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Summary of Contents for Ametek SPECTRO GENESIS FED37
- Page 1 Das verknüpfte Bild kann SPECTRO GENESIS FED37 76004570 Optical emission spectrometer with inductively-coupled plasma excitation Original operating instructions 14.12.2023 | Version 1.0...
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Page 3: Table Of Contents
Oxygen (optional) ....................27 Exhaust air (to the outside) ..................... 28 Operation ........................ 30 Overview of controls ....................... 31 Preparation of the instrument ..................32 Switch on the instrument, ready for operation, plasma start..........33 SPECTRO GENESIS FED37 — 14.12.2023 — 3... - Page 4 Fitting the lens and thelight pipe bracket ............54 Pump tubing maintenance ....................56 Cleaning agents ......................57 Troubleshooting ...................... 58 Spare parts and consumables................65 De-commissioning ....................66 Manufacturer address .................... 67 EC Declaration of Conformity ................68 — 4 SPECTRO GENESIS FED37 — 14.12.2023...
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Page 5: Description Of Instrument
FED37 Type/Part No.: 76004570 Function The SPECTRO GENESIS FED37 is an automatic optical emission spectrometer providing simultaneous measurements. It uses inductively coupled plasma excitation and a semiconductor-based detector system for quantitative and semi- quantitative analysis of liquids. The peristaltic pump is used to feed in the sample. -
Page 6: Safety
General warning sign! Warning! High voltage! Warning! Hot surface! Warning! Toxic substances! Warning! Sharp edges! Warning! Optical radiation! Warning! Risk of suffocation! Warning! Risk of hand injury! Warning! Toxic and corrosive substances! — 6 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 7: User Information
Never tamper with the safety devices! If you suspect that a safety device does not work properly, shut down the instrument immediately! Please contact your Service Center. SPECTRO GENESIS FED37 — 14.12.2023 — 7... -
Page 8: Working Zones And Hazardous Areas
The hazardous area must be entered for the following tasks: Inserting samples Assembly of samplers Setting up, installing, and optimizing the sample input Installing the plasma interface Measurement mode Maintenance Cleaning Troubleshooting — 8 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 9: Intended Use
Laboratory clothing must be tight-fitting so that the garment cannot be pulled into rotating parts (e.g. peristaltic pump). SPECTRO GENESIS FED37 — 14.12.2023 — 9... -
Page 10: Prohibited Operating Conditions
Unauthorized modification or conversion of the instrument and its safety devices without complying with the applicable rules and regulations. Bypassing or deactivating safety and protective devices. Improper use of accessories or peripheral devices linked to the instrument. — 10 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 11: Residual Risks
Never wear loose-fitting clothes drooping down or jewelry when working near rotating parts. A hairnet must be worn to cover long hair. Since the pump develops only max. 80 Ncm, there is only a low risk of injury. SPECTRO GENESIS FED37 — 14.12.2023 — 11... - Page 12 In order to ensure the availability and operational safety of the equipment, we recommend having the system checked for correct operation and performance at least once a year by specialized technicians. Addresses of service organizations authorized by SPECTRO can be found at www.spectro.com. — 12 SPECTRO GENESIS FED37 — 14.12.2023...
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Page 13: External Automatic Sample Introduction
Comply with the applicable occupational health and safety regulations relevant to the workplace and the samples used (hazardous substances). Comply with the safety data sheets for the hazardous substances. SPECTRO GENESIS FED37 — 14.12.2023 — 13... -
Page 14: Layout Of The Instrument
DSOI (Dual Side On Interface) Plasma chamber inspection Connection to sample introduction window system Extraction box housing (plasma Peristaltic pump (sample torch) transport) Connection point for fill level Generator exhaust indicator for waste container Plasma off — 14 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 15: Left-Hand Side
Layout of the instrument Left-hand side Fig. 2 Component Component Service flap Connection points Air filter (behind service flap) Main switch SPECTRO GENESIS FED37 — 14.12.2023 — 15... -
Page 16: Connections (Left-Hand Side)
Layout of the instrument Connections (left-hand side) Fig. 3 Component Component Status port (option) Power cable PC connection Argon connection Main switch Oxygen connection (option) — 16 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 17: Connections (Analysis Room)
Layout of the instrument Connections (analysis room) Fig. 4 Component Component Gas connection Spectro Intelligent Nebulizer gas Valve System (IVS) - optional Additional gas connection Control system Spectro Intelligent Valve System (IVS) - optional SPECTRO GENESIS FED37 — 14.12.2023 — 17... -
Page 18: Peristaltic Pump
Layout of the instrument Peristaltic pump Information Check the peristaltic pump’s hoses for damage and replace the hoses regularly. Fig. 5 Component Peristaltic pump — 18 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 19: Sample Introduction System
A waste container made from an appropriate resistant material is needed to collect excess sample material from the nebulizer chamber. The waste container with the appropriate hoses is included in the scope of supply of the instrument. SPECTRO GENESIS FED37 — 14.12.2023 — 19... -
Page 20: Plasma Torch Box
Plasma torch box Fig. 7 Component Component Extraction box housing and torch Connection to sample introduction system (spherical joint seal) DSOI (Dual Side-On Interface) Plasma torch bracket Load coil Plasma interface (SPI) Plasma torch — 20 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 21: Technical Data
∆T ≤ 3 °C/h. (5.4°F/h) Humidity < 80% rel. (non-condensing) Air quality No corrosive components and no high concentrations of dust Operation: Max. 3000 m above mean sea level SPECTRO GENESIS FED37 — 14.12.2023 — 21... - Page 22 Plasma chamber Dependent on ambient temperature 180 to 230 m³/h; 106 to 136 CFM Generator extraction or without 200 to 250 m³/h; 118 to 150 CFM extraction Blowing into the room without obstruction — 22 SPECTRO GENESIS FED37 — 14.12.2023...
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Page 23: Transportation/Setting-Up
Notice – Damage to the instrument! There is a risk of damage to the instrument whenever it is moved to another location after it has been set up. Please contact the SPECTRO Service Department regarding this matter. SPECTRO GENESIS FED37 — 14.12.2023 — 23... -
Page 24: Space Requirements
For operation and maintenance purposes a clearance of at least 1 m is required at the front and on both sides of the instrument. Install the instrument with these requirements in mind. — 24 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 25: Set-Up
A table of corresponding dimensions and load-carrying capacity is required, see page 21. In addition to the space required by the SPECTRO GENESIS FED37, some space is needed for the gas supply, unless fixed gas connections are available. -
Page 26: Dust Load
The parts and connections of the gas supply line must be checked regularly for leaks or possible damage. Compliance with country-specific national rules and regulations for the safe use of gases and gas cylinders is mandatory. — 26 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 27: Argon
Purging the optical system 0.5 to 1 l/min, typically 0.5 l/min 5.7.2 Oxygen (optional) Inlet pressure during 4.0 bar (58 psi) operation Quality ≥ 4.5 (99.995 %) Flow rate The flow rate depends on the application. SPECTRO GENESIS FED37 — 14.12.2023 — 27... -
Page 28: Exhaust Air (To The Outside)
All installation must be performed in a professional manner and in accordance with applicable engineering standards in order to prevent risk to life and limb and avoid damage to material property. — 28 SPECTRO GENESIS FED37 — 14.12.2023... - Page 29 Plasma torch box housing Generator extraction or without extraction 180 to 230 m³/h; 106 to 136 CFM 200 to 250 m³/h; 118 to 150 CFM Dependent on ambient temperature Blowing into the room without obstruction SPECTRO GENESIS FED37 — 14.12.2023 — 29...
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Page 30: Operation
If glass is broken, a suitable container (bucket) must be used to collect the larger pieces first. In order to remove small parts and glass fragments, a suitable vacuum must be used. — 30 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 31: Overview Of Controls
Operation Overview of controls Fig. 10 Control element Function Main switch Switches the power supply (On/Off) Plasma Off Switches the plasma off SPECTRO GENESIS FED37 — 14.12.2023 — 31... -
Page 32: Preparation Of The Instrument
Ensure that the extraction system is activated and that the specified exhaust capacity is reached. Ensure that all flaps and doors are closed. The instrument is ready for use. — 32 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 33: Switch On The Instrument, Ready For Operation, Plasma Start
Briefly open the torch box and close it back up to enable the safety relay. The instrument is ready for operation. Click the plasma icon to open the instrument control parameters: SPECTRO GENESIS FED37 — 14.12.2023 — 33... - Page 34 10 minutes in order to heat up and equalize the components. The instrument is now switched on and the plasma started. — 34 SPECTRO GENESIS FED37 — 14.12.2023...
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Page 35: Switch Off The Instrument/Plasma
If step 7 is omitted, the instrument is in the "Instrument Standby" mode. In order to reactivate the instrument, follow the instructions in chapter 6.3, starting at step 2, see page 33. The stabilization period is significantly reduced. SPECTRO GENESIS FED37 — 14.12.2023 — 35... -
Page 36: Energy Saving Mode
UV transmission. This timeframe depends on the following parameters: Duration of energy saving mode Ambient temperature Humidity For additional information, refer to the online Help. — 36 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 37: Carrying Out The Measurement
before proceeding with high-precision measurements. Aqueous applications The spectrum calibration of aqueous applications requires a solution of the following composition: Element Concentration mg/L Element Concentration mg/L The solution must also contain: SPECTRO GENESIS FED37 — 14.12.2023 — 37... - Page 38 Click the “Start Spectrum Calibration” button in order to calibrate the optics. The information box communicates whether the calibration has been completed successfully or if errors occurred. The optics is now calibrated. — 38 SPECTRO GENESIS FED37 — 14.12.2023...
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Page 39: Calibrating A Method
Proceed in this way until all standards contained in the list were measured. When all standards contained in the list were measured, click on the ”Calculate“ button. The method is now calibrated. SPECTRO GENESIS FED37 — 14.12.2023 — 39... -
Page 40: Start The Measurement
When the measurement is complete, the results are displayed on the screen. Press the “Finish” button to terminate the measurement process. The measurement process is finished. Perform further measurements as needed. — 40 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 41: Maintenance
42. Nebulizer Check quality of aerosol generation, see page 50. Air filter (underneath the left-hand Replace, if dirty. instrument cover) Further maintenance work Pump tubes Check for damage. Replace if required, see page SPECTRO GENESIS FED37 — 14.12.2023 — 41... -
Page 42: Cleaning The Plasma Torch
Switch off the plasma. Loosen and remove the clamp(s) and the spherical joint seal between the plasma torch and the nebulizer chamber. Loosen the plasma torch by turning it counterclockwise. Remove the plasma torch. — 42 SPECTRO GENESIS FED37 — 14.12.2023... - Page 43 Observe the corresponding information on hazardous materials. Let the acid/cleaning solution act for approx. 15 minutes. Subsequently, rinse the torch with distilled water and let it dry completely. Fig. 12 SPECTRO GENESIS FED37 — 14.12.2023 — 43...
- Page 44 (3). There is a clearance of ±1 mm to optimize the torch’s height. Reconnect the hoses (A = Auxiliary, C = Plasma gas). Fig. 13 — 44 SPECTRO GENESIS FED37 — 14.12.2023...
- Page 45 Inserting the plasma torch: Insert the torch in the appropriate position and turn the lever (1) clockwise until it snaps into place. Fig. 14: Radial plasma observation (DSOI) The plasma torch has been cleaned. SPECTRO GENESIS FED37 — 14.12.2023 — 45...
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Page 46: Clean The Nebulizer (Crossflow Nebulizer)
Disconnect all other connections from the nebulizer and the spray chamber. Separate the nebulizer from the spray chamber by slightly twisting it and disconnect the argon connection. Remove the adapter for the argon connection. — 46 SPECTRO GENESIS FED37 — 14.12.2023... - Page 47 10. Then flush the nebulizer with distilled water and let it dry completely. 11. Reinstall the components. 12. Check aerosol generation and optimize the gas flow of the nebulizer; see page 50. Cleaning of the nebulizer is now complete. SPECTRO GENESIS FED37 — 14.12.2023 — 47...
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Page 48: Clean The Nebulizer Chamber (Scott Chamber)
Loosen the Ar connection of the nebulizer. Loosen the clamp between the plasma torch and the spray chamber. Carefully pull off the spray chamber and remove the spherical joint seal. Remove the spray chamber. — 48 SPECTRO GENESIS FED37 — 14.12.2023... - Page 49 Now, use distilled water to flush the spray chamber thoroughly. 10. Reinstall the components. 11. Optimize the nebulizer gas flow; see page 50. Cleaning of the spray chamber is now complete. SPECTRO GENESIS FED37 — 14.12.2023 — 49...
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Page 50: Checking The Aerosol Formation Of The Nebulizer
Click the “Start” button in the dialog window. The instrument optimizes the nebulizer gas flow. Optimization of the nebulizer gas flow is now complete. For additional information, refer to the online Help. — 50 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 51: Cleaning The Side-On Plasma Interface (Spi)
If glass is broken, a suitable container (bucket) must be used to collect the larger pieces first. In order to remove small parts and glass fragments, a suitable vacuum must be used. SPECTRO GENESIS FED37 — 14.12.2023 — 51... - Page 52 Loosen the plasma torch (3) by turning the lever (2) counterclockwise. Remove the plasma torch. Fig. 16 Carefully pull the light pipe (1) to the right-hand side and out of its bracket (2). Fig. 17 — 52 SPECTRO GENESIS FED37 — 14.12.2023...
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Page 53: Cleaning The Lens
When cleaning the lens, proceed as follows (if necessary): Clean the contaminated lens using lens cleaning paper or a lint-free soft cloth. Use a lint-free cloth to clean all other parts. Cleaning of the lens is now complete. SPECTRO GENESIS FED37 — 14.12.2023 — 53... -
Page 54: Fitting The Lens And Thelight Pipe Bracket
Fig. 18 Carefully push the light pipe (1) to the left-side into the light pipe bracket (2) Ensure that the taper (3) in the light pipe points toward the plasma torch. — 54 SPECTRO GENESIS FED37 — 14.12.2023... - Page 55 Maintenance Use a lint-free cloth and isopropanol, if necessary, to clean the adapter. Install the plasma torch and adapter, see page 42. The lens is fitted. SPECTRO GENESIS FED37 — 14.12.2023 — 55...
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Page 56: Pump Tubing Maintenance
Sample introduction Inside diameter 0.89 mm; 0.035" channel: (Orange-orange stops). Outlet channel: Inside diameter 1.8 mm; 0.071" (Blue-green stops). Replacement of pump tubes is now complete. — 56 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 57: Cleaning Agents
Plasma torch Depending on the impurities use diluted hydrochloric acid, nitric acid or aqua regia, demineralized water Nebulizer Depending on the impurities use diluted hydrochloric acid, nitric acid or aqua regia, demineralized water SPECTRO GENESIS FED37 — 14.12.2023 — 57... -
Page 58: Troubleshooting
Waste container is full. its content Spectrum calibration Wrong sample or wrong pre-purge time. failed. Use correct sample of correct concentration. Check the sample introduction system. Repeat spectrum calibration procedure. — 58 SPECTRO GENESIS FED37 — 14.12.2023... - Page 59 Connect the tube and check fitting is switched on. Oxygen in sample introduction system. Flush the system with argon before restarting system. Leak in the sample introduction system. Check for leaks and eliminate these. SPECTRO GENESIS FED37 — 14.12.2023 — 59...
- Page 60 Plasma extinguished during operation. Please restart the plasma (no quick start). Should the problem persist, extend the purging duration and check the entire sample introduction system for leakage or droplets in the aerosol path. — 60 SPECTRO GENESIS FED37 — 14.12.2023...
- Page 61 It was not possible to start or shut off the plasma because the fan speed for the low-pass filter is too low. Please attempt to start the plasma again. Should the problem persist, please call the SPECTRO Service Department and state the error code. SPECTRO GENESIS FED37 — 14.12.2023 — 61...
- Page 62 The plasma could not be started due to an internal plasma coupler connection generator error (coupler connection). Please attempt to start the plasma again. Should the problem persist, please call the SPECTRO Service Department and state the error code. — 62 SPECTRO GENESIS FED37 — 14.12.2023...
- Page 63 It was not possible to start the plasma due to an internal error cable with the plasma generator (RFD cable). Please attempt to start the plasma again. Should the problem persist, please call the SPECTRO Service Department and state the error code. SPECTRO GENESIS FED37 — 14.12.2023 — 63...
- Page 64 Then attempt to start the plasma again (no quick start). Should the problem persist, please call the SPECTRO Service Department and state the error code. — 64 SPECTRO GENESIS FED37 — 14.12.2023...
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Page 65: Spare Parts And Consumables
Only the use of genuine spare parts and consumables ensures the safe operation and achievement of the specified output. This applies especially to all components of the sample introduction system and, in particular, to the Plasma torch. SPECTRO GENESIS FED37 — 14.12.2023 — 65... -
Page 66: Commissioning
De-commissioning De-commissioning Only organizations or persons authorized by the instrument manufacturer shall be permitted to de-commission the instrument. Please contact your Service Center. — 66 SPECTRO GENESIS FED37 — 14.12.2023... -
Page 67: Manufacturer Address
Manufacturer address Manufacturer address SPECTRO Analytical Instruments GmbH Boschstr. 10 D-47533 Kleve Germany Tel.: +49.2821.8 92-0 Fax: +49.2821.8 92-22 00 www.spectro.com Your local SPECTRO Organization or representative can be found under “Contact“ www.spectro.com SPECTRO GENESIS FED37 — 14.12.2023 — 67... -
Page 68: Ec Declaration Of Conformity
EC Declaration of Conformity EC Declaration of Conformity The EC Declaration of Conformity is enclosed with the instrument. — 68 SPECTRO GENESIS FED37 — 14.12.2023...
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