HP 5890 Series II Plus Reference Manual page 232

Test Sample Chromatograms
Test sample chromatograms
Figure 10-8.
Detector Type ECDw/MUG
Temp 300 DEGREES C
Inlet Type Split only or
splitless
Temp 200 DEGREES C
Operating Mode Split(Purge on)
Purge Time On
Purge Time Off
Oven Temp Isothermal
Init Temp
Init Time
Ramp
Rate
Fin Temp
Fin Time
Range 0
COLUMN:
Part No.
Dimensions
Sta Phase
ECD-Split Mode Capillary Inlet
232
HP 5890 Test Sample Operating
Conditions
0 min
0 min
170 DEGREES C
N/A min
0
19095S(#100)
¿
530 MID; 5 m
Methyl Silicone
.43
ST
FLOW RATES
Carrier (He)
Hydrogen
Air
Makeup (N2)
Split Vent
Septum Purge
SAMPLE:
Type ECD Sample
Inj Volume
Part No. 18713•60040
Composition 33 pg/
ppm (W/V)) each: lindane
and aldrin in isooctane
ALDRIN
2.64
15 +/• 1 ml/min
N/A ml/min
N/A ml/min
60 +/• 2 ml/min
60 +/• 2 ml/min
5 +/• 1 ml/min
¿
1 l
¿
l (0.033
3
. 7
LINDANE
1.13