Carrier Gas Considerations - HP 5890 Series II Plus Reference Manual

Hewlett-packard reference manual
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Inlet Systems
Split/splitless capillary inlet
The multiple•modesplit/splitless capillary inlet system may be used with
any of the common types of capillary columns (fused silica, quartz, glass,
metal).
Specific sampling modes include:
Split, for major•componentanalyses.
Purged splitless, for trace•componentanalyses.
Each mode requires installation of a specific inlet insert.
Figure 6-6
Available Inlet Inserts
Note that performance in capillary analyses is closely related to the
insert used (and sampling mode). Inserts supplied are average , suitable
for good performance over a variety of general applications. For
specialized applications, however, to optimize inlet performance,
custom•madeinserts may be used: any custom•madeinsert must not
exceed 6.52 mm od, and must be 78.5 + 0.1 mm in length to operate
properly.

Carrier gas considerations

Carrier gas choice, and its average linear velocity through the column,
strongly influences column efficiency, analysis time, and system stability.
108
SPLIT
SPLITLESS
Packing

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