HP 5890 Series II Plus Reference Manual page 239

Test Sample Chromatograms
Test sample chromatograms
Figure 10-15.
Detector Type FPD
Temp 200 DEGREES C
Inlet Type DED ON-COL CAP
Oven Track
Temp
Operating Mode
Purge Time On
Purge Time Off
Oven Temp Programmed (1 ramp)
Init Temp
Init Time
Ramp
Rate
Fin Temp
Fin Time
Flow Param (EPP)
Constant Flow
Range 5
COLUMN:
Part No.
Dimensions
Sta Phase Methyl Silicone
START
.13
1.91
3.35
IF
FPD On-column Inlet
HP 5890 Test Sample Operating
Conditions
On
N/A DEGREES C
N/A
N/A min
N/A min
90 DEGREES C
1.0 min
(1) (2)
20 10
110 170
0 3
Off
19095S•100
¿
5 M Length, 530 ID
Sulfer
Filter
DODECANETHIOL
4.06
FLOW RATES (FPD AIR MODE FLOWS)
Carrier (N2) 20 +/• 1
Hydrogen 75 +/• 2
Air 100 +/• 3
Makeup (N2)
Split Vent
Septum Purge 5 +/• 1
SAMPLE:
Type FPD Sample
¿
Inj Volume 1 l
Part No. 19395•60580
¿
COMPOSITION: 20 ng/
(20.0 ppm W/V) each of
1-dodecanethiol and
tributylphosphate in isooctane
START
.13
.49
Phosphorus
1.45 Filter
4.08
4.57
IF
ml/min
ml/min
ml/min
0 ml/min
N/A ml/min
ml/min
L
TRIBUTYLPHOS-
5.37
PHATE
239