Page 1 Agilent 1290 Infinity Quaternary Pump User Manual Agilent Technologies...
Page 2 1987) or any equivalent agency regulation or contract clause. Use, duplication or dis- closure of Software is subject to Agilent Technologies’ standard commercial license terms, and non-DOD Departments and Agencies of the U.S. Government will 1290 Infinity Quaternary Pump User Manual...
Page 3 In This Guide... In This Guide... This manual covers the Agilent 1290 Infinity Quaternary Pump (G4204A). 1 Introduction This chapter gives an introduction to the module, instrument overview and internal connectors. 2 Site Requirements and Specifications This chapter provides information on environmental requirements, physical and performance specifications.
Page 4 8 Test Functions and Calibrations This chapter will describe the tests for the module. 9 Maintenance This chapter describes the maintenance of the Agilent 1290 Infinity Quaternary Pump. 10 Parts and Materials This chapter provides information on parts for maintenance.
Page 5: Table Of Contents
Installation of Seal Wash Option 4 Using the Pump Leak and Waste Handling Preparing the Pump Algae Growth in HPLC Systems Setting up the Pump with the Instrument Control Interface Priming the Pump Flushing the Filter Solvent Information 1290 Infinity Quaternary Pump User Manual...
Page 6 Replacing the Inlet Valve Replacing the Outlet Valve Removing the Jet Weaver Installing the Jet Weaver Replacing the Seal Wash Pump Replacing the Multi-Channel Gradient Valve (MCGV) Releasing a Stuck Inlet Valve Replacing the Pump Head 1290 Infinity Quaternary Pump User Manual...
Page 7 Secondary Pump Head Parts Multi Purpose Valve Solvent Cabinet Cover Parts Leak Parts Accessory Kit Others 11 Identifying Cables Cable Overview Analog cables Remote Cables BCD Cables CAN/LAN Cable RS-232 Cable Kit Agilent 1200 Module to Printer 1290 Infinity Quaternary Pump User Manual...
Page 8 Automatic configuration with Bootp Manual Configuration PC and User Interface Software Setup Setup 14 Appendix General Safety Information The Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Radio Interference Sound Emission Agilent Technologies on Internet 1290 Infinity Quaternary Pump User Manual...
Page 9 1290 Infinity Quaternary Pump User Manual Introduction Features Overview of the Quaternary Pump Operating Principle Positions of the Multi Purpose Valve System Overview Leak and Waste Handling This chapter gives an introduction to the module, instrument overview and internal connectors.
Page 10: Introduction Features
• Fast defill function for improved intake and delivery performance. • Two pistons in series design for increased reliability. • High resolution piston movement control for smooth and reliable motion. For specifications, see “Performance Specifications” on page 28. 1290 Infinity Quaternary Pump User Manual...
Page 11: Overview Of The Quaternary Pump
The Agilent 1290 Infinity Quaternary Pump is suitable for a wide range of columns and HPLC und UHPLC applications starting from typical 250 x 4.6 mm HPLC columns going down to high resolution 50 x 2.1 mm UHPLC columns and can be used in a flow range between 0.05 –...
Page 12: Operating Principle
A high resolution encoder unit is attached to the pump drives, which divides a single turn into 65000 steps. Each step corresponds to a volume of about 300 pL, which allows an extremely precise control. 1290 Infinity Quaternary Pump User Manual...
Page 13: Operating Principle
Introduction Operating Principle Inline filter Jet Weaver (optional) Multi Purpose Valve Pressure sensor Solvent bottles Degasser Pump head Multi-channel gradient valve Inlet weaver Figure 1 The hydraulic path 1290 Infinity Quaternary Pump User Manual...
Page 14: Positions Of The Multi Purpose Valve
Valve. The flow passes the inline filter and leaves the valve through port 4 to the system (autosampler etc.). From pump To system Inline filter Figure 2 Valve position in normal operating mode without mixer 1290 Infinity Quaternary Pump User Manual...
Page 15: Positions Of The Multi Purpose Valve
Introduction Positions of the Multi Purpose Valve Purge Mode In purge mode, the flow is diverted to the waste container. From pump To waste Figure 3 Valve position in purge mode 1290 Infinity Quaternary Pump User Manual...
Page 16 In this mode, the flow passes an optional Jet Weaver and the inline filter. This configuration is recommended for special applications which require an increased mixing efficiency. From pump Jet Weaver To system Inline filter Figure 4 Valve position in normal operating mode with mixer 1290 Infinity Quaternary Pump User Manual...
Page 17 5, passes the inline filter in opposite direction and leaves to the waste through port 7. From pump To waste Inline filter Figure 5 Valve position in filter flush mode 1290 Infinity Quaternary Pump User Manual...
Page 18 Service Mode In service mode, the flow is diverted to port 3, where for example a restriction capillary can be installed for diagnostic tests. From pump Restriction capillary Figure 6 Valve position in service mode 1290 Infinity Quaternary Pump User Manual...
Page 19: System Overview
System Overview System Overview Leak and Waste Handling The 1200 Infinity Series has been designed for safe leak and waste handling. It is important that all security concepts are understood and instructions are carefully followed. 1290 Infinity Quaternary Pump User Manual...
Page 20: System Overview
Introduction System Overview Figure 7 Leak and waste handling concept (overview - typical stack configuration as an example) 1290 Infinity Quaternary Pump User Manual...
Page 21 The waste tube of the purge valve (6) guides solvents to waste. The waste tube connected to the leak pan outlet on each of the bottom instruments (7) guides the solvent to a suitable waste container. 1290 Infinity Quaternary Pump User Manual...
Page 22 Introduction System Overview 1290 Infinity Quaternary Pump User Manual...
Page 23: Site Requirements And Specifications
1290 Infinity Quaternary Pump User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications This chapter provides information on environmental requirements, physical and performance specifications. Agilent Technologies...
Page 24: Site Requirements
➔ Make sure the power connector of the instrument can be easily reached and unplugged. ➔ Provide sufficient space behind the power socket of the instrument to unplug the cable. 1290 Infinity Quaternary Pump User Manual...
Page 25 Never operate your instrumentation from a power outlet that has no ground connection. ➔ Never use a power cord other than the Agilent Technologies power cord designed for your region. Use of unsupplied cables WA R N I N G Using cables not supplied by Agilent Technologies can lead to damage of the electronic components or personal injury.
Page 26 Do not store, ship or use your module under conditions where temperature fluctuations could cause condensation within the module. ➔ If your module was shipped in cold weather, leave it in its box and allow it to warm slowly to room temperature to avoid condensation. 1290 Infinity Quaternary Pump User Manual...
Page 27: Physical Specifications
Operating altitude Up to 2000 m (6562 ft) Non-operating altitude Up to 4600 m (15092 ft) For storing the module Safety standards: IEC, CSA, Installation category II, Pollution degree 2 For indoor use only. 1290 Infinity Quaternary Pump User Manual...
Page 28: Performance Specifications
Delay volume Standard configuration: <350 µL With optional V380 Jet Weaver: <500 µL Composition range Settable range: 0 – 100 % Recommended range: 1 – 99 % or 5 µL/min per channel, whatever is greater. 1290 Infinity Quaternary Pump User Manual...
Page 29 Electronic records of maintenance and errors. Housing All materials recyclable. 1290 Infinity Quaternary Pump User Manual...
Page 30 Site Requirements and Specifications Performance Specifications 1290 Infinity Quaternary Pump User Manual...
Page 31: Installing The Module
Removing the Transport Foam Installing the Pump Flow Connections to the Pump Installation of Seal Wash Option This chapter gives information about the preferred stack setup for your system and the installation of your Agilent 1290 Infinity Quaternary Pump. Agilent Technologies...
Page 32: Unpacking The Module
Unpacking the Module Damaged Packaging If the delivery packaging shows signs of external damage, please call your Agilent Technologies sales and service office immediately. Inform your service representative that the instrument may have been damaged during shipment. "Defective on arrival" problems C A U T I O N If there are signs of damage, please do not attempt to install the module.
Page 33 For parts identification please check the illustrated parts breakdown in “Parts and Materials” page 201. Please report any missing or damaged parts to your local Agilent Technologies sales and service office. 1290 Infinity Quaternary Pump User Manual...
Page 34: Optimizing The Stack Configuration
Installing the Module Optimizing the Stack Configuration Optimizing the Stack Configuration If your module is part of a complete Agilent 1290 Infinity Liquid Chromatograph, you can ensure optimum performance by installing the following configurations. These configurations optimize the system flow path, ensuring minimum delay volume.
Page 35 Installing the Module Optimizing the Stack Configuration Instant Pilot Solvent cabinet Detector Column compartment Autosampler Pump Figure 8 Recommended stack configuration for 1290 Infinity with quaternary pump (front view) 1290 Infinity Quaternary Pump User Manual...
Page 36 Optimizing the Stack Configuration LAN to control software CAN Bus cable to Instant Pilot Analog detector signal (optional) AC Power CAN Bus cable Figure 9 Recommended stack configuration for 1290 Infinity with quaternary pump (rear view) 1290 Infinity Quaternary Pump User Manual...
Page 37: Two Stack Configuration
37 and Figure 11 on page 38). Instant Pilot Detector Column compartment Solvent cabinet Pump Autosampler Thermostat for the ALS (optional) Figure 10 Recommended two stack configuration for 1290 Infinity with quaternary pump (front view) 1290 Infinity Quaternary Pump User Manual...
Page 38 LAN to control software CAN Bus cable to Instant Pilot Analog detector signal (optional) Thermo cable (optional) CAN Bus cable AC Power Figure 11 Recommended two stack configuration for 1290 Infinity with quaternary pump (rear view) 1290 Infinity Quaternary Pump User Manual...
Page 39: Installation Information On Leak And Waste Handling
A printed copy of the guideline has been shipped with the solvent cabinet, electronic copies are available on the Internet. Recommendations for Solvent Cabinet N O T E For details, see the usage guideline for the Agilent 1200 Infinity Series Solvent Cabinets. 1290 Infinity Quaternary Pump User Manual...
Page 40 Installing the Module Installation Information on Leak and Waste Handling Figure 12 Leak and waste handling (overview - typical stack configuration as an example) 1290 Infinity Quaternary Pump User Manual...
Page 41 ➔ Do not bend tubes. ➔ Do not immerse tube end in waste liquid. ➔ Do not intubate tubes in other tubes. ➔ For correct tubing follow instructions on label attached to the module. 1290 Infinity Quaternary Pump User Manual...
Page 42 Installing the Module Installation Information on Leak and Waste Handling Figure 13 Warning label (illustration for correct waste tubing) 1290 Infinity Quaternary Pump User Manual...
Page 43: Removing The Transport Foam
Installing the Module Removing the Transport Foam Removing the Transport Foam Open the front cover of the module. Carfully remove the protective foam. Close the front cover. 1290 Infinity Quaternary Pump User Manual...
Page 44: Installing The Pump
1 Place the module on the bench in a horizontal position. 2 Ensure the power switch on the front of the module is OFF (switch stands out). Status indicator Power switch Serial number Figure 14 Front view of the quaternary pump 1290 Infinity Quaternary Pump User Manual...
Page 45 Figure 15 Rear view of the quaternary pump In an Agilent 1290 Infinity System, the individual modules are connected by CAN cables. An N O T E Agilent 1200 Series Instant Pilot can be connected to the CAN bus of any module.
Page 46: Flow Connections To The Pump
Multi Purpose Valve. This section describes the installation of additional flow connections. Parts required Description Other modules G4220-68755 Accessory Kit 5067-4644 Solvent Cabinet Kit 1290 Infinity Pump Preparations Pump is installed in the LC system. 1290 Infinity Quaternary Pump User Manual...
Page 47 5 Connect the inlet tubes of the bottle- head assemblies to the inlet connectors A to D at the left hand side of the vacuum degasser. Fix the tubes in the tubing grommets of the pump. Tubing clips Degasser inlets Tubing grommets 1290 Infinity Quaternary Pump User Manual...
Page 48 To autosampler From solvent bottles 8 If the pump is not part of an Agilent 1290 Infinity system stack or placed on the bottom of a stack, connect the waste tube to the waste outlet of the pump leak handling system.
Page 49: Installation Of Seal Wash Option
Installation of Seal Wash Option Installation of Seal Wash Option The 1290 Infinity Quaternary Pump is optionally available with a seal wash function. This option is recommended when using buffers or other non- volatile solvents or additives that could deposit on pistons and seals.
Page 50 Installing the Module Installation of Seal Wash Option 1290 Infinity Quaternary Pump User Manual...
Page 51: Using The Pump
Setting up the Pump with the Instrument Control Interface Overview Instrument Configuration The Pump User Interface (Dashboard Panel) Control Settings Method Parameter Settings Priming the Pump Flushing the Filter Solvent Information This chapter explains the operational parameters of the Agilent 1290 Infinity Quaternary Pump. Agilent Technologies...
Page 52: Leak And Waste Handling
N O T E For details, see the usage guideline for the Agilent 1200 Infinity Series Solvent Cabinets. For details on correct installation, see section Installation Information on Leak and Waste Handling in the service manual. 1290 Infinity Quaternary Pump User Manual...
Page 53: Preparing The Pump
• Never leave an unused pump with water in a channel for an extended period of time (2- 3 days). Always flush with organic solvent or add 10 % isopropanol to water. 1290 Infinity Quaternary Pump User Manual...
Page 54: Algae Growth In Hplc Systems
• Use the amber solvent bottle (Solvent bottle, amber (9301- 1450)) supplied with the instrument for your aqueous mobile phase. • If possible add a few mg/l sodium azide or a few percent organic solvent to the aqueous mobile phase. 1290 Infinity Quaternary Pump User Manual...
Page 55: Setting Up The Pump With The Instrument Control Interface
Parameters described in following sections is offered by the instrument control interface and can usually be accessed through Agilent instrument control software. For details, please refer to manuals and online help of respective user interfaces. 1290 Infinity Quaternary Pump User Manual...
Page 56: Instrument Configuration
The Quaternary Pump configuration parameters are in two sections: • Communication • Options Communication: The parameters in this dialog box are detected automatically during autoconfiguration. • Device name, • Type ID, • Serial number, • Firmware revision, • Button Connection settings 1290 Infinity Quaternary Pump User Manual...
Page 57 Configure Solvent Type Catalogs: Displays the Solvent Type Catalogs dialog box, which allows you to import and export solvent calibration data. See “Importing Solvent Calibration Tables” on page 88. Please refer to the online help of your user interface for more detailed information. 1290 Infinity Quaternary Pump User Manual...
Page 58: The Pump User Interface (Dashboard Panel)
The pressure setpoints. The red line shows the current maximum pressure limit; the green area shows the current pressure (also shown as text). The current solvent flow rate (in mL/min) is displayed above the pressure display. 1290 Infinity Quaternary Pump User Manual...
Page 59 “Instrument Configuration” on page 56). Tuning Indicates the tuning efforts of 1290 Infinity pumps. For pumps operating as expected, the signal should stay in a range of -1 to +1 within the full scale of -2 to +2. Pressure Limit The current maximum pressure limit.
Page 60 Flush Filter On/Off Allows you flushing a clogged inline filter, which is connected to the Multi Purpose Valve, see “Filter Flush Mode” page 17. Use the pump self-test for checking the filter back pressure. 1290 Infinity Quaternary Pump User Manual...
Page 61: Control Settings
• On all the time: The seal wash is active when the pump is on or in standby mode. Automatic Turn On Module can be turned on at a specified date/time. This feature can only be used if the module power switch is turned on. 1290 Infinity Quaternary Pump User Manual...
Page 62 Conditioning may be necessary if the pump may contain air, for example after running out of solvent, after a long period of standby or after service or repair. 1290 Infinity Quaternary Pump User Manual...
Page 63: Method Parameter Settings
• Used: Mark this check box if you want to use this solvent or blend in the method. • %: Enter the percentage of the solvent or blend in this field. • Name: Type a name for the solvent or blend in this field. 1290 Infinity Quaternary Pump User Manual...
Page 64 External Contacts The External Contacts section enables you to set up the switching of the external contacts. N O T E The External Contacts section is present only when a BCD/external contacts board is installed. 1290 Infinity Quaternary Pump User Manual...
Page 65 You can set a limit on the rate of change of the solvent flow to protect your Gradient 1000.000 mL/min/min analytical column. You can set individual values for Flow ramp up and Flow in steps of ramp down. 0.001 mL/min/min Default value: 100.000 mL/min/min 1290 Infinity Quaternary Pump User Manual...
Page 66 • Change Solvent Composition - You can only use solvents, which have been enabled in the solvents section. • Function centric view - This checkbox allows you displaying parameter changes instead of a time table. 1290 Infinity Quaternary Pump User Manual...
Page 67 Final conc. For the relationship of stock concentration and concentration in the mixture, the composition accuracy needs to be considered (see “Performance Specifications” page 28). • Conc. unit: The concentration can be defined as mM (mmol/L) or as %. 1290 Infinity Quaternary Pump User Manual...
Page 68: Priming The Pump
The pump should never be used for priming empty tubings (never let the pump run dry). Use N O T E a syringe to draw enough solvent for completely filling the tubings to the pump inlet before continuing to prime with the pump. 1290 Infinity Quaternary Pump User Manual...
Page 69 6 Observe the pressure fluctuations. The system is air free as soon as the pressure is stable. 7 Change solvents and column according to the analytical conditions and purge the system to change solvents. 1290 Infinity Quaternary Pump User Manual...
Page 70: Flushing The Filter
Solvent inlet filter 2 An outlet filter (average pore size 5 µm; Outlet filter 1290 Infinity Quaternary Pump (G4204- 60004)) between pump head and pressure sensor filters out particles which may be created in the pump by wear of piston or wash seals.
Page 71 Flushing the Filter 3 An inline filter connected to the Multi Purpose Valve with a small pore size of about 0.3 µm ( In- Line Filter Assembly for 1290 Infinity Quaternary Pump (5067- 5407)). This filter can be flushed using the graphical user interface or replaced as required.
Page 72: Solvent Information
UHMW-PE, SST Pressure sensor Multi Purpose Valve Polyimide, SST, DLC Ultra clean tubings are available for the use with high-end MS detectors. They are also compatible to THF. Inlet Weaver, Jet Weaver, Heat Exchanger 1290 Infinity Quaternary Pump User Manual...
Page 73 There is still a number of known incompatibilities with chemicals such as chloroform, methylene chloride, THF, DMSO, strong acids (nitric acid > 10 %, sulphuric acid > 10 %, sulfonic acids, trichloroacetic acid), halogenes or aequous halogene solutions, phenol and derivatives (cresols, salicylic acid etc.). 1290 Infinity Quaternary Pump User Manual...
Page 74 Polyethylene (PE) Agilent uses UHMW (ultra- high molecular weight)- PE/PTFE blends for yellow piston and wash seals, which are used in 1290 Infinity pumps and for normal phase applications in 1260 Infinity pumps. Polyethylene has a good stability for most common inorganic solvents including acids and bases in a pH range of 1 to 12.5.
Page 75 There are no documented incompatibilities for HPLC applications. Fused silica and Quartz (SiO Fused silica is used in 1290 Infinity Flow Cells and capillaries. Quartz is used for classical flow cell windows. It is inert against all common solvents and acids except hydrofluoric acid and acidic solvents containing fluorides.
Page 76 Sapphire, Ruby and Al -based ceramics Sapphire, ruby and ceramics based on aluminum oxide Al are inert to almost all common acids, bases and solvents. There are no documented incompatibilities for HPLC applications. 1290 Infinity Quaternary Pump User Manual...
Page 77 10 % isopropanol. • Regularly maintain the LC system. 1290 Infinity Quaternary Pump User Manual...
Page 78 Such systems should be flushed regularly with pure water and may require shorter maintenance cycles. Using a seal wash option should be considered for protecting pump heads. 1290 Infinity Quaternary Pump User Manual...
Page 79: How To Optimize The Performance Of Your Module
1290 Infinity Quaternary Pump User Manual How to Optimize the Performance of Your Module Using the Degasser Operational Hints for the Multi Channel Gradient Valve (MCGV) Delay Volume and Extra-Column Volume Delay Volume How to Configure the Optimum Delay Volume...
Page 80: Using The Degasser
How to Optimize the Performance of Your Module Using the Degasser Using the Degasser The quaternary pump has a built- in degasser, which should always be included to the flow path. 1290 Infinity Quaternary Pump User Manual...
Page 81: Operational Hints For The Multi Channel Gradient Valve (Mcgv)
(flow/retention time stability), a blockage or internal leak of the pump. Avoid the use of such solvent combinations, as they can cause irreproducible chromatographic results. 1290 Infinity Quaternary Pump User Manual...
Page 82: Delay Volume And Extra-Column Volume
For the 1290 Infinity Quaternary Pump, all pump parts downstream the MCGV contribute to the delay volume, i.e. inlet weaver, pump heads, capillary connections, filters and the optional Jet Weaver.
Page 83: How To Configure The Optimum Delay Volume
How to Configure the Optimum Delay Volume How to Configure the Optimum Delay Volume The design of the 1290 Infinity Quaternary Pump offers a strongly decreased delay volume compared to standard 600 bar pressure pumps. For the 1290 Infinity Quaternary Pump, mixing is done in the multi- channel gradient valve at ambient pressure.
Page 84 How to Optimize the Performance of Your Module How to Configure the Optimum Delay Volume Figure 16 The Jet Weaver mixer The installation procedure is illustrated in “Installing the Jet Weaver” page 141. 1290 Infinity Quaternary Pump User Manual...
Page 85: How To Achieve Higher Resolution
If an automated method development system was used in the decision on phases it is likely that short columns were used for fast analysis in each step of the scouting. 1290 Infinity Quaternary Pump User Manual...
Page 86 This is the reason that the 1290 Infinity LC system was designed to go to 1200 bar so that it can run sub- two- micron particles and column length can be increased to 100 mm or 150 mm.
Page 87 STM column (at temperatures above 40 °C) can generate higher peak capacity than a longer STM column by virtue of running it faster. (Refer to Petersson et al., J.Sep.Sci, 31, 2346- 2357, 2008, Maximizing peak capacity and separation speed in liquid chromatography). 1290 Infinity Quaternary Pump User Manual...
Page 88: Using Solvent Calibration Tables
5 Navigate to the location of the solvent calibration table and click Open. 6 The new solvent will now appear in the Solvent Type Catalogs. 7 The imported solvent is now available for selection as a solvent type, Table 4 on page 63. 1290 Infinity Quaternary Pump User Manual...
Page 89: Troubleshooting And Diagnostics
1290 Infinity Quaternary Pump User Manual Troubleshooting and Diagnostics Overview of the Module’s Indicators and Test Functions Status indicators Power Supply Indicator Module Status Indicator Available Tests vs User Interfaces Agilent Lab Advisor Software Overview about the troubleshooting and diagnostic features.
Page 90: Overview Of The Module's Indicators And Test Functions
Diagnostic Signals The module has several signals (internal temperatures, voltages and currents of lamps) that can be used for diagnosing baseline problems. These can be added like normal signals in the Agilent ChemStation software. 1290 Infinity Quaternary Pump User Manual...
Page 91: Status Indicators
Power switch Serial number Figure 17 Location of status indicators Power Supply Indicator The power supply indicator is integrated into the main power switch. When the indicator is illuminated (green) the power is ON. 1290 Infinity Quaternary Pump User Manual...
Page 92: Module Status Indicator
In such a case try to re- boot the module or try a cold- start (see “Special Settings” on page 256). Then try a firmware update (see “Replacing Module Firmware” on page 195). If this does not help, a main board replacement is required. 1290 Infinity Quaternary Pump User Manual...
Page 93: Available Tests Vs User Interfaces
“Agilent Lab Advisor Software” on page 94. • The Agilent ChemStation B.04.02 and above may not include any maintenance/test functions. • Screenshots used within these procedures are based on the Agilent Lab Advisor software. 1290 Infinity Quaternary Pump User Manual...
Page 94: Agilent Lab Advisor Software
Agilent 1200 Infinity and Infinity II Series instruments. The tests and diagnostic features that are provided by the Agilent Lab Advisor software may differ from the descriptions in this manual. For details, refer to the Agilent Lab Advisor software help files. 1290 Infinity Quaternary Pump User Manual...
Page 95: Error Information
1290 Infinity Quaternary Pump User Manual Error Information What Are Error Messages General Error Messages Timeout Shutdown Remote Timeout Lost CAN Partner Leak Sensor Short Leak Sensor Open Compensation Sensor Open Compensation Sensor Short Fan Failed Leak Pump Error Messages...
Page 96 Seal wash pump was missing when tried to turn on Valve hardware overcurrent (MCGV) This chapter describes the meaning of error messages, and provides information on probable causes and suggested actions how to recover from error conditions. 1290 Infinity Quaternary Pump User Manual...
Page 97: What Are Error Messages
In all cases, error propagation is done via the CAN bus or via an APG remote cable (see documentation for the APG interface). 1290 Infinity Quaternary Pump User Manual...
Page 98: General Error Messages
Leak detected in an external instrument restarting the module. with a remote connection to the system. Check external instruments for a shut-down Shut-down in an external instrument with a condition. remote connection to the system. 1290 Infinity Quaternary Pump User Manual...
Page 99: Remote Timeout
• Ensure all CAN cables are installed correctly. Exchange the CAN cable. Defective CAN cable. Switch off the system. Restart the system, and Defective main board in another module. determine which module or modules are not recognized by the system. 1290 Infinity Quaternary Pump User Manual...
Page 100: Leak Sensor Short
Leak sensor not connected to the main representative. board. Please contact your Agilent service Defective leak sensor. representative. Please contact your Agilent service Leak sensor incorrectly routed, being representative. pinched by a metal component. 1290 Infinity Quaternary Pump User Manual...
Page 101: Compensation Sensor Open
Please contact your Agilent service Defective power switch board representative. Please contact your Agilent service Loose connection between the power representative. switch board and the main board Please contact your Agilent service Defective main board. representative. 1290 Infinity Quaternary Pump User Manual...
Page 102: Fan Failed
This changes the resistance of the leak sensor which is sensed by the leak- sensor circuit on the main board. Probable cause Suggested actions Ensure all fittings are tight. Loose fittings. Exchange defective capillaries. Broken capillary. 1290 Infinity Quaternary Pump User Manual...
Page 103: Pump Error Messages
• Parameter: None Probable cause Suggested actions Check for leaks. Leak Check bottle filling. Bottle empty Check solvent. Wrong solvent (viscosity) Check flow rate and lower pressure limit. Inappropriate setting Replace column. Column degradation 1290 Infinity Quaternary Pump User Manual...
Page 104: Target Pressure Not Reached For Quaternary Pump Degasser
The counter for the solvent volume has exceeded the limit, which has been set in the user interface. Probable cause Suggested actions Refill solvent bottle. No solvent present. Check solvent counter setting in user interface. Inappropriate setting. 1290 Infinity Quaternary Pump User Manual...
Page 105: Waste Counter Limit Exceeded
Check for leaks in the pump and flow path. Leak Fill solvent bottle. Bottle empty. Open shutoff valve. Shutoff valve closed (if applicable). Replace pressure sensor. Drift of pressure sensor (unlikely for short tests taking some minutes). 1290 Infinity Quaternary Pump User Manual...
Page 106: Quaternary Pump Shutdown During Analysis
• Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Defect connection between encoder and representative. main board. Please contact your Agilent service Missing or defect tag Defect connection representative. between tag and encoder. 1290 Infinity Quaternary Pump User Manual...
Page 107: Writing The Pump Encoder Tag Failed
Pump drive blocked or encoder failed Error ID: 29214 Pump drive blocked or encoder failed. • Parameter: None Probable cause Suggested actions Please contact your Agilent service Blockage of the pump drive Drive encoder representative. failed. 1290 Infinity Quaternary Pump User Manual...
Page 108: Drive Current Too Low
• Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Check for blockage of e.g. outlet valve filter frit, Blockage of system before pressure sensor. Multi Purpose Valve, heat exchanger. Please contact your Agilent service Drive motor defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 109: Drive Timeout
• Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Check for blockage of e.g. outlet valve filter frit, Blockage of system before pressure sensor. Multi Purpose Valve, heat exchanger. Please contact your Agilent service Drive motor defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 110: Deliver Underrun
Defect encoder. representative. Pump drive encoder defect Error ID: 29209 Defect pump drive encoder. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Defect encoder. representative. 1290 Infinity Quaternary Pump User Manual...
Page 111: Multi Purpose Valve Failed
Error ID: 29232 Invalid pump drive encoder signals have been detected. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 112: Drive Position Limit
Error ID: 29237, 29238, 29239, 29215 An error has occurred for the pump drive encoder. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 113: Writing The Multi Purpose Valve Tag Failed
Error ID: 29211 The pump drive encoder has generated no signal. • Parameter: 1 – 2 referring to pump drive Probable cause Suggested actions Please contact your Agilent service Pump drive encoder is defect. representative. 1290 Infinity Quaternary Pump User Manual...
Page 114: Pump Drive Error
Probable cause Suggested actions Please contact your Agilent service Wiper shifted representative. Replace, clean or repair pump head. Pump head blocks piston movement Please contact your Agilent service Pump drive motor is mechanically blocked. representative. 1290 Infinity Quaternary Pump User Manual...
Page 115: Pump Drive Stop Not Found
Either the limit, time frame or the current value of the variable has been modified later directly or indirectly. Probable cause Suggested actions Verify control software, macros, manual Incorrect parameters have been sent to the commands. instrument by the control software or manual changes. 1290 Infinity Quaternary Pump User Manual...
Page 116: Timeout: Wait For Run Volume
(for example the flow rate). Probable cause Suggested actions Verify control software, macros, manual Incorrect parameters have been sent to the commands. instrument by the control software or manual changes. 1290 Infinity Quaternary Pump User Manual...
Page 117: Timeout: Wait For Flow
Verify control software, macros, manual Incorrect parameters have been sent to the commands. instrument by the control software or manual changes. Run system pressure test for identifying and Leak localizing the leak. Tighten leak. 1290 Infinity Quaternary Pump User Manual...
Page 118: Drive Encoder Failed
Suggested actions Please contact your Agilent service Leak in degasser chamber or degasser representative. tubing. Please contact your Agilent service Defect vacuum pump. representative. Block unused degasser channels. Degasser chamber empty or connected to air. 1290 Infinity Quaternary Pump User Manual...
Page 119: Seal Wash Pump Was Missing When Tried To Turn On
Error ID: 29227 Power consumption too high for one of the MCGV valves. Probable cause Suggested actions Replace MCGV. Cable defect. Replace MCGV. Valve defect Please contact your Agilent service Defective main board. representative. 1290 Infinity Quaternary Pump User Manual...
Page 120 Error Information Pump Error Messages 1290 Infinity Quaternary Pump User Manual...
Page 121: Test Functions And Calibrations
1290 Infinity Quaternary Pump User Manual Test Functions and Calibrations This chapter will describe the tests for the module. Currently, no diagnostic procedures are available. Agilent Technologies...
Page 122 Test Functions and Calibrations Pump Error Messages 1290 Infinity Quaternary Pump User Manual...
Page 123: Maintenance
1290 Infinity Quaternary Pump User Manual Maintenance Introduction to Maintenance Warnings and Cautions Overview of Maintenance Cleaning the Module Installing Fittings and Capillaries Replacing the Pressure Sensor Replacing the Inlet Weaver Replacing the Inlet Valve Replacing the Outlet Valve Removing the Jet Weaver...
Page 124 Maintenance Pump Error Messages Installing the Valve Rail Kit Replacing Module Firmware Preparing the Pump Module for Transport This chapter describes the maintenance of the Agilent 1290 Infinity Quaternary Pump. 1290 Infinity Quaternary Pump User Manual...
Page 125: Introduction To Maintenance
Introduction to Maintenance Figure 18 on page 125 shows the main user- accessible assemblies of the Agilent 1290 Infinity Quaternary Pump. These parts can be accessed from the front (simple repairs) and don’t require to remove the pump from the system stack.
Page 126: Warnings And Cautions
Agilent product user guides, or use of the products in violation of applicable laws, rules or regulations. ➔ Use your Agilent products only in the manner described in the Agilent product user guides. 1290 Infinity Quaternary Pump User Manual...
Page 127 C A U T I O N ➔ If you connect external equipment to the instrument, make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment. 1290 Infinity Quaternary Pump User Manual...
Page 128: Overview Of Maintenance
Maintenance Overview of Maintenance Overview of Maintenance The following pages describe maintenance (simple repairs) of the module that can be carried out without opening the main cover. 1290 Infinity Quaternary Pump User Manual...
Page 129: Cleaning The Module
WA R N I N G hazard and damage the module ➔ Do not use an excessively damp cloth during cleaning. ➔ Drain all solvent lines before opening any connections in the flow path. 1290 Infinity Quaternary Pump User Manual...
Page 130: Installing Fittings And Capillaries
The lifetime of a fitting depends on how firmly it has been tightened; firm tightening N O T E reduces the lifetime. If fitting has been overtightened, replace it. 1 Install fittings and capillaries. 2 Tighten fittings and capillaries. 1290 Infinity Quaternary Pump User Manual...
Page 131: Replacing The Pressure Sensor
Working on connections to the pressure sensor may slightly change the displayed N O T E pressure. In case of a pressure offset at ambient pressure, a pressure offset calibration may be run. 1290 Infinity Quaternary Pump User Manual...
Page 132 Carefully pull out the pressure sensor for about 2 cm. Connect the new pressure sensor to the pressure sensor Then unscrew the cable from the pressure sensor. connector. 1290 Infinity Quaternary Pump User Manual...
Page 133 Connect the capillary from the pump head outlet to the pressure sensor inlet. Two arrow signs on the pressure sensor indicate the flow direction. If applicable, connect the outlet of the pressure sensor to the central port of the Multi Purpose Valve. 1290 Infinity Quaternary Pump User Manual...
Page 134: Replacing The Inlet Weaver
Replacing the Inlet Weaver Parts required Description G4204-81090 1290 Infinity Quaternary Pump Inlet Weaver Assembly Preparations • Switch off pump at the main power switch • Remove the front cover • Use an optional solvent shutoff valve or lift up solvent filters inside solvent bottles for avoiding leakages •...
Page 135 Insert the new inlet weaver to the inlet valve. Fix the weaver with the plastic screw. Fix the fitting of the new inlet weaver to the MCGV. Reconnect tubings between MCGV and degasser. Fitting 1290 Infinity Quaternary Pump User Manual...
Page 136: Replacing The Inlet Valve
Torque wrench 2 – 25 Nm Parts required Description G4204-60022 Inlet Valve 1290 Infinity Quaternary Pump Preparations • Switch off pump at the main power switch • Remove the front cover • Use an optional solvent shutoff valve or lift up solvent filters inside solvent bottles for avoiding leakages •...
Page 137: Replacing The Outlet Valve
The seal can be heat exchanger. Then lift up the capillary and remove it replaced separately as needed. from the primary pump head. Hex screw Gold seal Heat exchanger 1290 Infinity Quaternary Pump User Manual...
Page 138 Purge the system to remove air. outlet valve. Using a torque wrench with a 2.5 mm hex bit, set 3 Nm and close the hex screw at the top of the outlet. 3 Nm 1290 Infinity Quaternary Pump User Manual...
Page 139: Removing The Jet Weaver
• Switch off the pump at the main power switch. Remove capillary connections from the Jet Weaver to the Open the screw, which fixes the Jet Weaver to the front Multi Purpose Valve. panel. 1290 Infinity Quaternary Pump User Manual...
Page 140 If no other Jet Weaver shall be installed, use plastic (2). fittings for closing unused ports of the valve and install the metal lid. Plastic fittings Otherwise continue at “Installing the Jet Weaver” page 141. 1290 Infinity Quaternary Pump User Manual...
Page 141: Installing The Jet Weaver
Maintenance Installing the Jet Weaver Installing the Jet Weaver When The optional Jet Weaver 380 µL for 1290 Infinity Quaternary Pump (G4204-68000) is available for applications which require highest mixing performance, see chapter Optimizing Performance. Tools required Description Screwdriver Pozidriv #1...
Page 142 Connect the inlet capillary of the Jet Weaver to port 2 of Configure the Jet Weaver as mixer in the user interface, the Multi Purpose Valve. Connect the outlet capillary to “Instrument Configuration” on page 56. port 1. Port 1 Port 2 1290 Infinity Quaternary Pump User Manual...
Page 143: Replacing The Seal Wash Pump
Remove the flow connections from and to the seal wash pump. For removing the seal wash pump, press the clips (1) and Insert the pump clips to the holes in the module housing. pull the pump to the front (2). 1290 Infinity Quaternary Pump User Manual...
Page 144 Maintenance Replacing the Seal Wash Pump Fix tubings of the peristaltic pump to the primary pump head outlet and secondary pump head inlet. 1290 Infinity Quaternary Pump User Manual...
Page 145: Replacing The Multi-Channel Gradient Valve (Mcgv)
For best performance and life time, use lower channels A and D for aqueous solvents in N O T E buffer applications, see “Operational Hints for the Multi Channel Gradient Valve (MCGV)” on page 81 for details. 1290 Infinity Quaternary Pump User Manual...
Page 146 Remove the inlet weaver, see “Replacing the Inlet between the degassing unit and the MCGV. Weaver” on page 134. Waste funnel Degassing unit MCGV Remove the waste funnel. Remove the cover from the MCGV. 1290 Infinity Quaternary Pump User Manual...
Page 147 Disconnect the MCGV cable (1), unscrew the two screws Place the new MCGV into position. (2, 3) and remove the valve. Channel A N O T E Make sure that channel A of the MCGV is put at the bottom-right position. 1290 Infinity Quaternary Pump User Manual...
Page 148 MCGV cover. Install the inlet weaver, see “Replacing the Inlet Weaver” on page 134. Waste tube holder Reconnect solvent tubes for channels A-D from the Waste MCGV to the degasser outlets. funnel Clips 1290 Infinity Quaternary Pump User Manual...
Page 149: Releasing A Stuck Inlet Valve
Open the fitting at the center of the multi-channel MCGV such that you can access the inlet weaver. gradient valve (MCGV). Do not open the screw marked with the red cross. Remove the inlet weaver from the MCGV. Fitting 1290 Infinity Quaternary Pump User Manual...
Page 150 Fill the syringe with a suitable wash solvent. Connect the syringe and adapter to the inlet weaver. N O T E For salt deposits, warm water is a good choice. For organic deposits, use ethanol or acetone. 1290 Infinity Quaternary Pump User Manual...
Page 151 Maintenance Releasing a Stuck Inlet Valve Push the syringe for flushing the inlet valve and pump Restore original connections. Flush the system for head. several minutes. 1290 Infinity Quaternary Pump User Manual...
Page 152: Replacing The Pump Head
Adapter ¼ in square to hex Parts required Description G4204-60200 1290 Infinity Quaternary Pump Head Assembly with Seal Wash Option G4204-60400 1290 Infinity Quaternary Pump Head Assembly without Seal Wash Option Preparations • Switch off pump at the main power switch •...
Page 153 In Lab Advisor go to Tools > Remove/Install Pump Head DO NOT REMOVE the capillary connection between the and follow instructions given on the screen. pump heads marked by the red X. If applicable, remove flow connections of the seal wash option. 1290 Infinity Quaternary Pump User Manual...
Page 154 Remove the complete pump head assembly by holding both heads and pulling it to the front. N O T E N O T E Open all screws step by step, not screw by screw. Do not further disassemble the pump head. 1290 Infinity Quaternary Pump User Manual...
Page 155 Install the new pump head assembly by tightening the screws step by step. Apply 5 Nm using a torque hex key, which is included to the 1290 Infinity Service Kit p/n 5067-4699. 1290 Infinity Quaternary Pump User Manual...
Page 156 Insert the heat exchanger capillary into the outlet of the primary pump head. Using a torque key, which is included to the 1290 Infinity Service Kit p/n 5067-4699, set 3 Nm and close the hex screw at the top of the outlet.
Page 157 Maintenance Replacing the Pump Head Connect the capillary from the pressure sensor to the pump head outlet filter. Pressure sensor Outlet filter 1290 Infinity Quaternary Pump User Manual...
Page 158: Disassembling The Pump Head
Such pump heads are available through Agilent service. The 1290 Infinity pump service kit (5067-4699) includes all tools required for the procedures described in subsequent sections.
Page 159 Then lift up the capillary and remove it from the primary pump head. Link plate Primary pump head Heat exchanger with connection capillary Secondary pump head Clips 1290 Infinity Quaternary Pump User Manual...
Page 160: Disassembling The Primary Pump Head
Remove the outlet valve at the top of the pump head and For disassembling the pump head, remove the 4 hex the inlet valve at the bottom of the primary pump head. screws at the rear of the pump head. Outlet valve Inlet valve 1290 Infinity Quaternary Pump User Manual...
Page 161 Pump chamber housing Remove the piston from the piston housing by pushing it Check the pump pistons for scratches grooves and dents. to the rear, then pull it out from the rear. Piston surface 1290 Infinity Quaternary Pump User Manual...
Page 162 Do not use the pump piston for that purpose, as this can break it! Pump head parts in contact with the piston seal need to be cleaned properly in order to get a smooth surface and a tight connection. 1290 Infinity Quaternary Pump User Manual...
Page 163 To clean the piston and the pump head sufrace, use the ultra fine abrasive mesh (p/n 8660-0852). If the wash seal shall be replaced by a new one, use the steel side of the insert tool for removing it. Wash seal 1290 Infinity Quaternary Pump User Manual...
Page 164: Disassembling The Secondary Pump Head
Do not use the piston for removing pump seals. Remove the outlet filter at the top of the pump head. For disassembling the pump head, remove the 4 hex screws at the rear of the pump head. 1290 Infinity Quaternary Pump User Manual...
Page 165 Insert tool Damaged pistons cause micro leaks and will decrease the lifetime of the seals. Pump seal N O T E Do not use the pump piston for that purpose, as this can break it! 1290 Infinity Quaternary Pump User Manual...
Page 166 (p/n 8660-0852). N O T E Pump head parts in contact with the piston seal need to be cleaned properly in order to get a smooth surface and a tight connection. 1290 Infinity Quaternary Pump User Manual...
Page 167 To dry the pump head and to remove residues, use If the wash seal shall be replaced by a new one, use the pressurized air ((1), (2) and (3)). steel side of the insert tool for removing it. Wash seal 1290 Infinity Quaternary Pump User Manual...
Page 168: Replacing The Heat Exchanger
Parts required Description G4220-81013 Heat Exchanger (secondary pump head only) G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20001 Spacer Fitting Preparations • Remove the pump head assembly from the pump • Remove the secondary pump head from the link plate...
Page 169 Remove the 19 mm screw at the front of the secondary Remove the front plate. pump head. Remove the screw at the bottom of the pump head. Do Lift out the heat exchanger. not drop the golden spacer fitting. 1290 Infinity Quaternary Pump User Manual...
Page 170 Use the 19 mm screw for fixing the front plate. new heat exchanger to the opening in the pump head and lift it over the pins. Pins Front plate Screw Spacer fitting Insert and fix the screw. 1290 Infinity Quaternary Pump User Manual...
Page 171: Replacing Wash Seal And Gasket
Use the soft plastic side of the insert tool for inserting the wash seal. wash seal into the support ring. Wet the wash seal with isopropanol or another suitable solvent before insertion. Wash seal 1290 Infinity Quaternary Pump User Manual...
Page 172 Maintenance Replacing Wash Seal and Gasket Put the gasket into the support ring and insert the seal holder. 1290 Infinity Quaternary Pump User Manual...
Page 173: Assembling The Pump Head
➔ Observe pins on the support ring, which help assembling the parts of the pump head in the correct orientation. 1290 Infinity Quaternary Pump User Manual...
Page 174 Wet the piston piston housing. Observe the pins on the support ring, seal with isopropanol or another suitable solvent before which help you assembling the pump head correctly. insertion. Insert tool Pump seal Pump chamber housing 1290 Infinity Quaternary Pump User Manual...
Page 175 Observe correct The screws will be fixed tightly later. orientation of the pin. N O T E Do NOT install the inlet and outlet valves and the outlet filter at this stage. 1290 Infinity Quaternary Pump User Manual...
Page 176 Not using will break the pump head. Insert the pump head to the pump head alignment tool, which is included to the 1290 Infinity Service Kit p/n 5067-4699. There are openings for the seal wash support ring and heat exchanger of the secondary pump head.
Page 177 For handling the torque wrench, setting and applying the right torque, consult the manual of your torque wrench. Using a torque key, which is included to the 1290 Infinity Service Kit p/n 5067-4699, set 5 Nm and fix the central alignment screw.
Page 178 Heat exchanger capillary wrench. Using a torque key, which is included to the 1290 Infinity Service Kit p/n 5067-4699, set 5 Nm and fix the 4 screws at the rear of the alignment tool. Tighten screws crosswise.
Page 179 For the primary pump head, install the inlet valve and outlet valve using the torque wrench, which is included to the 1290 Infinity Service Kit p/n 5067-4699. Set 10 Nm for the inlet valve and 10 Nm for the outlet valve.
Page 180 For the secondary pump head, install the outlet filter using the torque wrench (14 mm hex bit), which is included to the 1290 Infinity Service Kit p/n 5067-4699, set to 16 Nm. 16 Nm 1290 Infinity Quaternary Pump User Manual...
Page 181 Observe the correct orientation of the primary and the secondary pump head. This is important for correct fixation of the heat exchanger and the capillaries, as described in the following steps. N O T E Mind the orientation of the ID tag. 1290 Infinity Quaternary Pump User Manual...
Page 182 Correct wrench. Install the new pump head assembly by tightening the screws step by step. Apply 5 Nm using a torque hex key, which is included to the 1290 Infinity Service Kit p/n 5067-4699. 1290 Infinity Quaternary Pump User Manual...
Page 183 Insert the heat exchanger capillary into the outlet of the primary pump head. Using a torque key, which is included to the 1290 Infinity Service Kit p/n 5067-4699, set 3 Nm and close the hex screw at the top of the outlet.
Page 184 Maintenance Assembling the Pump Head Connect the capillary from the pressure sensor to the pump head outlet filter. Pressure sensor Outlet filter 1290 Infinity Quaternary Pump User Manual...
Page 185: Replacing The Multi Purpose Valve
Remove all capillary connections from the Multi Purpose Valve. Remove the clamp with the inline filter. Unscrew the black union nut and remove the head of the purge valve by pulling it to the front. Clamp Inlet filter 1290 Infinity Quaternary Pump User Manual...
Page 186 Replacing the Multi Purpose Valve Put the new valve head onto the valve drive such that the lobe fits to the groove. Screw the valve head onto the valve drive using the union nut. 1290 Infinity Quaternary Pump User Manual...
Page 187 • Port 6 is blocked by a blank nut (SST) • Port 7 is connected to the waste capillary • Port 8 is connected to the inlet of the inline filter Block unused ports with blank nuts. 1290 Infinity Quaternary Pump User Manual...
Page 188: Replacing Parts Of The Multi Purpose Valve
Description 8710-2394 9/64 inch hex key Parts required Description 1534-4045 Bearing ring 5068-0123 Rotor seal, Multi Purpose Valve 1290 Infinity Quaternary Pump, 1200 bar 5068-0120 Stator ring 5068-0001 Stator head 1535-4857 Stator screws, 10/Pk Preparations • Remove capillary connections from ports 1, 3 and 6.
Page 189: Replacing The Outlet Filter
Torque wrench head, 14 mm for torque wrench Parts required Description G4204-60004 Outlet filter 1290 Infinity Quaternary Pump Remove the capillary from the outlet filter to the pressure Remove the outlet filter using a 14 mm wrench. sensor. 1290 Infinity Quaternary Pump User Manual...
Page 190 Maintenance Replacing the Outlet Filter Mount the new outlet filter. Using a torque wrench set to Mount the capillary connection to the pressure sensor. 16 Nm is recommended. 16 Nm 1290 Infinity Quaternary Pump User Manual...
Page 191: Replacing Parts Of The Inline Filter
8710-0510 Wrench open 1/4 — 5/16 inch Parts required Description 5067-5407 In-Line Filter Assembly for 1290 Infinity Quaternary Pump 5067-4748 Capillary ST, 0.17 mm x 90 mm Multi Purpose Valve to inline filter 5023-0271 Frit 0.3 µm for inline filter, 5/pk...
Page 192 Remove the inline filter from the clamp attached to the the inline filter. Multi Purpose Valve. Inline filter Clamp Use two 5/16 wrenches for opening the inline filter. Replace the filter frit and reassemble the inline filter. Filter frit 1290 Infinity Quaternary Pump User Manual...
Page 193 Put the inline filter to the clamp and install its capillaries. The integrated capillary is connected to port 5 of the Multi Purpose Valve. The removable capillary is connected to port 8. Port 5 Port 8 Removable capillary Integrated capillary 1290 Infinity Quaternary Pump User Manual...
Page 194: Installing The Valve Rail Kit
1 The valve rail is fixed to the pump cover by 4 screws. The position of the lower screws is marked on the module cover. First tighten these screws, and then tighten the upper screws. Screws 1290 Infinity Quaternary Pump User Manual...
Page 195: Replacing Module Firmware
Update Tool and the documentation from the Agilent web. • http://www.chem.agilent.com/_layouts/agilent/downloadFirmware.aspx?whid=69761 2 For loading the firmware into the module follow the instructions in the documentation. Module Specific Information There is no specific information for this module. 1290 Infinity Quaternary Pump User Manual...
Page 196: Preparing The Pump Module For Transport
3 If applicable, remove tubings between the seal wash function and solvent bottle/waste. 4 Remove cable and capillary connections to other modules. 5 Remove the module from the stack. 6 Remove the waste tube. 1290 Infinity Quaternary Pump User Manual...
Page 197 7 Disconnect the degasser outlet tubings at the MCGV one after another. Use a syringe for removing liquid from the degasser and the solvent tubings. 8 Reconnect the degasser outlet tubings to the MCGV. Remove the degasser inlet tubings. 1290 Infinity Quaternary Pump User Manual...
Page 198 Maintenance Preparing the Pump Module for Transport 9 You may keep internal tubing and capillary connections. Degasser Multi channel gradient valve Pressure sensor Inlet weaver Pump heads Multi Purpose Valve 1290 Infinity Quaternary Pump User Manual...
Page 199 10 Carefully insert the protective foam to the front part of the instrument. Do not damage any tubing or capillary connections. 11 Close the front cover. 12 For transport or shipment, put the module and accessory kit to the original shipment box. 1290 Infinity Quaternary Pump User Manual...
Page 200 Maintenance Preparing the Pump Module for Transport 1290 Infinity Quaternary Pump User Manual...
Page 201: Parts And Materials
1290 Infinity Quaternary Pump User Manual Parts and Materials Overview of Main Assemblies Flow Connections Seal Wash Option Pump Head Assembly Parts Primary Pump Head Parts Secondary Pump Head Parts Multi Purpose Valve Solvent Cabinet Cover Parts Leak Parts Accessory Kit...
Page 202: Overview Of Main Assemblies
Parts and Materials Overview of Main Assemblies Overview of Main Assemblies Figure 19 Overview of maintenance parts 1290 Infinity Quaternary Pump User Manual...
Page 203 In-Line Filter Assembly for 1290 Infinity Quaternary Pump 5023-0271 Frit 0.3 µm for inline filter, 5/pk G4204-40000 Clamp for In-Line Filter G4204-60200 1290 Infinity Quaternary Pump Head Assembly with Seal Wash Option G4204-60400 1290 Infinity Quaternary Pump Head Assembly without Seal Wash Option G4204-81090...
Page 204: Flow Connections
Parts and Materials Flow Connections Flow Connections Figure 20 Flow connections of the pump 1290 Infinity Quaternary Pump User Manual...
Page 205 Tubing Kit 140 mm - Ultra Clean Tubing (tubes from SSV to shutoff valve or degassing unit to MCGV) G4220-60017 Bottle Head Assembly Ultra Clean Tubing (bottle heads and tubing to shutoff panel / degasser) 1290 Infinity Quaternary Pump User Manual...
Page 206: Seal Wash Option
Parts and Materials Seal Wash Option Seal Wash Option Figure 21 Seal Wash Pump Item Description 5067-4793 Peristaltic Pump with Fixation Springs 5065-9978 Tubing, 1 mm i.d., 3 mm o.d., silicone, 5 m 1290 Infinity Quaternary Pump User Manual...
Page 207: Pump Head Assembly Parts
Pump Head Assembly Parts Figure 22 Pump head assembly parts Item Description G4204-60200 1290 Infinity Quaternary Pump Head Assembly with Seal Wash Option G4204-60400 1290 Infinity Quaternary Pump Head Assembly without Seal Wash Option G4220-81013 Heat Exchanger (secondary pump head only)
Page 208: Primary Pump Head Parts
Parts and Materials Primary Pump Head Parts Primary Pump Head Parts Primary Pump Head with Seal Wash (Quaternary Pump) Figure 23 Primary pump head (Quaternary Pump) with seal wash 1290 Infinity Quaternary Pump User Manual...
Page 209 Inlet Valve 1290 Infinity Quaternary Pump G4204-40006 Fixation screw inlet weaver to PIV (not shown) G4220-60028 Outlet valve (primary pump head) G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20020 Internal gold seal for Outlet Valve 1290 Infinity Quaternary Pump User Manual...
Page 210 Parts and Materials Primary Pump Head Parts Primary Pump Head Without Seal Wash (Quaternary Pump) Figure 24 Primary pump head (Quaternary Pump) without seal wash 1290 Infinity Quaternary Pump User Manual...
Page 211 Inlet Valve 1290 Infinity Quaternary Pump G4204-40006 Fixation screw inlet weaver to PIV (not shown) G4220-60028 Outlet valve (primary pump head) G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20020 Internal gold seal for Outlet Valve 1290 Infinity Quaternary Pump User Manual...
Page 212: Secondary Pump Head Parts
Parts and Materials Secondary Pump Head Parts Secondary Pump Head Parts Secondary Pump Head With Seal Wash (Quaternary Pump) Figure 25 Secondary pump head (Quaternary Pump) with seal wash 1290 Infinity Quaternary Pump User Manual...
Page 213 Screw M5, 40 mm long G4220-20003 Pump Head Screw Pump Head Front Plate (order pump head) G4220-81013 Heat Exchanger (secondary pump head only) G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20001 Spacer Fitting Pump Chamber Housing (order pump head) 0905-1719 PE Seal G4220-60016...
Page 214 Parts and Materials Secondary Pump Head Parts Secondary Pump Head Without Seal Wash (Quaternary Pump) Figure 26 Secondary pump head (Quaternary Pump) without seal wash 1290 Infinity Quaternary Pump User Manual...
Page 215 Screw M5, 40 mm long G4220-20003 Pump Head Screw Pump Head Front Plate (order pump head) G4220-81013 Heat Exchanger (secondary pump head only) G4220-20028 Headless screw for 1290 Infinity pump heads G4220-20001 Spacer Fitting Pump Chamber Housing (order pump head) 0905-1719 PE Seal G4220-60015...
Page 216: Multi Purpose Valve
Parts and Materials Multi Purpose Valve Multi Purpose Valve Figure 27 Multi-purpose valve parts 1290 Infinity Quaternary Pump User Manual...
Page 217 5067-4174 Multi Purpose Valve Head 1535-4857 (3x) Stator screws, 10/Pk 5068-0001 Stator head 5068-0120 Stator ring 5068-0123 Rotor seal, Multi Purpose Valve 1290 Infinity Quaternary Pump, 1200 bar 1535-4045 Bearing ring 5068-0106 Spanner nut 1290 Infinity Quaternary Pump User Manual...
Page 218: Solvent Cabinet
Parts and Materials Solvent Cabinet Solvent Cabinet Figure 28 Solvent Cabinet Parts (1) Figure 29 Solvent Cabinet Parts (2) 1290 Infinity Quaternary Pump User Manual...
Page 219 Description 5065-9981 Solvent cabinet 1200 Infinity, including all plastic parts 5043-0207 Name plate 1260 5065-9954 Front panel, solvent cabinet 5042-8907 Leak panel 9301-1450 Solvent bottle, amber 9301-1420 Solvent bottle, transparent G4220-60007 Bottle Head Assembly 1290 Infinity Quaternary Pump User Manual...
Page 220: Cover Parts
Parts and Materials Cover Parts Cover Parts Figure 30 Cover parts 1290 Infinity Quaternary Pump User Manual...
Page 221 Parts and Materials Cover Parts Item Description 5067-5396 1290 Infinity Quaternary Pump Cover Kit (base, top, left, right) 5042-9964 Name plate for Agilent 1290 series 5067-4683 Front Panel 5042-8914 Serial number plate 1290 Infinity Quaternary Pump User Manual...
Page 222: Leak Parts
Parts and Materials Leak Parts Leak Parts Figure 31 Leak parts 1290 Infinity Quaternary Pump User Manual...
Page 223 Leak Parts Item Description 5041-8389 Leak funnel holder 5041-8388 Leak funnel 5062-2463 Corrugated tubing, PP, 6.5 mm id, 5 m G1361-47100 Sealing lip 5042-9922 Leak panel G4280-40016 Power Switch Coupler ZL 5041-8381 Power switch button 1290 Infinity Quaternary Pump User Manual...
Page 224: Accessory Kit
Parts and Materials Accessory Kit Accessory Kit The Accessory Kit 1290 Infinity Quaternary Pump (G4204- 68705) contains: Item Description 0100-1816 Fitting Waste Tube to Purge Valve 5067-4755 Flexible Waste Tube, 5 m 5063-6527 Leak tubing assembly, 1 m 5181-1519 CAN cable, Agilent module to module, 1 m...
Page 225: Others
Hex key 2.5 mm, 15 cm long, straight handle 8710-2438 Hex key 2.0 mm 8710-2509 Screwdriver Torx TX8 8710-2594 Double open end wrench 4 mm x 5 mm 9301-0411 Syringe, Plastic 9301-1337 Adapter syringe/solvent tube with fitting 1290 Infinity Quaternary Pump User Manual...
Page 226: 1290 Infinity Pump Service Kit
Torque wrench 2 – 25 Nm G4220-20013 4 mm hex bit G4220-20014 2.5 mm Hex Bit G4220-20015 Adapter ¼ in square to hex G4204-44000 Transport protection foam 5023-0285 Replacement kit for 1290 Infinity pump head alignment tool (piston/handle) 1290 Infinity Quaternary Pump User Manual...
Page 227: Identifying Cables
1290 Infinity Quaternary Pump User Manual Identifying Cables Cable Overview Analog cables Remote Cables BCD Cables CAN/LAN Cable RS-232 Cable Kit Agilent 1200 Module to Printer This chapter provides information on cables used with the Agilent 1200 Infinity Series modules.
Page 228: Cable Overview
Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent module to 3394/6 integrators...
Page 229 It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity Quaternary Pump User Manual...
Page 230: Analog Cables
Pin Agilent Signal Name module Not connected Shield Analog - Center Analog + Agilent Module to BNC Connector p/n 8120-1840 Pin BNC Pin Agilent Signal Name module Shield Shield Analog - Center Center Analog + 1290 Infinity Quaternary Pump User Manual...
Page 231 Identifying Cables Analog cables Agilent Module to General Purpose p/n 01046-60105 Pin Agilent Signal Name module Not connected Black Analog - Analog + 1290 Infinity Quaternary Pump User Manual...
Page 232: Remote Cables
Identifying Cables Remote Cables Remote Cables One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. Agilent Module to 3396A Integrators...
Page 233 5 - Pink connected 6 - Yellow 6 - Yellow Power on High 7 - Red 7 - Red Ready High 8 - Green 8 - Green Stop 9 - Black 9 - Black Start request 1290 Infinity Quaternary Pump User Manual...
Page 234 01046-60201 Wire Color Pin Agilent Signal Name Active module (TTL) White Digital ground Brown Prepare run Gray Start Blue Shut down Pink connected Yellow Power on High Ready High Green Stop Black Start request 1290 Infinity Quaternary Pump User Manual...
Page 235: Bcd Cables
Black BCD 0 Orange BCD 3 BCD 2 Brown BCD 1 Gray Digital ground Gray Gray/pink BCD 11 Red/blue BCD 10 White/green BCD 9 Brown/green BCD 8 not connected not connected + 5 V 1290 Infinity Quaternary Pump User Manual...
Page 236 Agilent Module to 3396 Integrators p/n 03396-60560 Pin 3396 Pin Agilent Signal Name BCD Digit module BCD 5 BCD 7 BCD 6 BCD 4 BCD0 BCD 3 BCD 2 BCD 1 Digital ground + 5 V 1290 Infinity Quaternary Pump User Manual...
Page 237: Can/Lan Cable
CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) 1290 Infinity Quaternary Pump User Manual...
Page 238: Rs-232 Cable Kit
It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity Quaternary Pump User Manual...
Page 239: Agilent 1200 Module To Printer
Agilent 1200 Module to Printer Description 5181-1529 Cable Printer Serial & Parallel, is a SUB-D 9 pin female vs. Centronics connector on the other end (NOT FOR FW UPDATE). For use with G1323 Control Module. 1290 Infinity Quaternary Pump User Manual...
Page 240 Identifying Cables Agilent 1200 Module to Printer 1290 Infinity Quaternary Pump User Manual...
Page 241: Hardware Information
1290 Infinity Quaternary Pump User Manual Hardware Information Firmware Description Electrical Connections Rear View of the Module Interfaces Overview Interfaces Setting the 8-bit Configuration Switch Special Settings Early Maintenance Feedback Instrument Layout This chapter describes the pump in more detail on hardware and electronics.
Page 242: Firmware Description
• an instrument specific section, called main system Resident System This resident section of the firmware is identical for all Agilent 1100/1200/1220/1260/1290 series modules. Its properties are: • the complete communication capabilities (CAN, LAN and RS- 232C) • memory management •...
Page 243 Update of main system can be done in the resident system only. Update of the resident N O T E system can be done in the main system only. Main and resident firmware must be from the same set. Figure 32 Firmware Update Mechanism 1290 Infinity Quaternary Pump User Manual...
Page 244 All these specific informations are described in the documentation provided with the firmware update tools. The firmware update tools, firmware and documentation are available from the Agilent web. • http://www.chem.agilent.com/_layouts/agilent/downloadFirmware.aspx?whid=69761 1290 Infinity Quaternary Pump User Manual...
Page 245: Electrical Connections
There are no externally accessible fuses, because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations.
Page 246: Rear View Of The Module
Hardware Information Electrical Connections Rear View of the Module APG-Remote Power supply for external CAN valves Configuration switch CAN-Bus RS232 USB port Power plug Figure 33 Rear of quaternary pump 1290 Infinity Quaternary Pump User Manual...
Page 247: Interfaces
G1364C FC-AS G1330B/K1330B μ CAN-DC- OUT for CAN G1364D FC- slaves G1367E HiP ALS K1367E HiP ALS Clinical Ed. G1377A HiP micro ALS G2258A DL ALS G5664A Bio-inert FC-AS G5667A Bio-inert Autosampler G4226A ALS 1290 Infinity Quaternary Pump User Manual...
Page 248 K1321B FLD Clinical Ed. G1321C FLD G1362A RID G4280A ELSD EXT Contact AUTOZERO Others G1170A Valve Drive G1316A/C TCC K1316C TCC Clinical Ed. G1322A DEG K1322A DEG Clinical Ed. G1379B DEG G4225A DEG K4225A DEG Clinical Ed. 1290 Infinity Quaternary Pump User Manual...
Page 249 • CAN connectors as interface to other modules • LAN connector as interface to the control software • RS- 232C as interface to a computer • REMOTE connector as interface to other Agilent products • Analog output connector(s) for signal output 1290 Infinity Quaternary Pump User Manual...
Page 250: Overview Interfaces
• one start bit and one stop bit are always used (not selectable). The RS- 232C is designed as DCE (data communication equipment) with a 9- pin male SUB- D type connector. The pins are defined as: 1290 Infinity Quaternary Pump User Manual...
Page 251 RS-232C Connection Table Direction Function Ground Figure 34 RS-232 Cable Analog Signal Output The analog signal output can be distributed to a recording device. For details refer to the description of the module’s main board. 1290 Infinity Quaternary Pump User Manual...
Page 252 APG Remote The APG Remote connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. Remote control allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.
Page 253 The module includes a DC- Out (24 VDC) power line that is intended to be used with certain modules that operate as CAN slaves, for example external valves. The line has a limited output of 1.7 A and is self resetting. 1290 Infinity Quaternary Pump User Manual...
Page 254: Setting The 8-Bit Configuration Switch
Location of Configuration Switch (example shows a G4212A DAD) To perform any LAN configuration, SW1 and SW2 must be set to OFF. For details on the N O T E LAN settings/configuration refer to chapter LAN Configuration. 1290 Infinity Quaternary Pump User Manual...
Page 255 When selecting the mode TEST, the LAN settings are: Auto-Negotiation & Using Stored. N O T E For explanation of "Boot Resident System" and "Revert to Default Data (Coldstart)" refer to N O T E “Special Settings” on page 256. 1290 Infinity Quaternary Pump User Manual...
Page 256: Special Settings
Save your methods and data before executing a forced cold start. If you use the following switch settings and power the instrument up again, a forced cold start has been completed. Table 12 Forced Cold Start Settings (On-board LAN) Mode Select TEST/BOOT 1290 Infinity Quaternary Pump User Manual...
Page 257: Early Maintenance Feedback
EMF limits, and then reset the EMF counters to zero. The next time the EMF counters exceed the new EMF limits, the EMF flag will be displayed, providing a reminder that maintenance needs to be scheduled. 1290 Infinity Quaternary Pump User Manual...
Page 258: Instrument Layout
• the plastic layers help cushion the electronic and mechanical parts from physical shock, and • the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself. 1290 Infinity Quaternary Pump User Manual...
Page 259: Lan Configuration
1290 Infinity Quaternary Pump User Manual LAN Configuration What You Have To Do First TCP/IP Parameter Configuration Configuration Switch Initialization Mode Selection Dynamic Host Configuration Protocol (DHCP) General Information (DHCP) Setup (DHCP) Link Configuration Selection Automatic configuration with Bootp About Agilent BootP Service...
Page 260: What You Have To Do First
PC network card using a crossover network cable (point- to- point) • a hub or switch using a standard LAN cable. MAC label LAN interface Figure 37 Location of LAN interfaces and MAC label 1290 Infinity Quaternary Pump User Manual...
Page 261: Tcp/Ip Parameter Configuration
TCP/IP parameters after power- on. The parameters may be derived from a Bootp cycle, non- volatile memory or initialized with known default values. The initialization mode is selected by the configuration switch, see Table 14 on page 263. 1290 Infinity Quaternary Pump User Manual...
Page 262: Configuration Switch
Initialization (‘Init’) Mode Bootp, all switches down. For details see “Initialization Mode Selection” on page 263 Link Configuration speed and duplex mode determined by auto-negotiation, for details see “Link Configuration Selection” on page 270 1290 Infinity Quaternary Pump User Manual...
Page 263: Initialization Mode Selection
They are not stored to the non- volatile memory of the module. Therefore, the parameters are lost with the next power cycle of the module. Figure 39 Bootp (Principle) 1290 Infinity Quaternary Pump User Manual...
Page 264 Use the initialization mode Bootp & Store carefully, because writing to the non-volatile N O T E memory takes time. Therefore, when the module shall obtain its parameters from a Bootp Server every time it is powered on, the recommended initialization mode is Bootp! 1290 Infinity Quaternary Pump User Manual...
Page 265 Using the default address in your local area network may result in network problems. Take N O T E care and change it to a valid address immediately. Table 15 Using Default Parameters IP address: 192.168.254.11 Subnet Mask: 255.255.255.0 Default Gateway not specified 1290 Infinity Quaternary Pump User Manual...
Page 266 In the Using Default mode, the parameters stored in the memory of the module are not N O T E cleared automatically. If not changed by the user, they are still available, when switching back to the mode Using Stored. 1290 Infinity Quaternary Pump User Manual...
Page 267: Dynamic Host Configuration Protocol (Dhcp)
2 It may be necessary to fully qualify the hostname with the DNS suffix, e.g. 0030d3177321.country.company.com. 3 The DHCP server may reject the hostname proposed by the card and assign a name following local naming conventions. 1290 Infinity Quaternary Pump User Manual...
Page 268: Setup (Dhcp)
Interface Card or the main board of above mentioned modules. Table 16 G1369C LAN Interface Card (configuration switch on the card) SW 4 SW 5 SW 6 SW 7 SW 8 Initialization Mode DHCP 1290 Infinity Quaternary Pump User Manual...
Page 269 4 Configure your Control Software (e.g. Agilent ChemStation, Lab Advisor, Firmware Update Tool) and use MAC address as host name, e.g. 0030d3177321. The LC system should become visible in the control software (see Note in section “General Information (DHCP)” on page 267). 1290 Infinity Quaternary Pump User Manual...
Page 270: Link Configuration Selection
SW 5 Link Configuration speed and duplex mode determined by auto-negotiation manually set to 10 Mbps, half-duplex manually set to 10 Mbps, full-duplex manually set to 100 Mbps, half-duplex manually set to 100 Mbps, full-duplex 1290 Infinity Quaternary Pump User Manual...
Page 271: Automatic Configuration With Bootp
Agilent BootP Service is installed on a server or PC on the LAN to provide central administration of IP addresses for Agilent instruments on a LAN. The BootP service must be running TCP/IP network protocol and cannot run a DHCP server. 1290 Infinity Quaternary Pump User Manual...
Page 272: How Bootp Service Works
• Does the Firewall block the BootP service? Add the BootP service as an exception. • Is the LAN Interface using the BootP- mode instead of "Using Stored" or "Using Default" modes? 1290 Infinity Quaternary Pump User Manual...
Page 273: Installation Of Bootp Service
9 The Destination Folder selection screen appears. Install BootP to the default folder or click Browse to choose another location. Click Next. The default location for installation is: C:\Program Files\Agilent\BootPService\ 10 Click Install to begin installation. 1290 Infinity Quaternary Pump User Manual...
Page 274 This completes installation. 16 Start BootP Service in the Windows® services: On the Windows® desktop click right on Computer icon, select Manage > Services and Applications > Services. Select the Agilent BootP Service and click Start. 1290 Infinity Quaternary Pump User Manual...
Page 275: Two Methods To Determine The Mac Address
2 Read the MAC address from the label and record it. The MAC address is printed on a label on the rear of the module. Figure 36 on page 260 and Figure 37 on page 260. 3 Turn on the instrument. 1290 Infinity Quaternary Pump User Manual...
Page 276: Assigning Ip Addresses Using The Agilent Bootp Service
5 Close the log file before turning on another instrument. 6 Uncheck the Do you want to log BootP requests? box after configuring instruments to avoid having the logfile use up excessive disk space. 1290 Infinity Quaternary Pump User Manual...
Page 277 5 Make these entries for the instrument: • MAC address • Host name, Enter a Hostname of your choice. The Host Name must begin with "alpha" characters (i.e. LC1260) • IP address • Comment (optional) 1290 Infinity Quaternary Pump User Manual...
Page 278 11 Use the PING utility to verify connectivity by opening a command window and typing: Ping 192.168.254.11 for example. The Tab File is located at C:\Documents and Settings\All Users\Application Data\Agilent\BootP\TabFile 1290 Infinity Quaternary Pump User Manual...
Page 279: Changing The Ip Address Of An Instrument Using The Agilent Bootp Service
1 Select Start > All Programs > Agilent BootP Service and select Edit BootP Settings. The BootP Settings screen appears. 2 When the BootP Settings screen is first opened, it shows the default settings from installation. 1290 Infinity Quaternary Pump User Manual...
Page 280 1 In the Windows control panel, select Administrative Tools > Services. The Services screen appears, see Figure 48 on page 279. 2 Right- click Agilent BootP Service and select Start. 3 Close the Services and Administrative Tools screens. 1290 Infinity Quaternary Pump User Manual...
Page 281: Manual Configuration
Therefore, manual configuration can be done at any time. A power cycle is mandatory to make the stored parameters become the active parameters, given that the initialization mode selection switches are allowing it. Figure 50 Manual Configuration (Principle) 1290 Infinity Quaternary Pump User Manual...
Page 282: With Telnet
Handheld Controller, or the default IP address (see “Configuration Switch” on page 262). When the connection was established successfully, the module responds with the following: Figure 52 A connection to the module is made 1290 Infinity Quaternary Pump User Manual...
Page 283 Then press [Enter], where parameter refers to the configuration parameter you are defining, and value refers to the definitions you are assigning to that parameter. Each parameter entry is followed by a carriage return. 1290 Infinity Quaternary Pump User Manual...
Page 284 IP setting to Initialization mode is Using Stored active TCP/IP settings stored TCP/IP settings in non-volatile memory connected to PC with controller software (e.g. Agilent ChemStation), here not connected Figure 55 Telnet - Change IP settings 1290 Infinity Quaternary Pump User Manual...
Page 285 If the Initialization Mode Switch is changed now to “Using Stored” mode, the instrument N O T E will take the stored settings when the module is re-booted. In the example above it would be 134.40.27.99. 1290 Infinity Quaternary Pump User Manual...
Page 286: With The Instant Pilot (G4208A)
Figure 57 Instant Pilot - LAN Configuration 5 Press the Edit button (only visible if not in Edit mode), perform the required changes and press the Done button. 6 Leave the screen by clicking Exit. 1290 Infinity Quaternary Pump User Manual...
Page 287: Pc And User Interface Software Setup Setup
This procedure describes the change of the TCP/IP settings on your PC to match the module’s default parameters in a local configuration (see also “Initialization Mode Selection” on page 263). Figure 58 Changing the TCP/IP settings of the PC 1290 Infinity Quaternary Pump User Manual...
Page 288: User Interface Software Setup
LAN Configuration PC and User Interface Software Setup Setup User Interface Software Setup Install you user interface software according the provided User Interface Software Setup Guide. 1290 Infinity Quaternary Pump User Manual...
Page 289: Appendix
1290 Infinity Quaternary Pump User Manual Appendix General Safety Information The Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Radio Interference Sound Emission Agilent Technologies on Internet This chapter provides additional information on safety, legal and web. Agilent Technologies...
Page 290: General Safety Information
C A U T I O N alerts you to situations that could cause loss of data, or damage of equipment. ➔ Do not proceed beyond a caution until you have fully understood and met the indicated conditions. 1290 Infinity Quaternary Pump User Manual...
Page 291 Agilent Technologies assumes no liability for the customer’s failure to comply with these requirements. Ensure the proper usage of the equipment.
Page 292 When working with solvents, observe appropriate safety procedures (for example, goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet by the solvent vendor, especially when toxic or hazardous solvents are used. 1290 Infinity Quaternary Pump User Manual...
Page 293: The Waste Electrical And Electronic Equipment (Weee) Directive (2002-96-Ec)
“Monitoring and Control instrumentation” product. Do not dispose off in domestic household waste To return unwanted products, contact your local Agilent office, or see www.agilent.com for more information. 1290 Infinity Quaternary Pump User Manual...
Page 294: Radio Interference
Appendix Radio Interference Radio Interference Never use cables other than the ones supplied by Agilent Technologies to ensure proper functionality and compliance with safety or EMC regulations. Test and Measurement If test and measurement equipment is operated with equipment unscreened cables and/or used for measurements on open set- ups, the user has to assure that under operating conditions the radio interference limits are still met within the premises.
Page 295: Sound Emission
This product has a sound pressure emission (at the operator position) < 70 dB. • Sound Pressure Lp < 70 dB (A) • At Operator Position • Normal Operation • According to ISO 7779:1988/EN 27779/1991 (Type Test) 1290 Infinity Quaternary Pump User Manual...
Page 296: Agilent Technologies On Internet
Appendix Agilent Technologies on Internet Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com 1290 Infinity Quaternary Pump User Manual...
Page 297 Bootp early maintenance feedback two stack & Store error messages cover parts automatic configuration compensation sensor open initialization modes 1290 Infinity Quaternary Pump User Manual...
Page 298 1290 Infinity Quaternary Pump User Manual...
Page 299: Features
LAN system tool kit maximum stroke too short 1290 Infinity Quaternary Pump User Manual...
Page 300 1290 Infinity Quaternary Pump User Manual...
Page 301 Index 1290 Infinity Quaternary Pump User Manual...
Page 302 In This Book This manual contains technical reference information about the Agilent 1290 Infinity Quaternary Pump G4204A. The manual describes the following: • Introduction, • Site requirements and specifications, • installation, • configuration, • using and optimizing, • troubleshooting and diagnostic, •...

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G4204a

Agilent Technologies 1290 User Manual

Table of Contents

Introduction Features

Site Requirements and Specifications

3 Installing the Module

4 Using the Pump

5 How to Optimize the Performance of Your Module

6 Troubleshooting and Diagnostics

7 Error Information

9 Maintenance

10 Parts and Materials

11 Identifying Cables

12 Hardware Information

13 LAN Configuration

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Summary of Contents for Agilent Technologies 1290