Teledyne CD14 User Manual
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Teledyne CD14 User Manual

Comparative dissolution tester and cd autoplus autosampler
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CD14 C
D
T
OMPARATIVE
ISSOLUTION
ESTER
AND
CD A
P
A
UTO
LUS
UTOSAMPLER
U
G
SER
UIDE
Use and disclosure of data: information contained herein is classified as EAR99 under U.S. Export Administration
Regulations. Export, re-export, or diversion contrary to U.S. law is prohibited.
75-108-800-Rev. B—31 May 2021
 

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  • Page 1 CD14 C OMPARATIVE ISSOLUTION ESTER CD A UTOSAMPLER UIDE Use and disclosure of data: information contained herein is classified as EAR99 under U.S. Export Administration Regulations. Export, re-export, or diversion contrary to U.S. law is prohibited. 75-108-800-Rev. B—31 May 2021...
  • Page 2 For more information, visit teledynehanson.com. Headquarters Teledyne Hanson 9810 Variel Avenue Chatsworth, CA 91311, USA Phone: +1 818.882.7266 www.teledynehanson.com CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 1 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 3 Email: hansontechsupport@teledyne.com Email: hansonsales@teledyne.com Phone: +1 818.882.7266 Teledyne Hanson 9810 Variel Avenue Chatsworth, CA 91311, USA CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 2 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 4 Note: To confirm that you have received the latest version of this user guide, contact Teledyne Hanson Technical Support. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 3 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 5: Table Of Contents

      ........................ 39 LECTRICAL  EQUIREMENTS     ........................ 39 NPACKING AND  NSPECTION     ........................ 40 LECTRICAL  ONNECTIONS CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 4 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 6 OLUME     ............................ 106 INSE  OLUME    ............................ 108 ARRYOVER    .................... 111   LUS  OVING AND  TORAGE CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 5 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 7  .................. 79 IGURE    AG  ALIBRATION  OOL IN  LACE   K‐1:   ......................... 123 ABLE    ETTED  ATERIALS CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 6 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 8: Section A - Cd14 Tester Introduction

    The on- CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 7 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 9: Features

    USP / FDA / ASTM / EP / JP compliant CE / RoHS compliant, includes earth-friendly packing CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 8 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 10: Cd14 Comparative Dissolution Tester Identification

    Section A – CD14 Tester Introduction CD14 Comparative Dissolution Tester Identification Figure A-1: Identification of the CD14 Tester CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 9 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 11: Section B - Cd Autoplus Sampler Introduction

    Collection racks include 16 x 100 mm test tubes for UV, 13 x 100 test tubes for UV, 12 x 32 vials for HPLC. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 10 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 12 The vial/test tube holder that fits on the AutoFill. Recurrence The dictated time at which a function repeats. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 11 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 13 The moving of liquid from a source to a destination. Wash The clearing out of old media from tubing with blank or wash media. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 12 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 14 AutoFill Dispense head Collector Tray handle Touchscreen Power switch Autosampler handle CD AutoPlus Autosampler Syringes CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 13 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 15 Section B – CD AutoPlus Introduction Figure B-2: Identification of the CD AutoPlus Fluidics CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 14 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 16: Section C - Regulatory And Safety

    Review all safety and environmental precautions pertaining to any chemicals that are to be used in conjunction with this equipment. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 15 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 17: Cd14 Tester Safety Considerations

    Additional hazards may exist if the equipment is not operated according to the instructions in the user guide. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 16 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 18: Safety Symbols

    CD14 Tester Warning Locations System warnings on the mast – Service warnings on the heater – CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 17 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 19: Cd Autoplus General Safety Considerations

     Additional hazards may exist if the equipment is not used correctly per the user guide. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 18 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 20 Figure C-1: CD AutoPlus/AutoFill Potential Pinch Hazards Between cap and vials/tubes Base of moving dispense Under removable head drip tray CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 19 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 21: Section D - Tester Installation

    Issues which may affect dissolution results include vibration, significant heat, or significant cold. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 20 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 22: Space Requirements

    Power cords should meet the following specifications: IEC 320-C13 connector; SJT 18AWG3C, 2 x 0.824 mm2, 60 °C, 300 V. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 21 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 23: General Unpacking And Installation

    Remove the heater enclosure out from under the unit. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 22 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 24: Attach Lifting Handles

    Important: Verify oval handle inserts will not pull out of the legs by pulling on the handles. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 23 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 25: Remove Counter-Weight Shipping Bolts

    CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 24 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 26: Moving The Unit

    CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 25 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 27 5 replacing that person originally there who has now backed away. The foot under the mast slides onto the bench. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 26 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 28 In the process the unit is turned to a forward-facing position. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 27 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 29: Level The Unit

    While doing so, maintain the height of the unit within the factory height range. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 28 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 30 Lock the upper nuts of all five feet to the frame. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 29 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 31: Heater Assembly

    Route the 24VDC power cable as shown and plug the connector into the back of the heater. Tie-wrap the cable to the tubing as shown. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 30 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 32: Heater Installation

    ‘threaded’ straight back as the heater is moved into its final position in the following steps. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 31 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 33 While still supporting the front of the heater, make the cable connections from the cable bundle to the rear of the heater. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 32 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 34 CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 33 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 35 Section D – Tester Installation CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 34 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 36 With the heater power switch in the off (O) position, plug in the heater power cord to a power source. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 35 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 37: Filling The Bath

    Check for leaks. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 36 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 38: Start The Pump

    (left and right) ports within the bath a couple of times with the supplied syringe. Start the pump again. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 37 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 39: Tester Installation Is Complete

    The next section describes the installation of the accessory autosamplers. If manual sampling is going to be used, skip to the operation section. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 38 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 40: Section E - Autosampler Installation

    Environmental Requirements The CD AutoPlus samplers should be placed one on the left (Side A) and one on the right (Side B) of the CD14 Tester. The Teledyne Hanson AutoFill collectors should be placed on top of each CD AutoPlus.

  • Page 41: Electrical Connections

    The panel illustrates port placement. (See Figures E-1 and E-2.) Figure E-1: CD AutoPlus Back Panel and Ports CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 40 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 42 CD AutoPlus on the right of the CD14 Tester to the ‘Sampler B’ port of the CD14 Tester. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 41 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 43: Cd Autoplus To Autofill Communication Connections

    Connect the other end of the RS-232 cable to the RS-232 port labeled Sampler on the back of the AutoFill. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 42 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 44 Touch the screen anywhere; the menu will appear. Touch the ‘x’ button at the bottom to exit back home. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 43 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 45 Enter the corresponding sampler ID’s to be associated with the samplers. Press the ‘Return’ button when done. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 44 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 46 NOTE: When a CD AutoPlus is configured in the sampling mode (as was done above), the CD14 Tester will also set the clocks of both samplers. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 45 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 47: Verifying Syringe Functions

    Touch the Manual (syringe) button located at the bottom of the screen. The Manual Syringe Control screen will appear. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 46 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 48 Ensure that the syringes go down and then return to the home position. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 47 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 49: Verifying Collector Functions

    “18” and touch the OK button. The dispense head should move to the last row of the installed rack. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 48 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 50 Touch the Initialize button to return the dispense head to the home position. Touch the Exit button to return to the menu screen. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 49 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 51: Section F - Operation

    Section F – Operation Drive Head Movement The CD14 Tester drive head can be moved by pulling the lock release lever on the left underside of the drive head (behind the handle bar), then moving the drive head up or down.

  • Page 52: Vessel Installation

    Note the witness marks. The vessels will only go in one way. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 51 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 53: Configuration And Programming

    ‘Program’ button. The set points for both side A and side B speeds can be linked using the checkbox. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 52 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 54 Tools: Access user tools such as adjusting temperature probe readings and magazine calibration. Run/Stop: Run/stop a dissolution method. Vessels: View/print vessel temperatures. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 53 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 55 Info/Logs: View instrument information such as event logs, instrument errors, test reports, serial numbers, and service logs. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 54 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 56: User Interface Screens

    These icons may also be grayed out depending on security settings. Exit/return Exit/return to previous screen. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 55 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 57: Instrument Setup

    The default value is ± 0.5 °C. The range is 0(off), 0.1 to 5.00 °C. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 56 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 58 Allows the user to enter the appropriate port of the target printer (0-65535). The default is 9100. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 57 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 59 Auto Dosage Delivery (ADD™): Selected when auto dosage delivery flask covers are installed in the instrument. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 58 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 60: Titles Button

    No more than 100 pixels wide by 50 pixels high  96 dpi  File size 15 KB or less CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 59 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 61 Method ID: A secondary ID for the method; this does not need to be unique. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 60 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 62 Comments: Allows the user to add any comments which should be noted related to this test run. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 61 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 63: Firmware Update

    Security Configuration screen. The CD14 Tester can be configured to require users to log in and allows for tracking of any changes made to the method. The security system allows for three types of users (administrators, managers, and operators) and can accommodate up to 100 users.
  • Page 64 Note: Importing the security data completely replaces the configuration and users in the destination instrument. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 63 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 65 (active/locked). Access button This button accesses the User Access Configuration screen. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 64 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 66 Instrument Config Run Diagnostics Display Settings Edit Methods Security Settings Use Tools Run Tests Edit Informatics CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 65 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 67: Diagnostics

    CD14 Tester. Touching Info/Logs brings up the Versions screen. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 66 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 68 Cumulative Heater On Time: Cumulative time on the instrument heater. Help tab Additional help information and links. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 67 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 69 It allows the user to select the test based on method name, time, and date, and to reprint the report. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 68 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 70 There are 12 groups for Side A and 12 groups for Side B. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 69 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 71 Preventive Maintenance Due Date: The date of the last preventive maintenance performed on the unit. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 70 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 72: Display

    Default Button: This button returns the touchscreen back to the factory default settings for brightness and volume. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 71 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 73: Time/Alarms

    Recurrence: The method by which the alarm repeats. Either never, at specific days of the week, or at day intervals. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 72 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 74 “Change Tester Bath Water” the text “Change Tester Bath Water” would be displayed when the alarm triggers. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 73 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 75 Alarm Tone: The tone the instrument will play when the alarm triggers. The current tone is played when the ‘Play’ icon is touched. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 74 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 76 Reminder: The text which is displayed when the alarm triggers. The default reminders are ‘Calibration Due’ or ‘Preventive Maintenance Due’. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 75 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 77 CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 76 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 78: Tools Button

    Touch the corresponding temperature reading and enter the corrected temperature as measured by an NIST traceable thermometer to make the correction. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 77 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 79 Magazine Sample Travel field. Pill Drop: Moves the magazine down to the height to trigger Auto Dosage Delivery (ADD) covers. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 78 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 80 The magazine is now calibrated. Repeat the above steps for the other magazine. Figure F-2: AutoMag Calibration Tool in Place CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 79 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 81 Warning: The Remote Command screen should only be used when instructed to by Teledyne Hanson Technical Support. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 80 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 82: Section G - Dissolution Testing

    Recent tab The Recent tab displays the methods from the database in the order of most recently selected. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 81 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 83 Labels tab. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 82 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 84: Method Screen

    7.4 phosphate buffer). Media Volume: Lists the media volume used for the dissolution test (e.g., 900 mL). CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 83 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 85 Digital Temperature Probes: When checked, allows vessel temperature probes mounted on the AutoMag of the CD14 Tester to be monitored during the test. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 84 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 86 All rinse and backflush-filter operations (if any) will occur before the programmed sample time. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 85 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 87 Vessel offset time is not used during automated sampling as the dosage is dropped and the samples are taken simultaneously. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 86 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 88 Infinity Test Speed: Sets the speed of the infinity test that follows the normal test. The range is 0, 25 to 250 rpm. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 87 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 89 Edit Event screen. To delete all the events in a method, touch the Delete All button. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 88 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 90 Event Time: This defines the start of the first event. The range is 0:00 to 999:00 (hhh:mm). Preset buttons are Pre-Run and Post-Run. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 89 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 91: How To Start A Test

    NOTE: this screen is also used to abort a test that is currently running. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 90 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 92 Lot Number: Lot number associated with the test run. Comments: Allows the user to add any comments related to the test run. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 91 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 93 Side A | Side B: This option is available to 6-vessel methods and determines which side A (left) or B (right) of the instrument will be used. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 92 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 94 If using the CD AutoPlus, the CD AutoPlus screen will switch to showing the method name and syringe position. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 93 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 95: Manual Staggered Start With Cd14 Tester

    Cover the vessels and allow the media to stabilize. Once the media has stabilized start the method procedure described below. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 94 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 96 Drop the dosage into position 1 by depressing the push pin. iv. Start the test. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 95 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 97 Repeat the previous steps for each of the remaining positions in turn based on the desired stagger time. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 96 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 98: Section H - Cd14 Tester Maintenance

    Inspect the O-rings, they should not be dried or cracked. Every Two Years Replace the drive belts. Replace the O-rings. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 97 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 99: O-Ring Inspection And Replacement

    Test this by pushing with your finger in-between pulleys. Replace the cover and then press down until it pops back into place. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 98 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 100: Draining The Waterbath

    From the main screen, touch the Tools button on the main toolbar. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 99 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 101: Moving And

    OK. Moving and Storage – CD14 Tester If the CD14 Tester will not be used for a short period of time (3 days or more), the power should be turned off. If the tester will not be used for an extended period of time (30 days or more), the instrument should be cleaned, the bath drained, and the tester unplugged from the power source.

  • Page 102: Section I - Cd Autoplus Maintenance

    Tools menu. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 101 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 103 CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 102 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 104: Cd Autoplus General Cleaning

    45 degrees in order to ensure a good seal and not damage the valve. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 103 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 105: Volume Calibration

    If the volume does not fall within the specifications in the specifications section, contact Teledyne Hanson Technical Support. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 104 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 106: Tubing Volume

    (Tubing length in. or cm) x (mL/in. or mL/cm) + (Tubing length in. or cm) x (mL/in. or mL/cm) and repeat for each section. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 105 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 107: Rinse Volume

    UV analysis. Place the probe back in the DI water and prime the system with 20 mL. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 106 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 108 = the average of the absorbance of the two blank diluent solution readings CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 107 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 109: Carryover

    Vials are not recommended due to sample size. b. Recommended sample size is 7 – 10 mL for UV analysis. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 108 of 130 EAR99 technology subject to restrictions on cover page.
  • Page 110 Repeat steps 4 through 9 until there are 3 samples of the absorbing solution and 3 samples of the blank solution. Clean probes using DI water. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 109 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 111 Blank value must not be more than 0.01 x (first absorbing solution for the line) + (first blank sample for the line). CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 110 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 112: Cd Auto Plus Moving And Storage

    Turn the power off. Remove the rack and secure the needle arm. Disconnect all tubing, communication, and electrical connections from the unit. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 111 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 113: Section J - Troubleshooting

    Detailed information about the problem. What is working and what is not? The troubleshooting steps that have already been taken. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 112 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 114: Electrical Troubleshooting

    If display screen cannot be reached, reboot system and touch the screen during the logo splash screen. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 113 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 115: Mechanical Troubleshooting

    Clamp has loosened or Perform the height spindle shaft was adjustment. replaced. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 114 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 116: Heater Troubleshooting

    Probe temperature probe. Error or --.-- is displayed Probe is damaged. Contact Teledyne Hanson Technical Support. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 115 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 117: Automag Troubleshooting

    Probe disconnected. probe. Error or --.-- is displayed Probe is Contact Teledyne Hanson damaged. Technical Support. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 116 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 118: Serial (Validation) Printer Troubleshooting

    Turn power off, hold down the LF button, and turn power back on. When unit begins to print, release button. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 117 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 119: Network Printer Troubleshooting

    Printer Ensure printer settings are settings correct for printer in system incorrect. configuration. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 118 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 120: Section K - Specifications

    Input: 100 – 230 V ± 10%, 50 – 60 Hz  Power: 700 – 1200 W CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 119 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 121: Cd14 Tester General Specifications

     Input: 24 VDC, 3.75 A, 90 W  Only use external power supply (listed below) CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 120 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 122: Autofill Specifications

    Input: 100 - 240 V~,50 - 60 Hz, 1.5 A max  Output: 24 VDC, 3.75 A, 90 W CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 121 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 123: Cd Autoplus/Autofill General Specifications

    Septum: Pre-cut type only. Warning: Failure to use pre-cut septa can result in damage to the AutoFill needles. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 122 of 130 EAR99 technology subject to restrictions on cover page.

  • Page 124: Wetted Materials

    316 stainless steel Factory Installed Digital Temp Probes w/PCB, 12 Positions, Field 75-107-181 316 stainless steel Installed CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 123 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 125 16 mm Evaporation Caps Polyethylene 61-105-029 Syringe Barrel Borosilicate Glass 91-425-028 Viton O-ring Viton 91-951-004 Silicone Compound Silicone CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 124 of 130 EAR99 technology subject to restrictions on cover page.  ...

  • Page 126: Section L - General Warranty

    Teledyne Hanson will give reasonable assistance to buyer in obtaining from the respective manufacturer whatever adjustment is available under the manufacturer’s own warranty. Teledyne Hanson shall be released from any and all obligations under any warranty, either expressed or implied, if the product covered is repaired or modified by other than its own personnel, or without written authorization from Teledyne Hanson.

  • Page 127: Appendix A: Errors

    2. Check lead screw and shutdown hot. magazine coupling 3. Spindle control board failure CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 126 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 128 2. Check spindle motor 2023 overheat error motor driver overheat. connection. 3. Spindle control board failure CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 127 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 129 Heater board mcode=0x800, task 1. Internal problem 2510 background task overflow. 2. Heater board failure overrun CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 128 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 130 0085 Invalid parameter Internal error Contact Teledyne Hanson. 0086 Finger is not pressed Try again. CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 129 of 130 EAR99 technology subject to restrictions on cover page.  ...
  • Page 131 Copyright © 2021 Teledyne Hanson, a division of Teledyne Instruments, Inc. Document 75-108-800 Rev. B CD14 Tester & CD AutoPlus Autosampler User Guide—75-108-800 Rev. B—31 May 2021 130 of 130 EAR99 technology subject to restrictions on cover page.  ...

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