch

    • For boot/test modes switches 1+2 must be UP plus required mode. For normal operation use the default (best) settings. N O T E Figure 15 Location of Configuration Switch (example shows a G4212A DAD) 1290 Infinity II High Speed Pump User Manual...
  • Page 205 When selecting the mode TEST, the LAN settings are: Auto-Negotiation & Using Stored. N O T E For explanation of "Boot Resident System" and "Revert to Default Data (Coldstart)" refer N O T E “Special Settings” on page 206. 1290 Infinity II High Speed Pump User Manual...

  • Page 206: Special Settings

    Forced cold start erases all methods and data stored in the non-volatile memory. Exceptions are calibration settings, diagnosis and repair log books which will not be erased. ➔ Save your methods and data before executing a forced cold start. 1290 Infinity II High Speed Pump User Manual...
  • Page 207 Setting the 8-bit Configuration Switch If you use the following switch settings and power the instrument up again, a forced cold start has been completed. Table 14 Forced Cold Start Settings (On-board LAN) Mode Select TEST/BOOT 1290 Infinity II High Speed Pump User Manual...

  • Page 208: Early Maintenance Feedback

    EMF limits, and then reset the EMF counters to zero. The next time the EMF counters exceed the new EMF limits, the EMF flag will be displayed, providing a reminder that maintenance needs to be scheduled. 1290 Infinity II High Speed Pump User Manual...

  • Page 209: Instrument Layout

    • the plastic layers help cushion the electronic and mechanical parts from physical shock, and • the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself. 1290 Infinity II High Speed Pump User Manual...
  • Page 210 Hardware Information Instrument Layout 1290 Infinity II High Speed Pump User Manual...
  • Page 211 1290 Infinity II High Speed Pump User Manual LAN Configuration What You Have to Do First TCP/IP parameter configuration Configuration Switch Initialization mode selection Dynamic Host Configuration Protocol (DHCP) General Information (DHCP) Setup (DHCP) Link configuration selection Manual Configuration With Telnet...

  • Page 212: Lan Configuration What You Have To Do First

    212) to • the PC network card using a crossover network cable (point-to-point) or • a hub or switch using a standard LAN cable. Figure 17 Location of LAN interface and MAC label 1290 Infinity II High Speed Pump User Manual...

  • Page 213: Tcp/Ip Parameter Configuration

    TCP/IP parameters after power-on. The parameters may be derived from non-volatile memory or initialized with known default values. The initialization mode is selected by the configuration switch, see Table 16 page 215. 1290 Infinity II High Speed Pump User Manual...

  • Page 214: Configuration Switch

    To perform any LAN configuration, SW1 and SW2 must be set to OFF. N O T E Table 15 Factory Default Settings Link Configuration speed and duplex mode determined by auto-negotiation, for details see “Link configuration selection” on page 220 1290 Infinity II High Speed Pump User Manual...

  • Page 215: Initialization Mode Selection

    The TCP/IP connection will be established using these parameters. The parameters were configured previously by one of the described methods. Figure 19 Using Stored (Principle) 1290 Infinity II High Speed Pump User Manual...
  • Page 216 In the Using Default mode, the parameters stored in the memory of the module are not N O T E cleared automatically. If not changed by the user, they are still available, when switching back to the mode Using Stored. 1290 Infinity II High Speed Pump User Manual...

  • Page 217: Dynamic Host Configuration Protocol (Dhcp)

    2 It may be necessary to fully qualify the hostname with the DNS suffix, e.g. 0030d3177321.country.company.com. 3 The DHCP server may reject the hostname proposed by the card and assign a name following local naming conventions. 1290 Infinity II High Speed Pump User Manual...

  • Page 218: Setup (Dhcp)

    0030d3177321. On the Local Controller the MAC address can be found under Details in the LAN section. Figure 22 LAN Setting on Instant Pilot 1290 Infinity II High Speed Pump User Manual...
  • Page 219 Lab Advisor, Firmware Update Tool) and use MAC address as host name, e.g. 0030d3177321. The LC system should become visible in the control software (see Note in section “General Information (DHCP)” on page 217). 1290 Infinity II High Speed Pump User Manual...

  • Page 220: Link Configuration Selection

    Link Configuration speed and duplex mode determined by auto-negotiation manually set to 10 Mbps, half-duplex manually set to 10 Mbps, full-duplex manually set to 100 Mbps, half-duplex manually set to 100 Mbps, full-duplex 1290 Infinity II High Speed Pump User Manual...

  • Page 221: Manual Configuration

    Therefore, manual configuration can be done at any time. A power cycle is mandatory to make the stored parameters become the active parameters, given that the initialization mode selection switches are allowing Figure 23 Manual Configuration (Principle) 1290 Infinity II High Speed Pump User Manual...

  • Page 222: With Telnet

    Handheld Controller, or the default IP address (see “Configuration Switch” on page 214). When the connection was established successfully, the module responds with the following: Figure 25 A connection to the module is made 1290 Infinity II High Speed Pump User Manual...
  • Page 223 Then press [Enter], where parameter refers to the configuration parameter you are defining, and value refers to the definitions you are assigning to that parameter. Each parameter entry is followed by a carriage return. 1290 Infinity II High Speed Pump User Manual...
  • Page 224 Initialization mode is Using Stored active TCP/IP settings stored TCP/IP settings in non-volatile memory connected to PC with controller software (e.g. Agilent ChemStation), here not connected Figure 28 Telnet - Change IP settings 1290 Infinity II High Speed Pump User Manual...
  • Page 225 If the Initialization Mode Switch is changed now to “Using Stored” mode, the instrument N O T E will take the stored settings when the module is re-booted. In the example above it would be 134.40.27.99. 1290 Infinity II High Speed Pump User Manual...

  • Page 226: Pc And User Interface Software Setup Setup

    This procedure describes the change of the TCP/IP settings on your PC to match the module’s default parameters in a local configuration (see also “Initialization mode selection” on page 215). Figure 30 Changing the TCP/IP settings of the PC 1290 Infinity II High Speed Pump User Manual...

  • Page 227: User Interface Software Setup

    LAN Configuration PC and User Interface Software Setup Setup User Interface Software Setup Install you user interface software according the provided User Interface Software Setup Guide. 1290 Infinity II High Speed Pump User Manual...
  • Page 228 LAN Configuration PC and User Interface Software Setup Setup 1290 Infinity II High Speed Pump User Manual...

  • Page 229: Appendix

    1290 Infinity II High Speed Pump User Manual Appendix General Safety Information General Safety Information Safety Standards General Before Applying Power Ground the Instrument Do Not Operate in an Explosive Atmosphere Do Not Remove the Instrument Cover Do Not Modify the Instrument...

  • Page 230: General Safety Information

    Do not use this product in any manner not specified by the manufacturer. The protective features of this product may be impaired if it is used in a manner not specified in the operation instructions. 1290 Infinity II High Speed Pump User Manual...

  • Page 231: Before Applying Power

    Verify that the voltage range and frequency of your power distribution matches to the power specification of the individual instrument. ➔ Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. ➔...

  • Page 232: Do Not Operate In An Explosive Atmosphere

    Personal injury (for example electrical shock, intoxication) ➔ Instruments that appear damaged or defective should be made inoperative and secured against unintended operation until they can be repaired by qualified service personnel. 1290 Infinity II High Speed Pump User Manual...

  • Page 233: Solvents

    For details, see the usage guideline for the solvent cabinet. A printed copy of the guideline N O T E has been shipped with the solvent cabinet, electronic copies are available in the Agilent Information Center or via the Internet. 1290 Infinity II High Speed Pump User Manual...

  • Page 234: Safety Symbols

    European Community directives. The European Declaration of Conformity is available at: http://regulations.corporate.agilent.com/DoC/search.htm Manufacturing date. Power symbol indicates On/Off. The apparatus is not completely disconnected from the mains supply when the power switch is in the Off position 1290 Infinity II High Speed Pump User Manual...
  • Page 235 C AU T I O N alerts you to situations that could cause loss of data, or damage of equipment. ➔ Do not proceed beyond a caution until you have fully understood and met the indicated conditions. 1290 Infinity II High Speed Pump User Manual...

  • Page 236: Waste Electrical And Electronic Equipment (Weee) Directive (2002-96-Ec)

    Do not dispose of in domestic household waste N O T E To return unwanted products, contact your local Agilent office, or see http://www.agilent.com for more information. 1290 Infinity II High Speed Pump User Manual...

  • Page 237: Radio Interference

    Appendix Radio Interference Radio Interference Cables supplied by Agilent Technologies are screened to provide optimized protection against radio interference. All cables are in compliance with safety or EMC regulations. Test and Measurement If test and measurement equipment is operated with unscreened cables, or...

  • Page 238: Sound Emission

    This product has a sound pressure emission (at the operator position) < 70 dB. • Sound Pressure Lp < 70 dB (A) • At Operator Position • Normal Operation • According to ISO 7779:1988/EN 27779/1991 (Type Test) 1290 Infinity II High Speed Pump User Manual...

  • Page 239: Agilent Technologies On Internet

    Appendix Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com 1290 Infinity II High Speed Pump User Manual...
  • Page 240 Encoder failed leak sensor open drive position limit leak sensor short cable drive timeout leak capillaries lost CAN partner cleaning 1290 Infinity II High Speed Pump User Manual...
  • Page 241 LongLife pump head install assembling doors disassembling fan failed instrument layout lost CAN partner firmware 1290 Infinity II High Speed Pump User Manual...
  • Page 242 1290 Infinity II High Speed Pump User Manual...
  • Page 243 TCP/IP parameter configuration telnet configuration temperature sensor tests pump leak rate test system pressure test timeout transport prepare troubleshooting error messages unknown purge valve type 1290 Infinity II High Speed Pump User Manual...
  • Page 244 In This Book This manual contains technical reference information about the Agilent 1290 Infinity II High Speed Pump (G7120A). • introduction and specifications, • using and optimizing, • troubleshooting and diagnose, • maintenance, • parts identification, • hardware information, •...

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