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M&C PMA Series Instruction Manual

Portable oxygen analyzer
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Oxygen – Analyzer Series PMA
®
PMA10, PMA10S
portable
Instruction Manual
Version 1.01.00

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Summary of Contents for M&C PMA Series

  • Page 1 Oxygen – Analyzer Series PMA ® PMA10, PMA10S portable Instruction Manual Version 1.01.00...
  • Page 2: Dear Customer

    Dear customer, Thank you for buying our product. In this instruction manual you will find all necessary information about this M&C product. The information in the instruction manual is fast and easy to find, so you can start using your M&C product right after you have read the manual.
  • Page 3: Table Of Contents

    Content General information ............................. 5 Declaration of conformity ........................... 5 Safety instructions ..............................6 Intended use ....................................6 Warranty................................. 6 Used terms and signal indications ........................7 Introduction ................................9 Serial number ....................................9 Application ................................9 Technical data ..............................10 Description .................................
  • Page 4: List Of Illustrations

    List of Illustrations Figure 1 Dimensions ..................................12 Figure 2 Front panel ..................................12 Figure 3 Gas flow diagram PMA10(S) ............................. 13 Figure 4 Scheme of the measuring cell and optical signal processing ..............14 Figure 5 Standard gas conditioning system........................17 Figure 6 Plug connection signal output ..........................
  • Page 5: General Information

    HEAD OFFICE M&C TechGroup Germany GmbH  Rehhecke 79  40885 Ratingen  Germany Telephone: 02102 / 935 – 0 Fax: 02102 / 935 – 111 E - mail: info@mc-techgroup.com www.mc-techgroup.com General information The product described in this manual has been built and tested in our production facility. All M&C products are packed to be shipped safely.
  • Page 6: Safety Instructions

    Safety instructions Follow these safety directions and instructions regarding installation, commissioning and operation of this device: Read this manual before commissioning and operating the product. Please make sure to follow all safety instruc- tions. Installation and commissioning of electrical devices must be carried out only by qualified skilled personnel in com- pliance with the current regulations.
  • Page 7: Used Terms And Signal Indications

    Used terms and signal indications This means that death, severe physical injuries and/or important material dam- age will occur in case the respective safety measures are not fulfilled. Danger This means that death, severe physical injuries and/or important material damage may occur in case the respective safety measures are not fulfilled. Warning This means that minor physical injuries may occur in case the respective safety measures are not fulfilled.
  • Page 8 Wear safety glasses! Protect your eyes while working with chemicals or sharp objects. Wear safety glasses to avoid getting something in your eyes. Wear protective clothes! Working with chemicals, sharp objects or extremely high temperatures re- quires wearing protective clothes. Use foot protection Use safety helmet and full protective goggles PMA10, PMA10S | 1.01.00...
  • Page 9: Introduction

    Introduction The portable M&C oxygen analyzer PMA10(S) is a non-thermostated instrument which has been designed for continuous and discontinuous measurement of oxygen concentrations in dry and particle-free sample gas. Serial number The type plate with the serial number is located on the back of the analyzer. Please refer to this serial number if you have any questions about your PMA 10(S).or if you need to order spare parts or consumables.
  • Page 10: Technical Data

    Technical data Oxygen analyzer Series PMA  Version PMA10 and PMA10S Part No. PMA10 : 01A1000 = 230 V, 50 Hz; 01A1000a = 115 V, 60 Hz PMA10S : 01A2000 = 230 V, 50 Hz; 01A2000a = 115 V, 60 Hz Measuring ranges Selectable for 0-3, 0-10, 0-30 and 0-100 vol% O , linear...
  • Page 11: Description

    Extra charge for gas sample pump incorporated in analyzer type PMA10. Capacity: 1 Nl/min with- 01A9102 out pressure 01A9050 Extra charge for PMA 10 with battery operation, battery charger incorporated in the analyzer 01A9150 Min.* or max.* alarm contact, adjustable from 0-100 % O Extra charge for alarm contact at analyzer type PMA10, adjustable from 0-100 % O .
  • Page 12: Front Panel

    The analyzer is not thermostated and should be operated only in areas with con- stant ambient temperature. If this is not possible, the analyzer has to be calibrated before every measurement, to guarantee the accuracy of measurement. Note Figure 1 Dimensions Front panel Analog/digital indication...
  • Page 13: Gas Flow Diagram Of The Analyzer Pma10(S)

    At the rear side there are: • Low heat device socket with 2 fine fuses for power supply • Push button for battery check - Option • Switch for the sample gas pump - Option • 3 pole bushing for alarm contact outlet - Option Gas flow diagram of the analyzer PMA10(S) Fine filter Flow meter with needle valve...
  • Page 14: Sample Gas Pump

    9.3.4 Sample gas pump A sample gas pump with a capacity of approx. 1 l/min – without pressure can be integrated in the device. The pump is designed for short time rating only. For long-term operation an external sample gas pump has to be be used.
  • Page 15: Receipt Of Goods And Storage

    The measuring cell consists of two nitrogen-filled spheres  which are arranged in the form of a dumbbell. In the dumbbell’s central point of rotation, a small mirror  is placed. The dumbbell is surrounded by a wire coil needed for the compensation procedure. The described system is fixed rotationally symmetrical inside a glass tube via a tightening strap out of platinum ...
  • Page 16: Connection Of Sample Gas Inlet And Sample Gas Outlet

    In case of outdoor operation protect the analyzer against sun, wind and rain. At the installation location constant climatic ambient conditions (pressure, temperature) are necessary to prevent a distortion of the measurement and Caution a condensation in the measuring cell in case the ambient temperature is fall- ing below the dew point temperature of the sample gas.
  • Page 17: Standard Gas Conditioning System

    Standard gas conditioning system PMA10(S)  +5 °C [41 °F]       Heated gas sample probe (e.g. portable probe PSP4000-H)  Heated gas sample line (e.g. PSP4M4/6)  Sample gas cooler  Peristaltic pump or condensate collecting vessel Diaphragm pump ...
  • Page 18: Option Alarm Contact Output

    The output signals are not galvanically isolated. For the connection of the signal output an adequate plug is provided. Figure 6 Plug connection signal output 14.2 Option alarm contact output The alarm contact output is designed as MIN- as well as MAX-contact. The factory default setting is a MAX- contact.
  • Page 19: Connections On The Rear Side

    Connections on the rear side  Low heat device socket with 2 x fine fuses for power supply  Space for push-button for battery check - Option  Space for pump switch ON-OFF - Option  Space for 3-pole bushing for alarm contact output - Option Figure 7 Rear side Preparations for commissioning...
  • Page 20: Version With Rechargeable Battery

    • Check electrical connections and gas connections. • Switch on mains voltage. • Turn measuring range selection switch from ‘0’ to the desired measuring range. The analyzer is ready for operation immediately. Caution If during transport the analyzer was exposed to extreme changes of temper- ature, an adequate time for temperature adaption has to be observed, to pre- vent condensation in the device.
  • Page 21: Calibration

    Calibration The accuracy of an analyzer mainly is dependent on its calibration. Before calibration it has to be assured that the calibration conditions corre- spond to the conditions during measurement. The flow rate, the ambient temperature and the barometric pressure conditions have to be constant. Un- Note der this terms a calibration of the analyzer is necessary aproximately one time a week to maintain the accuracy.
  • Page 22: Cross Sensitivities

    Output signal Measurement 0-1 V 0-20 mA 0 mA 4-20 mA 4 mA If a gas mixture is analysed, the single gas components have to be checked concerning po- tential cross sensitivity and regarded for zero calibration. (see chapter 18.1.1 and 18.1.2). Note 11.
  • Page 23: Consideration Of Cross Sensitivities

    Formula 20 °C [68 °F] 50 °C [122 °F] Krypton -0.49 -0.54 Methane -0.16 -0.17 Methanol -0.27 -0.31 Methylene chloride -1.00 -1.10 Neon +0.16 +0.17 n-octane -2.45 -2.70 Phenol -1.40 -1.54 Propane -0.77 -0.85 Propylene -0.57 -0.62 Propylene chloride -1.42 -1.44 Propylene oxide -0.90...
  • Page 24 The cross sensitivity values of above table are based on 100 vol% of the respective gases. Therefore, a con- version must be maid to the effective volume concentration. In principle, the following is valid: Table value x Volume concentration  Effective cross sensitivity = [vol%] For the components of the gas mixture, the following values are found:...
  • Page 25: Span Calibration

    18.2 Span calibration Before span calibration a finished zero calibration is necessary. Connect a flexible PVC- or FEP-hose with the pressure reducer of the N -zero-gas bottle. The pressure reducer should have an output control range of max. 0–1.5 bar abs.. Caution The outlet pressure is only allowed to be adjusted at max.
  • Page 26: Measuring

    Se = Final value, signal output Snp = Zero, signal output 13. Shut off pressure reducer output valve and bottle valve 14. Disconnect hose connection at the analyzer. The span calibration is finished. If during the span calibration great variations have to be compensated (>2 % O ) at the potentiometers, a second zero and span calibration is reasonable.
  • Page 27: Maintenance

    Maintenance The analyzer, woking with a physical measuring principle, requires no intensive and complex maintenance. But the preceding components necessary for the sample gas conditioning are to be maintained with special attention according to the respective operating manuals. The calibration of zero and span is to be effected with the corresponding test gases according to stability of the operating conditions and to the demands on the accuracy.
  • Page 28: Trouble Shooting

    Trouble shooting Error Possible reason Check/Repair No indication No supply voltage Check supply voltage according to type plate. Check wether mains cable is plugged in accurate. Check fine fuse in the low heat device socket. No sample gas Sample line or filter is Check sample system.
  • Page 29: Risk Assessment

    Risk assessment The risk assessment provided in this chapter is intended for all work activities on the product. The hazards can occur in the work steps of assembly, commissioning, maintenance, disassembly and in the event of a product fault. During normal operation, the product is protected by a system cabinet or appropriate covers. Only qualified personnel is permitted to perform the work.
  • Page 30 Aggressive condensate possible Risk rank group A Chemical burns due to aggressive media possible! This applies to all liquids in vessels and in the product. In general, for electrical and mechanical work on the product, wear personal pro- tective equipment (PPE) in accordance with the risk assessment. Caution hot surfaces Risk rank group A The temperature inside the product can be higher than >...
  • Page 31: Appendix

    Caution crushing hazard Risk rank group A The work must be performed by trained personnel only. This applies to products weighing less than < 40 kg [≈ 88.2 lbs]: The product can be transported by 1 to 2 person(s). The instructions for appropri- ate personal protective equipment (PPE) must be observed.
  • Page 32: Figure 10 Assembly Of The Components (Drawing-No.: 2355-5.01.0)

    Figure 10 Assembly of the components (Drawing-No.: 2355-5.01.0) PMA10, PMA10S | 1.01.00 www.mc-techgroup.com...

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