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1290 Infinity II
Agilent Technologies 1290 Infinity II Manuals
Manuals and User Guides for Agilent Technologies 1290 Infinity II. We have
10
Agilent Technologies 1290 Infinity II manuals available for free PDF download: User Manual, Technical Note
Agilent Technologies 1290 Infinity II User Manual (291 pages)
High-Speed Pumps
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 28.98 MB
Table of Contents
Table of Contents
5
Introduction
9
Agilent 1290 Infinity II High-Speed Pump
10
Product Description
10
Features
11
Agilent 1290 Infinity II Bio High-Speed Pump
12
Product Description
12
Features
13
Pump Principle
14
Leak and Waste Handling
16
Leak Sensor
19
Waste Concept
20
Site Requirements and Specifications
21
Site Requirements
22
Physical Specifications
25
Physical Specifications Agilent 1290 Infinity II High-Speed Pump (G7120A)
25
Physical Specifications Agilent 1290 Infinity II Bio High-Speed Pump (G7132A)
26
Performance Specifications
27
Performance Specifications Agilent 1290 Infinity II High-Speed Pump (G7120A)
27
Performance Specifications Agilent 1290 Infinity II Bio High-Speed Pump (G7132A)
30
Using the Pump
33
Magnets
34
Turn On/Off
35
Status Indicators
37
Best Practices
38
Daily / Weekly Tasks
38
Power up / Shut-Down the Pump
39
Prepare the Pump
40
Seal Wash
44
How to Deal with Solvents
44
Purging the Pump
45
Recommendations for Bio-Compatible and Bio-Inert Systems
47
Recommendations for Degassers
49
Solvent Information
50
Materials in Flow Path (G7120A)
50
Materials in Flow Path (G7132A)
51
General Information about Solvent/Material Compatibility
52
Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps
58
Normal Phase Applications
59
Solvent Handling
61
Algae Growth in HPLC Systems
64
How to Prevent And-Or Reduce the Algae Problem
64
Setting up the Pump with the Instrument Control Interface
65
Overview
65
Instrument Configuration
65
The Pump User Interface (Dashboard Panel)
67
Control Settings
70
Method Parameter Settings
71
Agilent Local Control Modules
75
Preparing the Pump
76
Capillary Coding Guide
77
Installing Capillaries
80
Optimizing Performance
85
Delay Volume and Extra-Column Volume
86
Delay Volume
86
How to Configure the Optimum Delay Volume
87
How to Achieve Higher Resolution
88
Using Solvent Calibration Tables
91
How It Works
91
How to Import the Latest Solvent Calibration Tables
92
Recommendations for Setting up Methods Using Salt-Containing Eluents
95
Troubleshooting and Diagnostics
96
User Interfaces
97
Agilent Lab Advisor Software
98
Pump Leak Rate Test
99
Troubleshooting the Pump Leak Rate Test
102
System Pressure Test
104
Error Information
106
What Are Error Messages
108
General Error Messages
109
Timeout
109
Shutdown
110
Remote Timeout
111
Lost CAN Partner
111
Leak Sensor Short
112
Leak Sensor Open
113
Compensation Sensor Open
113
Compensation Sensor Short
114
Fan Failed
114
Leak
115
Open Cover
115
Cover Violation
116
Pump Error Messages
117
Pressure of Binary Pump above Upper Limit
117
Pressure below Lower Limit
118
Target Pressure Not Reached for Binary Pump Degasser
118
Degasser's Pressure Limit Violation
119
Solvent Counter Exceeded Limit
119
Waste Counter Limit Exceeded
120
Flow Rate Limit Exceeded
120
Binary Pump Shutdown During Analysis
121
Reading the Pump Encoder Tag Failed
121
Writing the Pump Encoder Tag Failed
122
Pump Drive Blocked or Encoder Failed
122
Drive Current too Low
123
Drive Encoder Failed
123
Drive Current too High
123
Drive Timeout
124
Overcurrent of Pump Drive
124
Overcurrent of Solvent Selection Valve (SSV)
124
Deliver Underrun
125
Defect Connection between Main Board and Pump Drive Encoder
125
Pump Drive Encoder Defect
125
Purge Valve Failed
126
Reading of Purge Valve Tag Failed
126
Pump Drive Encoder Rollover
126
Drive Position Limit
127
Insufficient Power of Drive Encoder LED
127
Drive Encoder Error
127
Writing the Purge Valve Tag Failed
128
Current of Primary Pump Drive too High
128
Current of Secondary Pump Drive too High
129
Unknown Purge Valve Type
129
Pump Drive Encoder Error
129
Pump Drive Error
130
Pump Drive Stroke Blocked
130
Pump Drive Stop Not Found
131
Pressure Sensor Calibration Wrong or Missing
131
Seal Wash Pump was Missing When Tried to Turn on
132
Invalid Degasser Pressure Signal
132
Maintenance
133
Introduction to Maintenance
135
Warnings and Cautions
138
Overview of Maintenance
140
Cleaning the Module
141
Install Fittings and Capillaries
142
Remove and Install Doors
143
Replace the Shutoff Valve Panel
145
Replace the Pressure Sensor
146
Replace the Solvent Selection Valve (SSV)
148
Change Configuration or Replace the Jet Weaver
150
Replace the Seal Wash Pump
153
Replace the Inlet Valve (G7120A)
154
Replace the Inlet Valve (G7132A)
156
Release a Stuck Inlet Valve
158
Remove the Pump Head Assembly (G7120A)
160
Remove the Pump Head Assembly (G7132A)
163
Pump Head Maintenance (Tool Free)
166
Disassemble Longlife Pump Heads (G7120A)
167
Disassemble Longlife Pump Heads (G7132A)
171
Replace the Heat Exchanger (G7120A)
175
Replace the Heat Exchanger (G7132A)
177
Assemble Longlife Pump Heads (G7120A)
179
Assemble Longlife Pump Heads (G7132A)
185
Install the Pump Head Assembly (G7120A)
191
Install the Pump Head Assembly (G7132A)
193
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Agilent Technologies 1290 Infinity II User Manual (244 pages)
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 24.28 MB
Table of Contents
Table of Contents
5
Introduction
9
Introduction
10
Pump Principle
11
Leak and Waste Handling
13
Leak Sensor
16
Waste Concept
17
Product Description
10
Site Requirements and Specifications
19
Site Requirements
20
Site Requirements
21
Physical Specifications
23
Performance Specifications
24
3 Using the Pump
27
Magnets
28
Turn On/Off
29
Status Indicators
31
Best Practices
32
Daily / Weekly Tasks
32
Power up / Shut-Down the Pump
33
Prepare the Pump
33
How to Deal with Solvents
34
Purging the Pump
35
Solvent Information
37
Solvent Recommendation for Agilent 1290 Infinity and 1290 Infinity II and 1260 Infinity II Flexible Pumps
44
Normal Phase Applications
45
Solvent Handling
46
Algae Growth in HPLC Systems
49
How to Prevent And-Or Reduce the Algae Problem
49
Setting up the Pump with the Instrument Control Interface
50
Overview
50
Instrument Configuration
50
The Pump User Interface (Dashboard Panel)
52
Control Settings
55
Method Parameter Settings
55
Agilent Local Control Modules
60
4 Optimizing Performance
63
Delay Volume and Extra-Column Volume
64
Delay Volume
64
How to Configure the Optimum Delay Volume
65
How to Achieve Higher Resolution
67
Using Solvent Calibration Tables
70
5 Troubleshooting and Diagnostics
71
User Interfaces
72
Agilent Lab Advisor Software
73
Pump Leak Rate Test
74
Troubleshooting the Pump Leak Rate Test
77
System Pressure Test
79
6 Error Information
81
What Are Error Messages
83
General Error Messages
84
Timeout
84
Shutdown
85
Remote Timeout
86
Lost CAN Partner
87
Leak Sensor Short
88
Leak Sensor Open
89
Compensation Sensor Open
90
Compensation Sensor Short
90
Fan Failed
91
Leak
92
Open Cover
93
Cover Violation
93
Pump Error Messages
94
Pressure of Binary Pump above Upper Limit
94
Pressure below Lower Limit
94
Target Pressure Not Reached for Binary Pump Degasser
95
Degasser's Pressure Limit Violation
95
Solvent Counter Exceeded Limit
96
Waste Counter Limit Exceeded
96
Flow Rate Limit Exceeded
97
Binary Pump Shutdown During Analysis
97
Reading the Pump Encoder Tag Failed
98
Writing the Pump Encoder Tag Failed
98
Pump Drive Blocked or Encoder Failed
99
Drive Current too Low
99
Drive Encoder Failed
99
Drive Current too High
100
Drive Timeout
100
Overcurrent of Pump Drive
101
Overcurrent of Solvent Selection Valve (SSV)
101
Deliver Underrun
101
Defect Connection between Main Board and Pump Drive Encoder
102
Pump Drive Encoder Defect
102
Purge Valve Failed
103
Reading of Purge Valve Tag Failed
103
Pump Drive Encoder Rollover
104
Drive Position Limit
104
Insufficient Power of Drive Encoder LED
104
Drive Encoder Error
105
Writing the Purge Valve Tag Failed
105
Current of Primary Pump Drive too High
106
Current of Secondary Pump Drive too High
106
Unknown Purge Valve Type
107
Pump Drive Encoder Error
107
Pump Drive Error
107
Pump Drive Stroke Blocked
108
Pump Drive Stop Not Found
108
Pressure Sensor Calibration Wrong or Missing
109
Seal Wash Pump was Missing When Tried to Turn on
109
Invalid Degasser Pressure Signal
110
7 Maintenance
111
Introduction to Maintenance
112
Warnings and Cautions
114
Overview of Maintenance
116
Cleaning the Module
117
Install Fittings and Capillaries
118
Remove and Install Doors
119
Replace the Shutoff Valve Panel
121
Replace the Pressure Sensor
123
Replace the Solvent Selection Valve (SSV)
125
Change Configuration or Replace the Jet Weaver
127
Replace the Seal Wash Pump
130
Replace the Inlet Valve
131
Release a Stuck Inlet Valve
133
Remove the Pump Head Assembly
135
Pump Head Maintenance (Tool Free)
138
Disassemble Longlife Pump Heads
139
Replace the Heat Exchanger
144
Assemble Longlife Pump Heads
146
Install the Pump Head Assembly
153
Replace the Outlet Valve
155
Replace the Purge Valve Head
157
Replace Parts of the High Pressure Filter Assembly
160
Replace the Module Firmware
162
Prepare the Pump Module for Transport
163
Agilent Technologies 1290 Infinity II User Manual (230 pages)
Variable Wavelength Detector
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 5.02 MB
Table of Contents
Table of Contents
5
Introduction to the Variable Wavelength Detector
9
Introduction to the Detector
10
Product Description
11
Optical System Overview
12
Optical System Overview
13
Dual-Wavelength Mode
17
Leak and Waste Handling
18
Leak and Waste Handling
19
Waste Concept
20
Operating Principle
21
Operating Principle
22
Site Requirements and Specifications
23
Site Requirements
24
Physical Specifications
27
Performance Specifications G7114B
28
Lamp
28
3 Using the Module
31
Magnets
32
Turn On/Off
33
Status Indicators
34
Instrument Configuration
35
Set up the Detector with Agilent Open Lab Chemstation
37
The Detector User Interface
38
Detector Control Settings
40
Method Parameter Settings
41
Scanning with the VWD
45
4 Preparing the Module
47
Leak and Waste Handling
48
Waste Concept
49
Leak and Waste Handling
49
Setting up an Analysis
50
Before Using the System
50
Requirements and Conditions
52
Preparing the Detector
54
Preparing the HPLC System
54
Running the Sample and Verifying the Results
56
Solvent Information
57
5 Optimizing the Detector
63
Introduction
64
Match the Flow Cell to the Column
65
Set the Detector Parameters
68
Warm up of the Detector
69
Troubleshooting and Diagnostics
71
Available Tests Versus Interfaces
72
Introduction
72
Agilent Lab Advisor Software
73
7 Error Information
75
What Are Error Messages
77
General Error Messages
78
Timeout
78
Shutdown
78
Remote Timeout
79
Lost CAN Partner
80
Leak
80
Leak Sensor Open
81
Leak Sensor Short
81
Compensation Sensor Open
82
Compensation Sensor Short
82
Fan Failed
83
Open Cover
83
ERI Messages
84
Detector Error Messages
85
UV Lamp: no Current
85
UV Lamp: no Voltage
86
Ignition Failed
86
No Heater Current
87
Wavelength Calibration Setting Failed
88
Wavelength Holmium Check Failed
89
Grating or Filter Motor Errors
90
Wavelength Test Failed
91
Cutoff Filter Doesn't Decrease the Light Intensity at 250 Nm
91
ADC Hardware Error
92
Illegal Temperature Value from Sensor on Main Board
92
Illegal Temperature Value from Sensor at Air Inlet
93
Heater at Fan Assembly Failed
93
8 Test Functions
95
Introduction
96
Intensity Test
97
Intensity Test Evaluation
98
Intensity Test Failed
99
Cell Test
100
Cell Test Failed
101
Wavelength Verification-Calibration
102
When to Calibrate the Detector
102
ASTM Drift and Noise Test
104
Quick Noise Test
105
Dark Current Test
107
Dark Current Test Failed
108
Holmium Oxide Test
109
When to Do the Test
109
Interpreting the Results
110
Holmium Oxide Test Failed
111
D/A Converter (DAC) Test
112
D/A Converter Test Evaluation
114
Other Lab Advisor Functions
115
Emfs - Early Maintenance Feature
115
9 Maintenance
117
Introduction to Maintenance
118
Warnings and Cautions
118
Overview of Maintenance
120
Cleaning the Module
121
Remove and Install the Doors
122
Replace the Deuterium Lamp
123
Replace the Flow Cell / Cuvette Holder
126
Repairing the Flow Cells
128
Using the Cuvette Holder
131
Correcting Leaks
133
Replacing Leak Handling System Parts
135
Replace the Module Firmware
136
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Agilent Technologies 1290 Infinity II User Manual (222 pages)
Variable Wavelength Detectors
Brand:
Agilent Technologies
| Category:
Security Sensors
| Size: 3.96 MB
Table of Contents
Table of Contents
5
1 Introduction to the Variable Wavelength Detector
9
Introduction to the Detector
10
Product Description
11
Product Description G7114A
11
Product Description G7114B
12
Optical System Overview
13
Flow Cell
14
Entrance Slit Assembly
15
Lamp
15
Source Lens Assembly
15
Filter Assembly
16
Beam Splitter Assembly
17
Grating Assembly
17
Mirror Assemblies M1 and M2
17
Photo Diode ADC (Analog-To-Digital Converter)
17
Dual-Wavelength Mode
18
Photo Diodes Assemblies
17
Leak and Waste Handling
19
Leak Sensor
23
Waste Concept
23
Operating Principle
24
2 Site Requirements and Specifications
25
Site Requirements
26
Physical Specifications
29
Performance Specifications
30
Specifications
30
Specification Conditions
34
3 Using the Module
35
Magnets
36
Turn On/Off
37
Status Indicators
39
Instrument Configuration
40
Set up the Detector with Agilent Open Lab Chemstation
42
The Detector User Interface
43
Detector Control Settings
45
Method Parameter Settings
46
Scanning with the VWD
50
Agilent Local Control Modules
52
4 Preparing the Module
54
Leak and Waste Handling
55
Waste Concept
56
Setting up an Analysis
57
Before Using the System
57
Requirements and Conditions
59
Preparing the Detector
61
Preparing the HPLC System
61
Running the Sample and Verifying the Results
63
Solvent Information
64
5 Optimizing the Detector
69
Introduction
70
Match the Flow Cell to the Column
71
Set the Detector Parameters
74
Warm up of the Detector
75
6 Troubleshooting and Diagnostics
77
Available Tests Versus Interfaces
78
Agilent Lab Advisor Software
79
7 Error Information
80
What Are Error Messages
81
General Error Messages
82
Timeout
82
Shutdown
83
Remote Timeout
84
Lost CAN Partner
84
Leak
85
Leak Sensor Open
85
Leak Sensor Short
86
Compensation Sensor Open
86
Compensation Sensor Short
87
Fan Failed
87
Open Cover
88
ERI Messages
88
Detector Error Messages
89
UV Lamp: no Current
89
UV Lamp: no Voltage
90
Ignition Failed
90
No Heater Current
91
Wavelength Calibration Setting Failed
92
Wavelength Holmium Check Failed
93
Grating or Filter Motor Errors
94
Wavelength Test Failed
94
Cutoff Filter Doesn't Decrease the Light Intensity at 250 Nm
95
ADC Hardware Error
95
Illegal Temperature Value from Sensor on Main Board
96
Illegal Temperature Value from Sensor at Air Inlet
96
Heater at Fan Assembly Failed
97
Heater Power at Limit
97
Cover Violation
98
8 Test Functions
99
Introduction
100
Intensity Test
105
Intensity Test Evaluation
106
Intensity Test Failed
107
Cell Test
108
Cell Test Failed
109
Wavelength Verification-Calibration
110
When to Calibrate the Detector
110
ASTM Drift and Noise Test
112
Quick Noise Test
113
Dark Current Test
115
Dark Current Test Failed
116
Holmium Oxide Test
117
When to Do the Test
117
Interpreting the Results
118
Holmium Oxide Test Failed
119
D/A Converter (DAC) Test
120
D/A Converter Test Evaluation
122
Emfs - Early Maintenance Feature
123
Other Lab Advisor Functions
123
9 Maintenance
124
Introduction to Maintenance
125
Warnings and Cautions
126
Overview of Maintenance
128
Cleaning the Module
129
Remove and Install the Doors
130
Replace the Deuterium Lamp
132
Replace the Flow Cell / Cuvette Holder
135
Repair the Flow Cells
137
Using the Cuvette Holder
141
Correcting Leaks
143
Replace Leak Handling System Parts
145
Replace the Module Firmware
146
Agilent Technologies 1290 Infinity II User Manual (213 pages)
Preparative Open-Bed Sampler/Collector
Brand:
Agilent Technologies
| Category:
Samplers
| Size: 3.84 MB
Table of Contents
Table of Contents
5
1 Introduction
8
Intended Use
9
Product Description
10
Features
11
Overview of the Module
12
Leak and Waste Concept
14
Leak Sensor
15
2 Site Requirements and Specifications
17
Site Requirements
18
Exhaust and Vapour Management
21
Waste Management
22
Physical Specifications
23
Performance Specifications
24
3 Using the Sampler/Collector
30
Warnings and Cautions
31
Solvent Information
32
Solvent Compatibility
36
Wetted Materials
36
General Information about Solvent/Material Compatibility
38
Turn On/Off
43
Status Indicators
44
Drawer Status Indicator
45
Install a 1/16'' Preparative Loop
46
Install the Preparative Loop
46
Install a 1/8'' Preparative Loop
47
Install or Replace the Analytical Loop
50
Exchange Drawers
51
Exchange Containers
53
Replace the Fraction Collection Inlet/Outlet Tubings
55
Configuration and Operation of the Open-Bed Sampler/Collector
60
Delay Volumes and Delay Calibration
60
Perfom a Delay Calibration Run in Openlab CDS Chemstation Edition
62
Help
63
Delay Evaluation
66
Setting up a Fraction Collector Method
68
Prepare the Module for Transportation
73
4 Preparing the Sampler/Collector
76
Best Practices
77
Daily Startup Routine
77
Prepare the Sampler/Collector
78
Regular Inspections
78
Using the Fraction Collector
78
Capillary Color Coding Guide
79
Swage Fittings
80
Instrument Configuration
82
Overview
82
Setting up the Sampler/Collector with the Instrument Control Interface
82
Preparative Sampler User Interface (Dashboard Panel)
88
Preparative Sampler Control Parameters
90
Fraction Collector User Interface (Dashboard Panel)
91
Preparative Sampler Method Parameter Settings
93
Plug Settings
98
Advanced Settings
105
Injection Path Cleaning
107
Dilution
108
Fraction Collector Method Parameter Settings
110
Advanced Settings
113
Timetable Settings
115
Pooling
118
Challenging Samples
119
Analytical to Preparative Switching Procedure
120
Recommended Vials, Well Plates, and Containers
121
5 Troubleshooting and Diagnostics
123
User Interfaces
124
Agilent Lab Advisor Software
125
6 Error Information
126
What Are Error Messages General Error Messages
126
Timeout
128
Shutdown
129
Lost CAN Partner
130
Remote Timeout
130
Leak Sensor Open
131
Leak Sensor Short
131
Compensation Sensor Open
132
Compensation Sensor Short
132
Fan Failed
133
Leak
133
7 Maintenance
134
Introduction to Maintenance
135
Warnings and Cautions
136
Cleaning the Module
138
Overview of Maintenance
139
Install and Remove the Top Fume Hood
140
Clean the Leak Pan
142
Replace the Dripping Adapter for the Fraction Valve
143
Replace the Rotor Seal
145
Replace the Stator
149
Replace the Two Peristaltic Pump Cartridges
151
Replace the Needle Wash Plug Assembly
153
Install or Replace the Sampling Unit Tubing Kit
156
Install or Replace the Solvent Distribution Tubing
157
Install or Replace the Needle Tubing
159
Replace the Module Firmware
161
Agilent Technologies 1290 Infinity II User Manual (158 pages)
Preparative Open-Bed Fraction Collector
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 8.15 MB
Table of Contents
Table of Contents
5
1 Introduction
8
Intended Use
9
Product Description
10
Features
11
Overview of the Module
12
Fraction Collector Principle
13
Leak and Waste Concept
14
Leak Sensor
15
2 Site Requirements and Specifications
16
Site Requirements
17
Exhaust and Vapour Management
20
Waste Management
21
Physical Specifications
22
Performance Specifications
23
3 Using the Fraction Collector
27
Warnings and Cautions
28
Solvent Information
29
Recommended Wash Solvents
30
Material Information
31
Turn On/Off
36
Status Indicators
37
Drawer Status Indicator
38
Exchange Drawers
39
Exchange Containers
41
Replace Inlet/Waste Tubings
43
Configuration and Operation of the Open Bed Fraction Collector
47
Delay Volumes and Delay Calibration
47
Perfom a Delay Calibration Run in Openlab CDS Chemstation Edition
49
Help
50
Delay Evaluation
53
Setting up a Fraction Collector Method
56
Prepare the Module for Transportation
61
4 Preparing the Fraction Collector
63
Best Practices
64
Power up / Shut down
64
Prepare the Fraction Collector
64
Regular Inspections
64
Using the Fraction Collector
64
Capillary Color Coding Guide
65
Swage Fittings
66
Instrument Configuration
68
Overview
68
Setting up the Fraction Collector with the Instrument Control Interface
68
Fraction Collector User Interface (Dashboard Panel)
72
Method Parameter Settings
74
Advanced Settings
77
Timetable Settings
79
Pooling
82
5 Troubleshooting and Diagnostics
83
User Interfaces
84
Agilent Lab Advisor Software
85
6 Error Information
86
What Are Error Messages General Error Messages
86
Timeout
88
Shutdown
89
Lost CAN Partner
90
Remote Timeout
90
Leak Sensor Short
91
Compensation Sensor Open
92
Leak Sensor Open
92
Compensation Sensor Short
93
Fan Failed
93
Leak
94
7 Maintenance
95
Introduction to Maintenance
96
Warnings and Cautions
97
Cleaning the Module
99
Overview of Maintenance
100
Install and Remove the Top Fume Hood
101
Clean the Leak Pan
103
Replace the Dripping Adapter for the Fraction Valve
104
Replace the Module Firmware
106
Agilent Technologies 1290 Infinity II User Manual (146 pages)
Preparative Open-Bed Fraction Collector
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 2.44 MB
Table of Contents
Table of Contents
5
1 Introduction
9
Product Description
10
Features
11
Overview of the Module
12
Fraction Collector Principle
13
Leak and Waste Concept
14
2 Site Requirements and Specifications
15
Site Requirements
16
Physical Specifications
19
Performance Specifications
20
3 Using the Fraction Collector
23
Solvent Information
24
Turn On/Off
26
Status Indicators
27
Drawer Status Indicator
28
Exchange Drawers
29
Exchange Containers
31
Replace Inlet/Waste Tubings
32
4 Preparing the Fraction Collector
37
Best Practices
38
Regular Inspections
38
Power up / Shut down
38
Prepare the Fraction Collector
38
Using the Fraction Collector
38
Solvent Information
39
Material Information
40
Capillary Color Coding Guide
45
Installing Capillaries
46
Setting up the Fraction Collector with the Instrument Control Interface
49
Overview
49
Instrument Configuration
49
Fraction Collector User Interface (Dashboard Panel)
53
Method Parameter Settings
55
Advanced Settings
58
Timetable Settings
60
Pooling
63
5 Troubleshooting and Diagnostics
65
User Interfaces
66
Agilent Lab Advisor Software
67
6 Error Information
69
What Are Error Messages
70
General Error Messages
71
Timeout
71
Shutdown
72
Remote Timeout
73
Lost CAN Partner
74
Leak Sensor Short
75
Leak Sensor Open
75
Compensation Sensor Open
76
Compensation Sensor Short
76
Fan Failed
77
Leak
77
7 Maintenance
79
Introduction to Maintenance
80
Warnings and Cautions
81
Cleaning the Module
83
Overview of Maintenance
84
Install and Remove the Top Fume Hood
85
Clean the Leak Pan
87
Prepare the Module for Transportation
88
Replace the Module Firmware
90
8 Parts for Maintenance and Repair
91
Supported Containers
92
List of Recommended Fraction Tubes
93
Fraction Collector Accessory Kit
94
Tubing Kits
95
Top Fume Hood Kit
97
9 Identifying Cables
99
Cable Overview
100
Analog Cables
102
Remote Cables
104
CAN/LAN Cables
108
Cables
109
Usb
110
Agilent Technologies 1290 Infinity II User Manual (122 pages)
Evaporative Light Scattering Detector
Brand:
Agilent Technologies
| Category:
Measuring Instruments
| Size: 3.83 MB
Table of Contents
Table of Contents
5
1 Introduction to the Detector
7
Introduction to the ELSD
8
System Overview
9
Basic Principles of Operation
9
Operational Parameters
12
Overview of ELS Detector
13
2 Site Requirements and Specifications
17
Pre-Installation Requirements
18
Laser Safety
19
Power Considerations
19
Site Requirements
19
Physical Specifications
22
Performance Specifications
23
Specifications
23
Specification Conditions
24
3 Installing the Module
25
Unpacking the Module
26
Delivery Checklist
27
Installing the Module
28
Connecting the Detector to Your LC System
28
Checking Operation of the ELS Detector
31
4 LAN Configuration
33
4 LAN Configuration What You Have to Do First
34
TCP/IP Parameter Configuration
35
Configuration Using Instrument Front Panel
36
Configuration Using Web Browser
37
With Telnet
40
PC and Agilent Openlab Chemstation and Ezchrom Setup
43
PC Setup for Local Configuration
43
Agilent Chemstation Setup
46
5 Using the Module
49
Before Using the Detector
50
Instrument Controls
51
Display Screen
51
Keypad
51
Main Menu Bar
52
Sub-Menu Screen
52
Status Mode
53
Error Conditions
54
Clearing an Error
54
Operational Parameters
55
Method
55
Evaporator Temperature
55
Nebuliser Temperature
56
Evaporator Gas Flow
56
Response Time (Smoothing)
57
Power Mode
57
Data Output Rate (Hz)
57
LAN (TCP/IP Settings)
58
Controlling the ELSD During an Injection
59
Real-Time Operation
59
Creating a Real-Time Program
59
Starting and Stopping Real-Time Control
60
Controlling the ELSD Within Chemstation or Ezchrom
62
General Considerations
63
Solvent Recommendations
64
Sample Preparation
64
Column Considerations
64
Transferring ELSD Temperature Methods
66
6 Optimizing Performance
67
Do's and Don'ts of ELS Detection
68
Location of the Detector Module
69
Pumping Systems
70
Mobile Phase Priming
71
7 Troubleshooting and Diagnostics
73
Troubleshooting
74
Troubleshooting an HPLC System
75
General Problems
76
Baseline Noise
76
Baseline Spikes
77
Low Sensitivity
77
Spiky Peak Tops but Flat Baseline
78
Large Baseline Offset
78
Peak Tailing
79
Instrument Fails to Zero
79
No Power
79
No Response (Completely Flat Baseline)
80
Temperature Error as Soon as Instrument Powered on
80
Display Not On, but Power Connected
80
Cooled Evaporator Temperature Reads Zero at Start-Up and Cannot be Changed
81
Unit
81
Cooled Evaporator will Not Reach Low Temperature E.g. 10 °C
81
High Back-Pressure from Detector
82
Agilent Technologies 1290 Infinity II User Manual (120 pages)
InfinityLab LC Series MS Flow Modulator
Brand:
Agilent Technologies
| Category:
Laboratory Equipment
| Size: 5.5 MB
Table of Contents
Table of Contents
5
Introduction
7
1290 Infinity II MS Flow Modulator
8
Features (G7170B)
9
Leak and Waste (G7170B)
10
Operating Principle
11
Site Requirements and Specifications
13
Site Requirements
14
Physical Specifications
17
Performance Specifications
18
3 Installing the Module
19
Unpacking the Module
20
Installation of the MS Flow Modulator
21
Assembling and Installing the Leak Tray and Leak Sensor
22
Mounting the MS Flow Modulator to an Instrument
23
Mount the MS Flow Modulator to the 1290 Infinity II Preparative Column Compartment
24
Install the MS Flow Modulator
25
Install the Valve Head and Connecting Capillaries
27
4 Using the Module
31
Overview
32
Solvent Information
33
Material Information
35
Status Indicator
40
Leak and Waste Handling
41
Waste Concept
42
Configure the Flow Modulator
43
Troubleshooting and Diagnostics
47
User Interfaces
48
Agilent Lab Advisor Software
49
6 Error Information
51
What Are Error Messages
52
General Error Messages
53
Timeout
53
Shutdown
54
Remote Timeout
55
Lost CAN Partner
55
Leak Sensor Short
56
Leak Sensor Open
56
Leak
57
Module Specific Error Messages
58
Initialization of Valve Failed
58
Valve Switching Failed
59
Valve Tag Violation
59
7 Maintenance
61
Introduction to Maintenance
62
Warnings and Cautions
63
Cleaning the Module
64
Replacing the Fuses of the Infinity Valve Drive
65
Replace Rotor and Stator
67
Replace Valve Heads
70
Replacing the Module Firmware
74
Module Specific Information
75
Parts and Materials
77
Accessory Kit for the Flow Modulator
78
Optional Parts
80
Agilent Technologies 1290 Infinity II Technical Note (40 pages)
Long Life Pump Head
Brand:
Agilent Technologies
| Category:
Water Pump
| Size: 2.85 MB
Table of Contents
Table of Contents
1
Introduction
2
Long Life Upgrade Kit (Binary and High Speed Pumps)
3
Long Life Upgrade Kit (Quaternary and Flexible Pumps)
3
Remove Pump Heads (Binary and High Speed Pumps)
4
Remove Pump Heads (Quaternary and Flexible Pumps)
7
Replace the Pump Drives (Binary and High Speed Pumps)
10
Replace the Pump Drive (Quaternary and Flexible Pumps)
12
Pump Head Maintenance (Tool Free)
13
Install Long Life Pump Heads (Binary and High Speed Pumps)
24
Install Long Life Pump Heads (Quaternary and Flexible Pumps)
26
Pump Head Parts
28
Seal Wash Function
33
Install the Seal Wash Function (Binary Pump)
33
Install the Seal Wash Function (Quaternary Pump)
35
Seal Wash Upgrade Kit (Binary Pump)
38
Seal Wash Upgrade Kit (G4204A)
39
Upgrade the Valve Support (G4204A Only)
40
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