HP 5890 Series II Plus Reference Manual page 230

Test Sample Chromatograms
Test sample chromatograms
Figure 10-6.
Detector Type
Temp 250 DEGREES C
Inlet Type SPLIT ONLY OR
SPLIT/SPLITLESS Temp
Operating Mode SPLIT(PURGE ON)
Purge Time On
Purge Time Off
Oven Temp Programmed (1 ramp)
Init Temp
Init Time
Ramp
Rate
Fin Temp
Fin Time
Range 7
COLUMN:
Part No. 19095Z•121
Dimensions
Sta Phase Methyl Silicone
START
FID-Split Mode Capillary Inlet
230
HP 5890 Test Sample Operating Conditions
FIDw/MUG
200 DEG C
0 min
0 min
100 DEGREES C
0 min
20
180
1
¿
530 ; 10 M
2.21 2.35
2.81
ST
FLOW RATES
Carrier (He) 15 +/• 1
Hydrogen 30 +/• 1
Air 400 +/• 20
Makeup (N2) 20 +/• 1
Split Vent 200 +/• 20
Septum Purge 5 +/• 1
SAMPLE:
Type Capillary Sample
¿
Inj Volume 1
Part No. 18740•60900
Composition: Soln of 0.1%(w/w)
n-nonane,n-hexadecane and 0.1%
(w/w)each of 1-octanol,nonanol,
n-undecane,naphthalene,2-deca-
none,n-dadecane,n-tridecane,
1-pentadecane in tetradecane.
2.64
3.67
ml/min
ml/min
ml/min
ml/min
ml/min
ml/min
l
.40
C9
C16