Page 1 Return to Document Menu ICP OPTICAL EMISSION 8000 PTIMA Customer Hardware and Service Guide...
Page 3 Optima 8000 Customer Hardware and Service Manual...
Page 4 The information contained in this document is subject to change without notice. Except as specifically set forth in the terms and conditions of sale, PerkinElmer makes no warranty of any kind with regard to this document, including, but not limited to, the implied warranties of merchantability and fitness for a particular purpose.
Page 5: Table Of Contents
Contents Customer Service ..............11 Safety and Regulatory Information .
Page 6 WEEE Instructions for PerkinElmer Products ........
Page 7 Contents Sample Introduction System ............75 Sample and Torch Compartments .
Page 8 Contents Setting the Torch Viewing Position ........... . .121 Switching On the System .
Page 9 Contents Cleaning the Torch ............. . . 153 Replacing the Torch .
Page 10 Contents GemCone Liquid Fitting Maintenance ..........206 Concentric Glass Nebulizer .
Page 11 Contents Troubleshooting Form ............260 General: .
Page 12 Contents...
Page 13: Customer Service
Tel: (800) 762-4000 or (203) 762-4000 Supplies, accessories, and replacement parts can be ordered directly from PerkinElmer using the eight-digit part numbers provided in this manual. To place an order for supplies and many replacement parts, request a free catalog, or ask for information visit our website.
Page 14: Safety And Regulatory Information
The protection provided by this equipment may be impaired if Caution the equipment is used in a manner not specified by PerkinElmer. This manual contains important information regarding potential hazards that may arise during the operation of the instrument. It is essential that this information is read and thoroughly understood by all potential users of the instrument.
Page 15: Fcc Compliance (United States)
FCC Compliance (United States) This product is classified as Industrial, Scientific and Medical (ISM) equipment and has been tested and found to comply with the limits specified for non-consumer equipment, pursuant to Part 18 of the FCC Rules. These limits are designed to provide reasonable protection against harmful interference in a non-residential installation.This equipment generates, uses, and can radiate radio frequency energy and, if not installed and used in accordance with the instructions, may cause harmful interference to radio communications.
Page 16: Environment
Environment Operating Conditions Explosive Atmosphere This instrument is not designed for operation in an explosive atmosphere. Warning Pollution Degree This equipment will operate safely in environments that contain non-conductive foreign matter up to Pollution Degree 2 in EN/IEC 61010–1. Recommended operating conditions: •...
Page 17: Symbols Used On The Instrument
When you remove the instrument from storage, before unpacking or putting it into operation, allow it to stand for at least a day under the approved operating conditions. Symbols Used on the Instrument The three different types of warning symbols that appear on the instrument are shown below: This symbol indicates Caution, risk of electric shock.
Page 18 Indicates the ON position of the main power switch. Indicates alternating current.
Page 19: Warning Labels On The Instrument
Warning Labels on the Instrument Labels on the front of the instrument Label Location Instructions for Safety Label #1 in UV Radiation. Risk of eye damage. Figure A. Rayonnement UV. Risque de blessure des yeux. The plasma may emit UV radiation which can damage your eyes. Do not gaze into the emitted light.
Page 20: Warning Labels On The Back And Side Of The Instrument
Warning labels on the back and side of the instrument Marking Location Instructions for Safety Vmax = 30 V AC, Imax = 0.5 A AC Label #1 in Vmax = 30 V DC, Imax= 2 A DC Figure B. Do not exceed stated voltage and current. Air / N Label #2 in Figure B.
Page 21 PerkinElmer d’effectuer un quelconque controle de circuit en courant alternatif. The instrument has AC line surge suppressing components which require disconnection before testing. For safety reasons, testing and servicing should be carried out only by a PerkinElmer service engineer or similarly authorized and trained person.
Page 22 Figure B. Location of warning labels on the back and side of the instrument. Caution: Do not restrict air intake or exhaust. Attention: N’obstruez pas l’arrivée ou l’évacuation d’air. To provide adequate space for ventilation, allow at least 30 cm (12 inches) of free space around the instrument.
Page 23: Warning Labels In The Torch Compartment
Warning labels in the torch compartment Marking Location Instructions for Safety WARNING – Do not defeat interlocks. Label #1 in Avertissement: Ne pas desengager les enclenchements de securite. Figure C The instrument has safety interlocks to protect the operator from exposure to radio frequency and ultraviolet radiation.
Page 24 Figure C. Location of warning labels in the sample compartment.
Page 25: Using This Guide
Using this Guide This manual is your hardware guide to the Optima 8000 instrument. Main topics include: • safety practices • preparing your laboratory • a description of the system • installation • maintenance • troubleshooting • error messages Documents to Help You This manual contains hardware information for Optima 8000 instrument.
Page 26: How This Guide Is Organized
To find out about... 1 Safety Practices Important safety information. 2 Preparing Your Laboratory The preparation of your laboratory needed for the Optima 8000 instrument. Environmental, electrical, space, exhaust, gases, and cooling water requirements are reviewed. 3 System Description The components of the instrument, how the echelle spectrometer works and instrument specifications.
Page 27: Using The Index
A Word on Troubleshooting We recommend that you consult the troubleshooting information included in this manual before you call a PerkinElmer service engineer. The Troubleshooting chapter contains suggestions to help you determine systematically whether instrument problems are due to improper analytical techniques, improper selection...
Page 29: Chapter 1: Safety Practices
Safety Practices...
Page 30: Introduction
General The protection provided by this equipment may be impaired if the Caution equipment is used in a manner not specified by PerkinElmer. This equipment requires no specified inspection or preventive Note maintenance to ensure the continuous functioning of its safety features Always wear safety glasses when using the instrument.
Page 31: Environmental Conditions
Handling of the Instrument Contact a PerkinElmer service engineer for assistance in installing or evaluating the system after moving. The Optima 8000 weighs 146 kg (321 pounds), or 201 kg (442 pounds) with the shipping container. If the instrument needs to be moved please contact PerkinElmer Service.
Page 32: Instrument Safety Practices
The protection provided by this equipment may be impaired if Caution the equipment is used in a manner not specified by PerkinElmer. Safety Interlocks The instrument has safety interlocks to protect the operator from radio frequency (RF) radiation and ultraviolet radiation, and to prevent access to high voltage areas.
Page 33: Radio Frequency Radiation
This section describes some recommended electrical safety practices. Lethal voltages are present at certain areas within the instrument. Installation and internal maintenance of the instrument should only be performed by a PerkinElmer service engineer or similarly authorized and trained person. Warning When the instrument is connected to line power, opening the instrument covers is likely to expose live parts.
Page 34 Safety Practices Grounding circuit continuity is vital for safe operation of the equipment. Never operate equipment with grounding conductor disconnected. Warning Connect the instrument to an AC line power outlet that has a protective ground connection. To ensure satisfactory and safe operation of the instrument, it is essential that the protective ground conductor (the green/yellow lead) of the line power cord is connected to true electrical Warning...
Page 35: High Temperatures
Instrument Safety Practices When working with the instrument: • Connect the instrument to a correctly installed line power outlet that has a protective conductor connection (earth ground). • Do not operate the instrument with any covers or internal parts removed unless required to do so.
Page 36: Safe Use Of Drain Systems
Safety Practices Safe Use of Drain Systems For safe operation of the system, the pumped drain system should be properly installed. Never place the vessel in an enclosed cabinet. Doing so could result in a build-up of hazardous gases, which may result in a serious explosion or fire.
Page 37: Weee Instructions For Perkinelmer Products
Requirements for waste collection reuse, recycling, and recovery programs vary by regulatory authority at your location. Contact your local responsible body (e.g., your laboratory manager) or authorized representative for information regarding applicable disposal regulations. Contact PerkinElmer at the web site listed below for information specific to PerkinElmer products. Web address:...
Page 38: Safe Handling Of Gas Cylinders
Safety Practices For Customer Care telephone numbers select "Contact us" on the web page. Products from other manufacturers may also form a part of your PerkinElmer system. These other producers are directly responsible for the collection and processing of their own waste products under the terms of the WEEE Directive.
Page 39 Safe Handling of Gas Cylinders Storing Cylinders • Cylinders should be stored in accordance with the regulations and standards applicable to the customer’s locality, state, and country. • When cylinders are stored indoors in storage rooms, the storage room should be well ventilated and dry.
Page 40: Hazardous Chemicals Warnings
Safety Practices • Check the condition of pipes, hoses, and connectors regularly. Perform gas leak tests at all joints and seals of the gas system regularly, using an approved gas leak detection solution. • When the equipment is turned off, close all gas cylinder valves tightly at the cylinder.
Page 41: Safe Use Of Chemical Reagents
Safe Handling of Gas Cylinders Operator: "Person operating equipment for its intended purpose." [per EN/IEC 61010-1]. Safe Use of Chemical Reagents This section provides some general safety practices that should be observed when working with any chemicals. Give careful attention to the hazards associated with the chemical reagents being used.
Page 42: Sample Preparation
Safety Practices • Store solvents in an approved cabinet (with the appropriate ventilation, as required) away from the instrument. • The responsible body has the responsibility for carrying out appropriate decontamination if hazardous material is spilt on or inside the instrument. Sample Preparation Sample preparation for ICP spectroscopy may require the handling of organic or corrosive solutions.
Page 43: Dissolving Solid Samples Using Acids
Sample Preparation When selecting a solvent, consider the following: • Is the solvent compatible with the equipment? Aliphatic hydrocarbons, ketones and esters, alcohols, and xylene, are the most frequently used solvents. Make sure that all equipment that will come into contact with the solvent is compatible with the solvent, e.g., tubing, sample cups, storage and waste containers, etc.
Page 44: Acid Digestions
Safety Practices Acid Digestions Acid digestions, either at atmospheric pressure or at increased pressure, require special care. Spattering and foaming of the sample/acid mixture may expose the user to a hazard, as well as compromise the sample integrity. A digested sample containing concentrated acid will react violently with water.
Page 45 Sample Preparation • Always wear suitable protective equipment, including goggles, a face shield, acid-resistant gloves, and protective clothing when using hydrofluoric acid. • Do not breathe HF vapors. Always work in a fume hood when using hydrofluoric acid. • Do not use a glass beaker. Hydrofluoric acid attacks glass. •...
Page 46: Fusion Mixtures
Decontamination and Cleaning Before using any cleaning or decontamination methods except those specified by PerkinElmer, users should check with PerkinElmer that the proposed method will not damage the equipment. Decontamination Customers wishing to return instrumentation and/or associated materials to PerkinElmer for repair, maintenance, warranty or trade-in purposes are advised that all returned goods must be certified as clean and free from contamination.
Page 47: Cleaning The Instrument
The customer's responsible body is required to follow the "Equipment Decontam- ination Procedure" and complete the "Certificate of Decontamination". These documents are available on the PerkinElmer public website. http://las.perkinelmer.com/OneSource/decontamination.htm If you do not have access to the internet and are located in the U.S., call toll free at 1-800-762-4000 or (+1) 203-925-4602, 8:30 a.m.
Page 48: References
Safety Practices References 1. Furr, K., ed., CRC Handbook of Laboratory Safety, 5th ed., The Chemical Rubber Co. Press, 2000. 2. National Research Council, Prudent Practices for Handling Hazardous Chemicals in Laboratories, National Academy Press, Washington, D.C., USA, 1981. 3. Compressed Gas Association (USA), "Safe Handling of Compressed Gases in Containers,"...
Page 49: Chapter 2: Preparing Your Laboratory
Preparing Your Laboratory...
Page 50: Environmental Conditions
Free of excessive vibration. • Altitude: in the range -400 to 2,000 m (sea level to 6,562 feet) The Optima 8000 has been designed for indoor use. Do not use the instrument in an area where explosion hazards may exist. Pollution Degree: This product will operate safely in environments that contain nonconductive foreign matter up to Pollution Degree 2 in EN/IEC 61010-1.
Page 51 Preparing Your Laboratory Exhaust Vent Requirements The Optima 8000 requires an exhaust vent to remove combustion fumes and vapors from the torch compartment. Exhaust venting is important for the following reasons: • It protects laboratory personnel from toxic vapors that may be produced by some samples.
Page 52 Compartment Chimney located on top of the sample compartment. For proper instrument venting, order PerkinElmer Venting Kit (Part No. 03030447 Kit for 115 V or Part No. 03030448 Kit for 230 V) by contacting your PerkinElmer sales representative. The minimum distance from the top of the instrument’s Torch Compartment Chimney to the bottom of the extraction vent should be 7.5-12.5 cm.
Page 53 Preparing Your Laboratory Figure 2-1 Location of the Torch Compartment Chimney and Vent. Item Description Recommended Vent Width: 30.6 cm (12 in.) Depth: 15.3 cm (6 in.) Height: 30.6 cm (12 in.) Torch Compartment Chimney 28 cm (11 in.) from the instrument edge to the chimney center 7.5 to 12.5 cm (3 to 5 in.)
Page 54 The Optima 8000 weighs 146 kg (321 pounds), or 201 kg (442 pounds) with the shipping container. The Optima 8000 may be placed on a bench. The main power cable length is 2.4 m (8.0 ft.). To provide access for servicing and space for ventilation, allow at least 61 cm (24 in.) of space between the instrument and the laboratory walls.
Page 55 Preparing Your Laboratory Figure 2-2 Outside Dimensions of the Optima 8000 Instrument. Item Description 76 cm (30 in.) 81 cm (32 in.) 132 cm (52 in.) PolyScience Chiller ® The PolyScience WhisperCool (or equivalent) is usually located on the floor, to the right side of the instrument.
Page 56: Cooling Water Requirements
A PolyScience Recirculating Chiller meets these requirements and is recommended ® for the instrument. The PolyScience WhisperCool chiller is available through PerkinElmer in the following two configurations: • 230V, 60 Hz (Part No. N0772046) • 240V, 50 Hz (Part No. N0772045) ®...
Page 57: Optima 8000
• Optima 8000 requires an AC line voltage of 200 - 230 VAC +/-10% (180 - 253 VAC) 50/60 Hz. +/-1% under full instrument load, that has a correctly wired protective earthing system (ground connection) and a separate circuit breaker.
Page 58 As an alternative you can use the following receptacle part numbers which can be directly ordered from Hubble. For the US/Canada (20A service) use PerkinElmer Part Number 09997529 Hubble Part No. C320R6SVL or C320R6W. For Europe (16A service) use Hubble Part No.
Page 59: Argon
Pneumatic Requirements Argon Liquid or gaseous argon can be used with the Optima 8000 system. The use of liquid or gaseous argon tanks is determined primarily by the usage rate. Liquid argon is usually less expensive per unit volume to purchase, but cannot be stored for extended periods.
Page 60: Shear Gas
Preparing Your Laboratory Shear Gas Air or nitrogen can be used to shear the plasma for the Optima 8000. The Optima 8000 RF generator typically consumes the shear gas at a rate of 25 L/min. The flow rate should be approximately 25 L/min (1.0 cu. ft/min).
Page 61 Preparing Your Laboratory...
Page 62: Chapter 3: System Description
System Description...
Page 63: Introduction
This modular system design facilitates system access, testing and servicing. NOTE: All illustrations in this guide are based on the Optima 8000 instrument. The spectrometer for the Optima 8000 consists of the following modules: •...
Page 64 System Description Figure 3-1. The Optima 8000. Item Description Sample Introduction Compartment with the Quick Change Adjustable Torch Module (inside) Peristaltic Pump Torch Compartment Spectrometer...
Page 65: Transfer Optics
System Description Spectrometer Introduction The core of the optical system comprises a dual Echelle monochromator with a dual, backside-illuminated, cooled, CCD detector. The system is specifically designed for ICP-OES. Computer controlled transfer optics direct the radiation from the plasma into the monochromator. The optics housing is sealed and continuously purged with high purity nitrogen.
Page 66 System Description 88 1 Figure 3-2 Schematic diagram of the optical system. Item Description Radial View Transfer Optics Mirrors Echelle Grating...
Page 67: Monochromator
System Description Item Description Detector Parabolic Collimators Prism (internally reflective face) Entrance Slit Intermediate Slit (This is where the neon reference beam enters) Torch Axial View Transfer Optics Mirrors Echelle Grating Detector Parabolic Collimators Prism (i internally reflective face) Entrance Slit Intermediate Slit (This is where the neon reference beam enters) This mirror moves out of the optical path for Axial viewing.
Page 68 System Description Wavelength selection is achieved by simultaneous rotation of the prism and grating. Since the maximum rotation required for either element is not more than ± 2°, the average wavelength selection time is less than 2 seconds. To further optimize the analysis time, the wavelengths required are sorted to minimize the change-over time between any two consecutive wavelengths.
Page 69: Detector
System Description Figure 3-3 Monochromator Item Description Echelle Grating Detector Intermediate Slit Fiber optic for the neon reference beam. Entrance Slit Prism Detector The detector is a two-dimensional CCD device containing approximately 25,600 pixels. The photosensitive area is separated into two differently sized arrays that are used for separate reference and analytical measurements.
Page 70 System Description The rear of the actual detector area is thinned to a few micrometers to allow illumination from the rear. This prevents the absorption of radiation by components other than the detector pixels and maximizes the quantum efficiency without the use of a fluorescent coating.
Page 71 System Description Item Description CCD Array Output Register for the reference measurement. 3 mm At 240 nm the array covers a wavelength range of approximately 0.52 nm, and at 850 nm, approximately 25 nm. Thus the emission line for the analyte of interest and emission on each side of the analytical line fall simultaneously on the array.
Page 72: Wavelength Correction
System Description Figure 3-5 Storage of photoelectrons during integration. Item Description Photons Photosensitive Register Register Wavelength Correction The optical system uses a two-component, active wavelength stabilizing system. The overall stability is controlled by temperature and pressure sensors in the optics housing.
Page 73: Icp Source
The photons from the torch are detected optically and measured electronically in the spectrometer section of the Optima 8000. It is displayed in terms of wavelength and intensity, which are converted to sample concentration.
Page 74 System Description Figure 3-6 Block diagram illustrating the RF Power Control (RFPC) Item Description AC Power Input 40 MHz RF Power Generator RF Power to Plasma Induction Plates Plasma Control Feedback Signal...
Page 75: Rf Control Electronics
System Description Item Description Power Measurement Signal RF Power Control Loop Microprocessor RF Control Electronics The RF generator uses solid-state circuits. The solid state RF generator is designed to significantly increase reliability and reduce the need for recalibration. The RF generator also monitors plasma conditions. If the plasma is unstable, the system automatically shuts it off.
Page 76: Nebulizers
Scott-type spray chamber and the GemTip Cross-Flow pneumatic nebulizer are one of the standard configurations. This rugged combination provides the best results for a variety of elements and sample types. Nebulizers PerkinElmer offers these nebulizers for a wide variety of applications: Description/Part No. Uses/Advantages GemTip Cross-Flow...
Page 77 System Description MEINHARD Type C Used for samples containing high dissolved solids (up to 20%). 00472022 MEINHARD Type K Optimized for samples that require reduced nebulizer gas flow rates, such as N0681574 organic-based samples. For samples with low analyte and low matrix concentrations. Typically U-6000AT Ultrasonic improves detection limits by a factor of 10 over conventional pneumatic...
Page 78 System Description Figure 3-8 GemCone nebulizer and end cap N0680343 (also shown in cross-sec- tional view).
Page 79: Nebulizer Heater (Optional)
System Description Figure 3-9 Concentric glass nebulizer and end cap N0680343 (also shown in cross-sectional view). Nebulizer Heater (optional) The nebulizer heater allows you to set the temperature of the spray chamber enclosure to provide a constant temperature for the spray chamber. The nebulizer heater ensures maximum long-term stability even as room temperature varies.
Page 80: Peristaltic Pump
TubingSaver mode is a feature for extending the life span of pump tubing. Autosampler PerkinElmer offers autosamplers for automated sample handling. These autosamplers consist of a sample table, a sample tray, and a motorized sampling arm with an attached probe. Different sample trays are available for each autosampler, covering a variety of sample volume and total sample capacity requirements.
Page 81: Software Controls
System Description EMO Switch The EMO switch, , is the illuminated red switch on the front of Emergency Off Switch the instrument. If it is blinking slowly the instrument is in the middle of an ignition cycle.It blinks rapidly after the Emergency Off Switch is depressed. This is an indication that the switch has been depressed and to remind you to push the switch again to release it.
Page 82 System Description • Nebulizer argon flow rate: The flow rate is automatically controlled using a mass flow controller in 0.01 L/min increments. • Pump rate: By specifying the desired flow rate (adjustable in 0.1 mL/min increments) and the tubing diameter, the software calculates the pump speed. •...
Page 83: Connections To Electrical, Gas, And Cooling Water Supplies
System Description Connections to Electrical, Gas, and Cooling Water Supplies See the following figure. Marking Function Main power switch. Connections for remote control of accessories. Do not exceed the stated voltage and current: Umax = 30 V AC, Imax = 0.5 A AC Umax = 30 V DC, Imax= 2 A DC IEEE 488.2 IEEE-488 cable 0999-1355 to connect instrument to the computer.
Page 84 System Description Figure 3-11 Electrical, gas, and cooling water connections on the spectrometer side of the instrument. Item Description Gas Connections Ar Supply Shear Gas Supply...
Page 85: System Initialization
System Description Item Description N 2 Supply Coolant IN Coolant OUT IEEE Computer Connection Terminal strip (Part No. 09987900) for chiller remote operation Power Switch Instrument to 200-240 VAC, 16 AMP, IEC-309 Outlet White Tie Wrap (Part No. N0770342) Red Tie Wrap (Part No. N0770341) Chiller System Initialization When you switch on the spectrometer:...
Page 86: Technical Data
System Description Technical Data General Inductively coupled plasma optical emission spectrometer. Principle Computer controlled, using a special application program running under a graphical user interface. 200 to 240 V AC ~, 50/60 Hz Power requirements Power consumption 2800 VA (maximum) Insulation: Class I Electrical protection...
Page 87: Gas Flow Controls
System Description Cooling Water: System requires a flow of 1 gal/min at 310 to 550 kPa at a temperature between 15 °C and 25 °C. A recirculating cooling system is required ® (PolyScience WhisperCool chiller or equivalent is recommended). Automatic Ignition: Plasma ignition is computer controlled and totally automated. The plasma can be turned on at a set time, warming up the system prior to an analysis, and can be turned off automatically after an analysis.
Page 88: Optical System
System Description Spray Chamber: Scott-type designed to minimize pulsations from the peristaltic pump and constructed of Ryton for complete corrosion resistance to most acids, including HF, and all organic solvents normally used in ICP analyses. Nebulizer: Cross-flow design with chemically resistant GemTips manufactured from corrosion-resistant (sapphire tips in a PEEK body) material.
Page 89: Chapter 4: Installation
Installation...
Page 90: Installation Summary
200 kg (440 pounds) with the shipping container. If the instrument needs to be moved please contact PerkinElmer Service. A PerkinElmer service engineer should install your system for the first time or help you in moving the system. This chapter is provided for your reference should you need information on moving the system, or reinstalling accessories.
Page 91: Setting Up The Computer And Printer
Moving the Instrument Caution f moving the Optima 8000 will subject the instrument to any freezing temperatures you must contact a PerkinElmer service engineer to assist you in the move. The PerkinElmer service engineer will flush all traces of cooling water from the RF generator to prevent freezing of RF generator components.
Page 92: Connecting The Gases And Cooling Water
Installation procedures later in this chapter Installing the Quick-Change Adjustable Torch Module on page 107. Connecting the Gases and Cooling Water After the instrument has been moved into its position, it can be connected to the various services in the laboratory. Connecting the Gases All gas hose connections use 1/4 inch Swagelok fittings.
Page 93 Installation Figure 4-1. Pneumatic, water and shear gas connections. Item Description Air Supply Air/ N 2 Shear Gas and RF Cooling Gas Supply N 2 Supply Out (water Hose with White Tie Wrap) Cooling Water In (Water Hose with Red Tie Wrap) Cooling minimum pressure no maximum...
Page 94 An air hose (Part No. N0770348) with 1/4-in. Swagelok fittings at each end, is supplied in the hose kit that is shipped with the instrument. A second air hose is also included. The following procedure describes how to connect the PerkinElmer air compressor, filter and regulator.
Page 95 (125 °F). At a higher pressure, the filter bowls can be blown off and cause injury. The following procedure describes how to set the shear gas pressure when using the PerkinElmer Air Dryer Filter. 1. Make sure the shut-off valve on the Air Dryer Filter is closed (knob turned fully clockwise), then set the air pressure on the air compressor to between 550 kPa and 825 kPa (5.5 to 8.25 bar or 80-120 psig).
Page 96: Connecting The Polyscience Chiller
PolyScience WhisperCool chiller. ® The PolyScience WhisperCool is available through PerkinElmer in the following two configurations: 208/230V, 60 Hz 220/240V, 50 Hz Connecting the Chiller to the Instrument Teflon tape (PTFE tape) should be used for all pipe-thread (NPT) fittings.
Page 97: Remote Chiller Connections
The chiller can be turned on or off via the software. Your service engineer will connect the remote cable (Part No. N0770175) from the chiller to the Optima 8000 so that the chiller can be operated remotely. See the following figure for the location...
Page 98 Installation Figure 4-2 Remote chiller connections. Item Description Terminal Strip Part No. 09987900 (For Chiller Remote) Coolant Out 3/8 in. Space Collars (Part No. 09920584) Remote Cable (Part No. N0770175)
Page 99 Initiating WinLab 32 will have no effect on the chiller if the chiller is already on. If the Optima 8000 Spectrometer is in Sleep or Standby mode and the instrument is still ignited, the chiller will remain on. If the instrument is not ignited in Sleep or Standby mode the chiller will turn itself off.
Page 100 Installation Figure 4-3 Water flow diagram with the chiller Item Description Terminal Strip Part No. 09987900 (For Chiller Remote) 3/8 in. Space Collars (Part No. 09920584) Remote Cable (Part No. N0770175) Coolant Out (Part No. N0770342) White Tie Wrap...
Page 101 Installation Item Description Coolant In (Part No. N0770341) Red Tie Wrap Line Cord Plug Chiller Filling the PolyScience Chiller ® Use the following procedure to fill the PolyScience WhisperCool Chiller, and refer to the following figure. 1. Turn the filler cap counter clockwise and lift the cap off. 2.
Page 102: Starting Up The Polyscience Chiller
Installation Figure 4-4 Filling the chiller. Item Description Reservoir Plug Starting Up the PolyScience Chiller ® Check the following before starting up the PolyScience WhisperCool Chiller: • All plumbing connections are tight. • The chiller reservoir is full. • The chiller power cord is plugged in.
Page 103: Connecting The System Components
Note: Extending IEEE cables by making tandem connections will compromise instrument communication. • The Optima 8000 is equipped with an IEC 309 250 V 16/20A 2 pole plus protective earth plug (PerkinElmer Part No. 09997530) that inserts into an equivalent IEC 309 series receptacle (see Section 2, Electrical Requirements).
Page 104 Installation Caution Risk of damage to the instrument. Make sure that signals from accessories connected to the instrument connector do not exceed: Vmax = 30 V AC, Imax = 0.5 A AC Vmax = 30 V DC, Imax = 2 A DC...
Page 105 Installation Figure 4-5 System component connections. Item Description Power Cord Instrument to 200-240 VAC 16 AMP (Europe) 20 AMP (US) IEC-309 Outlet Computer...
Page 106: Installing The Quick-Change Adjustable Torch Module
Installation Item Description IEEE Cable Part No. 09991355 Computer to Instrument Autosampler IEEE Cable Part No. 09991355 Computer to Autosampler Printer AC Outlet Installing the Quick-Change Adjustable Torch Module The Quick-Change Adjustable Torch Module is shipped pre-assembled as one unit. It includes the torch, spray chamber, injector, and nebulizer.
Page 107 Installation 3. Firmly slide the torch coupler, clockwise, into the torch mount so the two locking lugs and guide pin in the torch coupler engage the channels in the torch mount. Rotate the torch coupler completely clockwise until it cannot be rotated any further.
Page 108 Installation Figure 4-6 Installing the torch through the torch mount. Item Description End View of Torch Coupler (Spray Chamber removed) Align markings as shown before engagement procedure shown below. Torch Coupler Locking Lugs Guide Pin Channels Torch Mount...
Page 109 Installation 5. Make sure that the Ground Pointer is in close proximity to the end of the torch glass but not inside the torch glass. If needed, push the Ground Pointer gently slightly towards the rear of the torch box. Also make sure that the inner glass tube in the torch is positioned 1.5 mm from the last turn of the plasma induction plates.
Page 110: Connecting The Nebulizer (Neb) Tubing
Installation Connecting the Nebulizer (NEB) Tubing 1. Connect one end of the nebulizer (NEB) tubing to the nebulizer end cap and the other end to the quick disconnect. 2. For more detailed instructions on connecting the tubing, see Table 5-7 on page 213.
Page 111 Installation Figure 4-8 Nebulizer (NEB) connections to torch and nebulizer end cap. Item Description Nebulizer (NEB) Argon Tubing (Detail) Quick Disconnect (Detail) Left Side of Instrument Quick Disconnect...
Page 112: Installing The Autosampler
Drain Tubing Waste Vessel Installing The Autosampler The instrument can be used with the PerkinElmer S10 Autosamplers. The following procedures describe the electrical connections necessary to install the PerkinElmer autosamplers. After the autosampler is installed, the software must be configured for the type of autosampler you are using.
Page 113 Installation Figure 4-9 Electrical connectors and switches located on the underside of the autosampler. 2. Place the autosampler either adjacent to the spectrometer or on top of the spectrometer. When used alone, the autosampler is connected directly to the nebulizer's sample tube.
Page 114 Installation Figure 4-10 Electrical connection for the S10 autosampler to the Optima spec- trometer. Item Description Instrument Serial Communication Cable (Part No. 09290259) Autosampler Com 1 Power Plug-In Power Supply...
Page 115 Installation 3. Connect the RS232/serial communication cable provided, between the Com 1 port on the underside of the autosampler (as shown in Figure 4-10 on page 115) and one of the Com ports on the PC. 4. Connect the autosampler to the line power supply using the plug-in power supply provided.
Page 116: Fitting And Connecting The Autosampler Sampling Probe
Installation Fitting and Connecting the Autosampler Sampling Probe When you fit the sampling probe, take care not to press forcefully Caution in any direction on the autosampler arm since this can damage the arm. The sampling probe is a complete assembly. Do not attempt to take the probe apart as this will damage it, and reassembly is not possible.
Page 117 Installation The standard sampling probe is a PTFE-lined epoxy polymer tube. This Note polymer is resistant to the acids, alkalis and organic solvents normally used in atomic spectroscopy. If your samples contain an organic solvent that attacks this polymer, a PTFE-lined stainless steel sampling probe is offered as an option (B3000152).
Page 118: Adjusting The Sampling Probe Height
Installation Adjusting the Sampling Probe Height The procedure described below assumes that you are using a spectrometer Note operated via ICP WinLab software. If you are using an AA or ICP-MS instrument, please refer to the information on operating an autosampler in the online help for the respective instrument.
Page 119 Installation Figure 4-12 Inserting the sampling probe. Item Description Sampling Probe Rinsing Probe This completes installation of the sampling probe. For detailed information on adjusting the sample probe height and connecting the sample tube between the sample probe and the spectrometer’s sample input system see the S10 Autosamplers User’s Guide (Part No.
Page 120: Setting The Torch Viewing Position
Installation Setting the Torch Viewing Position This procedure adjusts the torch viewing position for the highest signal intensity. Perform this procedure when: • the instrument or software is first installed • the instrument is moved to a new location • the torch is removed or replaced •...
Page 121: Switching On The System
Installation Select Manganese, which is typically used as the alignment wavelength for the majority of analyses. -or- Select another element from the drop-down list. This feature is for specialized analyses where you want to optimize the intensity for an individual analyte of interest. This may adversely affect the intensities of other analytes.
Page 122: Setting Instrument Parameters
Installation • Purge gas: 2.75 to 8.25 bar or 40-120 psig. 3. Make sure that the torch is correctly installed, the torch compartment door is shut, and the EMO switch is released. 4. Make sure the drain vessel is empty. 5.
Page 123: Instrument Settings For Aqueous Solutions
Installation Instrument Settings for Aqueous Solutions Aqueous Organics RF power: 1500 watts 1500 watts Nebulizer Flow: 0.6 L/min 0.4-0.5 L/min (for Cross-Flow Nebulizer) Auxiliary Flow: 0.2 L/min 1.0-1.5 L/min Plasma Flow: 15 L/min 15 L/min Sample Flow Rate: 1.5 to 2.5 mL/min 3.0 mL/min Equilibration Time: 8 sec...
Page 124: Hardware Settings And Options
Instructions for removing the window that are given in Removing and Cleaning the Windows on page 168. • PerkinElmer offers different types of nebulizers for a wide variety of applications. For descriptions of the nebulizers and their different uses and advantages, see Nebulizers on page 76.
Page 125: Shipping List
Installation Shipping List Every day you count on PerkinElmer to provide you with solutions that deliver reliable performance, control operating costs and maximize operational time. Our complete portfolio of consumables, parts, supplies, training and service helps you meet both routine and demanding measurement challenges. We invest heavily in testing and validating our products to ensure you receive guaranteed compatibility and performance - on-time, every time, for every instrument in your laboratory.
Page 126: Maintenance
Installation Table 4-2. Shipping Kit (Part No. N0780011) Part No. Description Quantity 02113330 Product Certification 09401056 PCB-PCI/GPIB 09991356 Cable Assembly-IEEE N0770425 Receptacle-AC Power 250 Volt N0770432 Installation Kit N0771014 Shipping Pack N0780200 Instrument Assembly N0780433 Spares Kit N0800439 Window and O-Ring DV Spares Kit N0780607 Torch Assembly-ADJ Cyclonic/Conc For FP Table 4-3.
Page 127 Installation Table 4-4. Spares Kit (Part No. N0770433) Part No. Description Quantity 00473550 Solvent Flex Pump Tubing, 0.76 mm ID, (Black/Black-Sample Tubing) 02506516 Tygon Tubing 1/4 in. OD x 1/8 in. ID 0.98 feet 02506532 Organic Drain Tubing 0.63 feet 09902033 O-Ring for Cross Flow Nebulizer End Cap 09903730...
Page 128: Maintenance
Alumina Injector, 2.0 mm ID, 141mm LG N0775220 Air Filter for RF Generator N0781097 Copper Foil for Dual View Torch Glassware Table 4-5. Spares Available for the Optima 8000 Part No. Description Documentation N0582325 Concepts, Instrumentation and Techniques in ICP-OES...
Page 129 Installation Table 4-5. Spares Available for the Optima 8000(Continued) Software: N0777030 CD-ROM ICP WinLab32 Software Peristaltic Pump Tubing 09908585 PVC Pump Tubing, 1.14 mm ID, Red/Red (Drain Tubing) 09908587 PVC Pump Tubing, 0.76 mm ID, Black/Black (Sample Tub- ing) 00473550 Solvent Flex Pump Tubing, 0.76mm ID, Black/Black (Sample...
Page 130 Installation Table 4-5. Spares Available for the Optima 8000(Continued) N0770358 Low Flow Gemcone Nebulizer N0690670 High Solids GemCone Nebulizer N0770336 Quick Disconnect Tubing Assembly for GemCone Nebulizer N0680504 End Cap for GemCone Nebulizers 00473194 O-Ring (for Nebulizer Seal on N0680504 End Cap)
Page 131 Installation Table 4-5. Spares Available for the Optima 8000(Continued) N0775358 Eluo Nebulizer Cleaner N0770351 Drip Tray for Nebulizer Compartment N0691709 CETAC U-6000AT+ Ultrasonic Nebulizer System, 115V, 50/ 60 Hz N0691710 CETAC U-6000AT+ Ultrasonic Nebulizer System, 230V, 50/ 60 Hz N0690770...
Page 132 Installation Table 4-5. Spares Available for the Optima 8000(Continued) N0774080 UniFit Drain Connector with Tubing for Cyclonic Spray Chambers (1/16in. OD x 0.75mm ID x 700mm LG) WE024372 4mm Liquid-End Connector N8122258 Pump Tubing Adapter N8120160 O-Rings for Cyclonic Spray Chamber (PK/10)
Page 133 Installation Table 4-5. Spares Available for the Optima 8000(Continued) N0776025 Nut for Injector Adapter N0776036 Injector Seal Nut N0776091 DV Injector Adapter (1.2mm ID) N0770448 Dual View Nut Wrench Assembly Sample Introduction System and Related Parts 09904991 Drain Bottle (Carboy 15 Liter)
Page 134 09921057 Purge Outlet O-Ring Radial Purge Tube N0690672 09992731 Axial Purge Window N0800439 Spares Kit - Dual View Attachment Optima 8000 Filters 09995098 Air Filter for Spectrometer N0775220 Air Filter for RF Generator N0775325 Air Dryer Filter Assembly with R250 Regulator...
Page 135 Spares Kit N0770433 N0770437 O-Ring Kit for the Dual View Torch Periscope O-Ring Kit for Injector Support Adapter N0770438 Spares Kit - Dual View Attachment Optima 8000 N0770439 Miscellaneous 09401056 PCB-PCI/GPIB N0690360 Peristaltic Pump Head Assembly with Stainless Steel Rollers...
Page 136: Chapter 5: Maintenance
Maintenance...
Page 137: Introduction
You should perform only the maintenance procedures described in this chapter. Record your daily maintenance procedures in the ICP-OES Maintenance Log (Part. No. 09936225). If additional maintenance is required, contact a PerkinElmer service engineer. This instrument requires no specified inspection or preventive maintenance to ensure the continuous functioning of its safety features.
Page 138: Purge Gas Supply
Nitrogen output pressure: 275-825 kPa (40-120 psig) Shear Gas Supply The Optima 8000 requires a supply of shear gas. The shear gas used is typically compressed air; however, nitrogen may also be used. Make sure that an adequate supply of shear gas is available and connected to the system. Check that the supply has sufficient pressure, and that a spare cylinder is ready if necessary.
Page 139: Nebulizer
Maintenance Caution T o extend the life and aid in preventing devitrification of glassware, it is necessary to remove all traces of alkali on glassware caused by handling it with bare hands. To remove the alkali, wipe the glassware clean with cotton wool dipped in alcohol.
Page 140: Periodic Checks
The plasma induction plates must be kept clean to prevent arcing across the plasma induction plates. Inspect the plasma induction plates for any deformations or carbon buildup. Contact your PerkinElmer Service Representative to replace the plasma induction plates if there are any signs of pitting. Pitting causes weakness in the plasma induction plates which can result in a hole in the plasma induction plates and a gas leak.
Page 141: Spray Chamber
Maintenance Spray Chamber Check for leaks around the nebulizer and drain fitting. Inspect the spray chamber for deposits and check the condition of the O-rings. Peristaltic Pump Check that the pump rollers are clean, not scored, free from deposits due to spills, and move freely.
Page 142: Torch Viewing Position Alignment
Maintenance Torch Viewing Position Alignment The torch viewing position alignment procedure is used to set the plasma viewing position of the spectrometer entrance optics for the highest signal intensity.See Setting the Torch Viewing Position on page 121. Perform this procedure when: the instrument is first installed or moved to a new location, or the torch is removed or replaced, or the plasma induction plates is replaced (important)
Page 143 Maintenance Table 5-1. Recommended Cleaning Procedure (Continued) GemTip or GemCone Clean with soap and water; rinse thoroughly. Nebulizer/End Cap Assembly Concentric Glass Do not use an ultrasonic cleaner. Do not use a cleaning (MEINHARD) wire. See Concentric Glass Nebulizer later in this Nebulizer chapter.
Page 144: Quick-Change Adjustable Torch Module
Maintenance Quick-Change Adjustable Torch Module The Quick-Change Adjustable Torch Module consists of the torch assembly, spray chamber, and nebulizer. These components are easily removed from the system for regular inspection and maintenance. Normal wear on these components is shown by metal or salt deposits on the quartzware or injector, glazed or devitrified quartz, worn O-rings, or clogged nebulizer tips.
Page 145: Plasma Induction Plates
Maintenance Figure 5-1. Quartz Torch. Item Description Torch Plasma Induction Plates Slot Plasma Induction Plates Regularly inspect the plasma induction plates. It should not show any signs of deforming or pitting. If your lab has high humidity, check the plasma induction plates to make sure it is dry.
Page 146: Removing The Scott Spray Chamber
Maintenance and adjust the plasma induction plates refer to the procedure, see Replacing the Plasma Induction Plates on page 166. Removing the Scott Spray Chamber 1. Place the sample tubing in deionized water and turn on the pump to flush the spray chamber.
Page 147 Maintenance Figure 5-2 Removing the spray chamber assembly. Item Description Left Side of Instrument Front of Instrument Drain Tubing Spray Chamber...
Page 148: Removing And Disassembling The Torch
Maintenance Item Description Clamp Torch Coupler Injector Lock Injector Removing and Disassembling the Torch 1. Turn off the plasma if it is on. If the plasma has been on, the torch glass will be very hot and can cause serious burns. Wait five minutes after turning off the plasma before you begin these maintenance procedures.
Page 149 Maintenance Figure 5-3 Removing the torch coupler from the torch mount. Item Description Spray Chamber Clamp Nebulizer Torch Coupler Torch Glass Torch Mount Torch Holder Spray Chamber 4. Pull open the clamp that holds the spray chamber in place. The action of opening the clamp will partially push the spray chamber out.
Page 150 O-rings and damage the O-ring seats. Replace with new O-rings. An Injector Adapter O-ring kit is available from PerkinElmer (Part No. N0770438). n the next step, be sure to carefully remove the torch so you will avoid breaking the glassware and risking possible injury.
Page 151: Cleaning The Torch
Maintenance Figure 5-4 Disassembling the torch. Item Description Torch Coupler Torch Holder O-Rings After installation, you will need to perform the Torch Viewing Position Alignment Procedure described in Chapter 4, Installation. Cleaning the Torch The torch components should be cleaned regularly to remove accumulated deposits. After prolonged use, a torch may lose its transparency and become crystalline.
Page 152: Replacing The Torch
Maintenance The copper foil ignitor (Part No. N0781097) contact must be removed Caution from the torch glassware before it is cleaned in acid. Replace a new piece of copper foil tape over the ignitor hole in the torch after the glass is clean and dry.
Page 153 Maintenance mark on the torch mount and the guide pin on the torch coupler. Firmly tighten the knurled nut. See the following figure. Figure 5-5 Replacing the torch. Item Description Torch Glass (Part No. N0780131) Copper Foil (Part No. N0781097) Torch Cutout...
Page 154 Maintenance Item Description Knurled Nut (Part No. N0776027) Washer (Part No. N0776028) O-Ring (Part No. 09902223) Spacer (Part No. N0776029) O-Ring (Part No. 09921061) O-Ring (Part No. 09921062) O-Ring (Part No. 09902131) Torch Coupler Stripe on Torch Index Mark on Torch Holder Guide Pin If the torch glass does break, discard the broken torch and replace (Part No.
Page 155 Maintenance For a complete set of spare Injector Adapter O-rings order Kit (Part No. Note N0770438). Figure 5-6 Using the injector positioning tool to remove O-rings. Item Description Injector Positioning Tool Use this end to remove Injector Seal Nut Injector Seal Nut Injector Seal (open side up)
Page 156 Maintenance Figure 5-7 Inserting the injector. Item Description Torch Coupler Spray Chamber Clamp (Part No. N0776031) Injector (Part No. N0781014)
Page 157: Replacing The Torch On The Mount
Maintenance Item Description O-Rings (Part No. 09921028) Injector Adapter (Part No. N0776024) O-Rings (Part No. 09902207) Washer (Part No. N0770602) Locking Collar (Part No. N0776025) Injector Lock Knurled Nut Use this end to remove O-Rings Injector Positioning tool (Part No. N0770602) Torch Injector (1 1/2 mm set below the inner glass) Injector Positioning tool (Part No.
Page 158 Maintenance 3. For proper ignition, turn the torch coupler fully clockwise and continue an additional 2 mm from where you want to go. For example, if you want the torch set in the -3 position, turn clockwise to -5 position and then return the torch coupler to -3 position.
Page 159 Maintenance Figure 5-8 Assemble the torch assembly to the mount. Item Description End View of the Torch Coupler (Spray chamber removed) Align markings as shown before starting engagement procedure shown next. Torch Coupler Locking Lug Guide Pin...
Page 160 Maintenance Item Description Locking Lug Channels Torch Mount 4. Carefully slide the torch through the plasma induction plates. Make sure that the Ground Pointer is in close proximity to the end of the torch glass but not inside the torch glass. If needed, gently push the Ground Pointer slightly towards the rear of the torch box.
Page 161 Maintenance Figure 5-9 Positioning of torch in the sample compartment. Item Description Front of Instrument, Torch Compartment Door Open Torch Plasma Induction Plates Ground Pointer Ignitor Contact Finger Copper Foil 5. Check that the injector is flush or slightly below the inner glass tube of the torch. If the injector tube is not seated properly an air leak could occur or sample could drip into the torch.
Page 162: Replacing The Spray Chamber
Maintenance Replacing the Spray Chamber 1. Orient the spray chamber so that the drain connection is facing down and towards the rear of the sample compartment. See the following figure. 2. Check the condition of the two O-rings (Part No. 09921028) on the spray chamber/injector adapter.
Page 163 Maintenance Figure 5-10 Nebulizer (NEB) connections to torch and nebulizer end cap. Item Description Nebulizer (NEB) Argon Tubing Quick Disconnect Detail Instrument Left Side...
Page 164: Replacing The Plasma Induction Plates
Maintenance Item Description Quick Disconnect Nebulizer (NEB) Argon Tubing Drain Tubing Waste Vessel Sample Capillary Tubing Replacing the Plasma Induction Plates Plasma Induction Plates Regularly inspect the plasma induction plates. It should not show any signs of deforming or pitting. If your lab has high humidity, check the plasma induction plates to make sure it is dry.
Page 165 Maintenance Table 5-2. Replacement Parts: Torch Module (Continued) N0770600 Torch Module (no spray chamber or nebulizer) Part No. Description N0770602 Torch Assembly Injector Seal N0770603 Injector Adapter Assembly (includes O-Rings but no injector) N0770606 Dual View Torch Module (includes Torch, Glassware, Injector (Alumina Injector, 2.0mm ID), Scott-type Spray Chamber &...
Page 166: Windows
Maintenance Windows Removing and Cleaning the Windows If the plasma has been on, the torch will be very hot and can cause serious burns. Wait five minutes after turning off the plasma before you begin these maintenance procedures. Warning Gradually, deposits may accumulate on the windows, for example, metallic oxides, and the windows may become etched.
Page 167 Maintenance Remove the two screws that hold the shear gas nozzle assembly in position and move the assembly carefully to one side See the following figure. Figure 5-11 Purge Window Item Description Torch Axial Window to Purge Extension Shear Gas Nozzle Screws Retaining Ring Radial Window...
Page 168: Cleaning The Windows
Maintenance 4. Remove the O-ring that holds the axial window in the mount and remove the window. 5. Unscrew and remove the radial window retaining ring. 6. Lift the radial window and O-ring out of the mount — take care if the spectrometer purge is set to high and you have not removed the axial window, the pressure inside the spectrometer may force out the radial window.
Page 169 Maintenance 1. Install the O-ring in the radial window mount. 2. Place the retaining ring loosely over the mount. 3. Hold the radial window with an optical-quality cloth. Carefully push the open end of the cylinder through the O-ring right to the base of the mount. The closed end must be at the top.
Page 170: Replacing The Axial Window
Maintenance Replacing the Axial Window Do not leave fingermarks on the window. Use an optical cloth to handle Note the window. 1. Hold the axial window with an optical-quality cloth and refit the window in the mount. 2. Install the O-ring that holds the window in the mount. 3.
Page 171 Maintenance Figure 5-13 Replacing the axial window. Item Description Axial Snout Radial Window (Part No. N0690672) O-Ring (Part No. 09921036) Radial Window Mount Axial Window (Part No. 09992731) Axial Window O-Ring (Part No. 09921062) Purge Outlet O-Ring (Part No. 09921057)
Page 172: Replacing And Adjusting The Shear Gas Nozzle
Maintenance Replacing and Adjusting the Shear Gas Nozzle Risk of heat damage to the axial window. Never set the nozzle slit behind Caution the front edge of the axial window mount. The basic shear gas nozzle position is with a 1 to 2 mm gap between the nozzle slit and the front edge of the axial window mount.
Page 173: Adjusting The Position Of The Shear Gas Nozzle
Maintenance Adjusting the Position of the Shear Gas Nozzle Risk of heat damage to the axial window. Never set the nozzle slit behind Caution the front edge of the axial window mount. The basic shear gas nozzle position is with a 1 to 2 mm gap between the nozzle slit and the front edge of the axial window mount.
Page 174: Scott-Type Spray Chamber
Maintenance Scott-Type Spray Chamber Check the spray chamber periodically for leaks around the nebulizer end cap and drain fitting. Examine the end cap O-ring for cracking and wear and replace if necessary. Deposits and plated out metals can accumulate in the spray chamber, which can introduce “memory effects.”...
Page 175: Cleaning The Scott-Type Spray Chamber
Maintenance Figure 5-14 Spray chamber, end cap, and associated parts. (Illustration shows cross-flow nebulizer end cap assembly, Part No. N0770546.) Item Description Spray Chamber (Part No. N0770357) O-Ring (Part No. 09902033) End Cap Ring (Part No. 00473543) End Cap (Part No. N0681688 not complete assembly) Knurled Screw (2) (Part No.
Page 176: Cyclonic Spray Chamber
Maintenance if necessary. Acid solutions must be used with care. Observe all of the manufacturer's safety recommendations. These recommendations are normally provided in a material safety data sheet (MSDS) supplied with the chemical. If you have been analyzing organic solutions, the spray chamber can be cleaned using a solvent or diluted soap solution.
Page 177 Maintenance The large baffled (8 mm) and unbaffled cyclonic spray chamber can be Note ordered with or without a cap. The narrow baffled (4 mm) cyclonic spray chamber assembly (Part No. N0776090) does not come with a cap. You must order this cap separately as needed. A cap (Part No. N0770614) does not have to be ordered with every replacement cyclonic spray chamber.
Page 178 Maintenance Figure 5-15 Installing the cyclonic spray chamber into the cyclonic spray chamber cap. Item Description Cyclonic Spray Chamber...
Page 179 Maintenance Item Description Cyclonic Spray Chamber Cap (opened position) Cyclonic Spray Chamber (seated in cap) Cyclonic Spray Chamber Cap (closed position) 3. Slide the chamber onto the injector adapter. Close the clamp to secure the cyclonic spray chamber assembly in place. Tighten the nut at the end of the cyclonic spray chamber assembly.
Page 180 Maintenance Figure 5-16 Installing the cyclonic spray chamber. Item Description Torch Coupler Cyclonic Spray Chamber Tygon Tubing (Part No. 02506516) Tubing Coupler (Part No. 09920186)
Page 181: Etching The Cyclonic Spray Chamber
Maintenance 5. To the open end of the tubing coupler (Part No. 09920186) connect the drain tubing to the peristaltic pump tubing. See the procedure Installing the Drain Tubing on page 221 later in this chapter for information on connecting the drain tubing to the drain bottle.
Page 182 Maintenance Cleaning the Cyclonic Spray Chamber If you have been analyzing aqueous solutions, the spray chamber should be cleaned in an acid bath. An ultrasonic bath may be used. Start with a solution of 5% nitric acid or aqua regia and, if deposits persist, increase the acid concentration, up to 20% if necessary.
Page 183: Nebulizers
Oil or Organics Analysis Nebulizers PerkinElmer offers different types of nebulizers for a wide variety of applications. For descriptions of the nebulizers and their different uses and advantages, refer to Chapter 3, System Description. Part numbers and replacement parts for the different types of nebulizers are listed on the next page.
Page 184 Maintenance Table 5-5. Nebulizer Flow Rates Concentric Glass 0.55 L/min 0.4 - 0.95 L/min (MEINHARD) Type K Ultrasonic 0.5 L/min Mira Mist 0.55 L/min 1 L/min Table 5-6. Replacement Parts: Nebulizers and End Caps Part No. Description 00472020 MEINHARD Nebulizer (Type A, General purpose) 00472022 MEINHARD Nebulizer (Type C, High dissolved solids) 00473194...
Page 185: Gemtip Cross-Flow Nebulizer
Maintenance Table 5-6. Replacement Parts: Nebulizers and End Caps N0770546 GemTip Cross-Flow II Nebulizer N0775330 PEEK Mira Mist Nebulizer N0776006 Nebulizer Adapter for Cyclonic Spray Chamber N0776007 O-Rings for Nebulizer Adapter GemTip Cross-Flow Nebulizer The following procedures cover the maintenance of the GemTip Cross-Flow nebulizer supplied with the instrument.
Page 186: Removing The Nebulizer/End Cap
Maintenance When checking the spray pattern of the nebulizer pump only use deionized water. Do not use any other solution. Warning Removing the Nebulizer/End Cap To remove the nebulizer/end cap assembly: 1. Turn off the plasma if it is on. If the plasma has been on, allow one minute for the Quick-Change Adjustable Torch Module to cool and an additional two minutes for the torch to cool before handling.
Page 187: Checking The Spray Pattern
Maintenance Figure 5-17 The nebulizer/end cap assembly removed from the spray chamber. Il- lustration shows cross-flow nebulizer end cap assembly. Item Description Cross-Flow GemTip Nebulizer End Cap Assembly (Part No. N0770546) Knurled Screw (Part No. 00473539) Knurled Screw (Part No. 00473539) Spray Chamber (Part No.
Page 188: Disassembling The Cross-Flow Nebulizer
Maintenance When checking the spray pattern of the nebulizer pump only use deionized water. Do not use any other solution. Warning 1. Set the nebulizer argon flow to 1.0 L/min. 2. Place the sample capillary tubing in a beaker of deionized water and start the pump at a rate of 1.0 mL/min.
Page 189 Maintenance Figure 5-18 Cross-section of GemTip Cross-Flow Nebulizer shown with Cross- Flow End Cap, N0770546. Item Description Clear GemTip Red GemTip Argon Inlet Sample Inlet To begin disassembling the nebulizer: 1. If you have not already done so, remove the nebulizer/end cap assembly from the spray chamber.
Page 190: Removing The Sample Tip From The End Cap, N0770546
Maintenance 2. Disconnect the sample capillary tubing by removing it from the pump tube. 3. Disconnect the nebulizer argon tubing at the gas fitting. Do not disconnect nebulizer argon tubing from the end cap because the GemTip could fall out. 4.
Page 191 Maintenance Figure 5-19 Clear GemTip for sample inlet and associated parts for Cross-Flow End Cap, N0770546. Item Description O-Ring (Part No. 09921045) Clear GemTip Nebulizer (Sample Inlet Available in GemTip Kit Part No. N0690676) Ferrule (Part No. 09920518)
Page 192 Maintenance Item Description Nut (Part No. 09920546) 1/16 inch O.D. teflon Tubing Piece (Part No. 09985708) Sample Capillary Tubing 5. Check the condition of the tubing piece (Part No. 09985708). If the tubing is worn, replace it as follows: • Obtain a new piece of 1/16-in.
Page 193: Removing The Argon Tip From The End Cap, N0770546
Maintenance 7. With the tubing and ferrule assembled as shown in the previous figure, screw the nut into the sample inlet making a finger-tight connection. Do not use any tools to tighten the nut. 8. Examine the two GemTips in the end cap. These tips should almost butt up to each other at an angle of 90 .
Page 194 Maintenance Figure 5-21 Red GemTip for argon inlet and associated parts for Cross-Flow End Cap (Part No. N0770546). Item Description End Cap O-Ring (par No. 09902033) O-Ring (Part No. 09921045) Red GemTip Nebulizer -Argon Inlet (Part No. N0690676) Ferrule (Part No. 09920515) Nut (Part No.
Page 195 Maintenance 6. Check the condition of the argon inlet tubing (Part No. 09985723). If the tubing is worn, replace it as follows. See the next figure. a. Obtain a new piece of 1/8-in. O.D. teflon tubing (Part No. 09985723). b. Using a razor blade, make a straight cut on one end of the tubing. Wire cutters or scissors do not make acceptable cuts.
Page 196: Connecting The Nebulizer Argon Tubing (Cross-Flow End Cap, N0770546)
Maintenance Connecting the Nebulizer Argon Tubing (Cross-Flow End Cap, N0770546 1. Pass the tubing (Part No. 09985723) through the nut (Part No. 09920545) and attach the ferrule (Part No. 09920515) on the end of the tubing. See the following figure. 2.
Page 197 Maintenance Figure 5-23 Connecting the nebulizer argon tubing. Cross-Flow End Cap (Part No. N0770546). Item Description Instrument Left Side 1/8 inch O.D. Tubing (Part No. 09985723) Nut (Part No. 09920545)
Page 198: Replacing The Nebulizer/End Cap
Maintenance Item Description Ferrule (Part No. 09920515) Quick Disconnect-Male (Part No. N0775206) Quick Disconnect-Female (Part No. N09920861) Nut (Part No. 09920545) Ferrule (Part No. 09920515) Replacing the Nebulizer/End Cap Before replacing the end cap: • Check the end cap O-ring (Part No. 09902033) for nicks or cracks. If you need to replace the O-ring, remove the two knurled screws and the end cap ring.
Page 199: Gemcone Nebulizer
Maintenance GemCone Nebulizer Daily Cleaning of the Low-Flow GemCone Nebulizer Each day after use, the low-flow GemCone nebulizer should be rinsed out by pumping deionized water to the nebulizer for several minutes. This should be done with both the plasma on and the nebulizer gas on. This helps prevent the formation of salt crystals near the exit of the nebulizer gas orifice.
Page 200: Installing The Gemcone Nebulizer On The Scott-Type Spray Chamber
Maintenance Installing the GemCone Nebulizer on the Scott-Type Spray Chamber To install the GemCone nebulizer on the Scott-type spray chamber, the end cap assembly (Part No. N0680504) and the tubing assembly (Part No. N0770336) must be used. 1. Remove the existing nebulizer/end cap assembly (if the wrong one is installed) by loosening the knurled nuts on the end cap.
Page 201 Maintenance Figure 5-24 Installing the GemCone nebulizer to a Scott-type spray chamber. Item Description End Cap Assembly (Part No. N0680504) Knurled Nut-2 (Part No. 00473539) Capillary Tubing (Part No. 09908265) GemCone Nebulizer Assembly Argon Gas Fitting Tubing Assembly (Part No. N0770336)
Page 202: Installing The Gemcone Nebulizer On The Cyclonic Spray Chamber
Maintenance Installing the GemCone Nebulizer on the Cyclonic Spray Chamber 1. Before inserting the GemCone nebulizer into the chamber, connect the argon gas fitting to the nebulizer threads. First, tighten the gas fitting by hand. Tighten the fitting another 1/8 of a turn using a 9/16-in. open-end wrench. Support the nebulizer with a back-up wrench when tightening or loosening fittings.
Page 203 Maintenance Figure 5-25 Connecting the GemCone nebulizer to the cyclonic spray chamber. Item Description Torch Coupler Cyclonic Spray Chamber Tubing Assembly for the GemCone Nebulizer (Part No. 0770336) Argon Gas Fitting GemCone Nebulizer Assembly Teflon Tubing-1 inch (Part No. 09985708) Capillary Tubing (Part No.
Page 204: Cleaning The Gemcone Nebulizer
Maintenance Cleaning the GemCone Nebulizer With routine use it may become necessary to perform a thorough cleaning. 1. Remove the nebulizer from the end cap (loosen both thumbscrews). 2. Disconnect the argon gas fitting and the capillary tube connection from the nebulizer.
Page 205 Maintenance 1. Wet the outside of a short length of tubing cut from pump tubing (Part No. 00473550 or 09908587). Insert this tubing as far into the concentric nebulizer as possible. 2. After you have inserted this Viton Orange-Orange tubing, cut the tubing so that one inch extends out from the nebulizer.
Page 206 Maintenance Item Description 2.54 cm or 1 inch Clamp Argon Line 4. With an adapter connect the argon tubing from the nebulizer to the NEB/ NEBULIZER fitting. 5. Insert the Concentric Glass nebulizer, as far as it will go, through the opening in the end cap.
Page 207: Cleaning The Concentric Glass Nebulizer
Cleaning the Concentric Glass Nebulizer For detailed information on cleaning MEINHARD Concentric Glass nebulizer, see Maintenance Tips for Users of the MEINHARD Concentric Glass Nebulizer (PerkinElmer Part No. 099936334), which is also available upon request from J.E. Meinhard Associates, Inc. J.E. Meinhard Associates, Inc.
Page 208 Maintenance (714) 250-3332 Internet address: http://www.meinhard.com The following table summarizes the cleaning procedures for the MEINHARD Concentric Glass nebulizer. Figure 5-28 Cleaning Strategy for the MEINHARD Nebulizer. (Reprinted with the permission of JE Meinhard Assoc., Inc.) When cleaning the concentric glass nebulizer, do not use ultrasonic Caution cleaning.
Page 209: Mira Mist Nebulizer
Maintenance Mira Mist Nebulizer This device operates on compressed gases. Appropriate care must be taken. If in doubt about correct operating procedures, call an experienced operator. Burgener Mira Mist Nebulizers require 45 - 55 psi to have a 1 liter per minute of Argon gas flow, so the Warning operating pressures are in the range of 25 - 45 psi, depending on the torch optimum flow rate.
Page 210: Gas Line
The gas line terminates in the Optima 8000 quick disconnect. It is a direct replacement for typical concentric nebulizers.
Page 211: Peristaltic Pump
Maintenance Peristaltic Pump The peristaltic pump requires routine maintenance to ensure that the system will run properly. The pump tubing should be replaced when flat spots develop (on a daily basis or after approximately eight hours of use). When replacing the pump tubing, the drain tubing should be replaced at the same time since uneven wear can cause the spray chamber to back up.
Page 212: Installing The Sample And Drain Tubing
Maintenance Installing the Sample and Drain Tubing The peristaltic pump is used to pump sample into the nebulizer and pump the waste out of the spray chamber. Figure 5-29 Tubing installed on pump for sample and drain (side view). Item Description From Spray Chamber To Nebulizer...
Page 213: Installing The Sample Tubing
Maintenance Installing the Sample Tubing To install the sample tubing refer to the instructions below and the next two figures: 1. Turn off the peristaltic pump using the software control. 2. Take a piece of 0.76 mm (0.030 in.) pump sample tubing. New pump tubing will work better if it is pre-stretched and analytical precision will be improved.
Page 214 Maintenance Figure 5-30 Peristaltic pump tubing installed with cover in place. Item Description Cover Door Spray Chamber Peristaltic Pump Tubing...
Page 215 Maintenance Make sure that the closed cover door does not pinch the tubing. If the Caution tubing is pinched, pressure will build up in the pump tubing and liquid will not flow. 4. Take two pieces of 0.58 mm i.d. (0.023 in.) polyethylene tubing (Part No. 09908265), one for the sample capillary and one for the nebulizer capillary.
Page 216: Connecting The Drain Tubing Assembly
Maintenance Item Description Pump Tubing 0.76 mm i.d. (different part numbers available) Polyethylene tubing (including with the Nebulizer, 0.58 mm i.d. Part No. 09908265) To Sample Inlet 6. Insert the beveled end of the nebulizer capillary tubing into the other end of the pump tubing.
Page 217 Maintenance 3. Use the other end of the tubing coupler (Part No. 09920186) to connect the drain tubing to the peristaltic pump. Drain tubing with 1 mm i.d. (0.04 in.) can also be used by following these steps: 1. Attach a small piece of 1.5 mm (0.06 in.) i.d. PVC tubing (Part No. 09985729) to the barbed fitting (Part No.
Page 218 Maintenance Figure 5-32 Drain tubing assembly. Item Description Barbed Fitting (Par t No. 09920267) Adapter (Part No. N0695414) Sleeve (Part No. N0695415) Spray Chamber...
Page 219: Installing The Drain Tubing
Maintenance Item Description PVC Tubing 1.5 mm i.d. (Part No. 09985735) Coupler (Part No. 09920186) Pump Tube 1.14 mm i.d. Teflon Tubing 1 mm i.d. (Part No. 09985708) Drain bottle Installing the Drain Tubing Install the drain tubing on an open channel of the peristaltic pump as follows: 1.
Page 220: Adjusting The Pump Tubing
Maintenance Adjusting the Pump Tubing Adjust the tension on the sample and drain tubing, one at a time, using deionized water as follows: Adjusting the Sample Tubing 1. Make sure the sample tubing is centered in the channel, then place the clamp around the tubing and swing back the cam lever.
Page 221: Cleaning The Pump
Maintenance 5. Loosen the adjustment screw until the bubbles stop moving. 6. Tighten the adjustment screw slowly until the bubbles just start moving again. 7. Tighten the adjustment screw until the bubbles move in a segmented flow (about 1/2 to 1 turn on the peristaltic pump). 8.
Page 222: Removing The Pump Head On The Peristaltic Pump
Replace the washer and tighten the screw. Drain One drain is used on the Optima 8000. This pumped drain leads from the spray chamber. To connect the drain to the drain bottle, refer to the next figure and follow the steps below: 1.
Page 223 Maintenance Figure 5-33 Tubing connections to the drain bottle. Item Description Sample Compartment Spray Chamber PVC Tubing 1.5 mm i.d. (Part No. 09985735) Coupler (Part No. 09920186)
Page 224: General System Maintenance
Maintenance Item Description Drain Tubing Piece 1.6 mm i.d. (Part No. 02506241) Teflon Tubing 1 mm i.d. (Part No. 09985708) Pump Tubing 1.14 mm i.d. Peristaltic Pump General System Maintenance Cleaning the Instrument Exterior surfaces may be cleaned with a soft cloth, dampened with a mild detergent and water solution.
Page 225: Changing The Spectrometer Air Filter
Maintenance Changing the Spectrometer Air Filter The filter for the spectrometer cooling is inside the snap-on plastic grid. Refer to Figure 5-34. 1. Shut down and switch off the spectrometer. 2. Carefully pull off the plastic grid on the ventilator. 3.
Page 226: Changing The Neon Lamp
Maintenance Changing the Neon Lamp The neon lamp (Part No. B0810144) is in an assembly that plugs into a connector on the right-hand side of the optics tub. A panel in the side of the spectrometer housing gives access to the neon lamp. Refer to Figure 5-34. 1.
Page 227: Fuses
Maintenance Figure 5-35 Location of the filter on the chiller. Item Description Chiller Water Filter (remove in this direction) Fuses Fuses may only be replaced by a PerkinElmer service engineer.
Page 228: Replacement Parts: General
Maintenance Replacement Parts: General Every day you count on PerkinElmer to provide you with solutions that deliver reliable performance, control operating costs and maximize operational time. Our complete portfolio of consumables, parts, supplies, training and service helps you meet both routine and demanding measurement challenges. We invest heavily in testing and validating our products to ensure you receive guaranteed compatibility and performance - on-time, every time, for every instrument in your laboratory.
Page 229 Maintenance Table 5-11. Gas and Water Supply Connections Part No. Description N0690275 Nitrogen Supply Hose N0770341 Water Supply Hose N0770342 Water Drain Hose N0770348 Shear Gas Supply Hose N0775220 Air Filter for RF Generator N0775325 Air Dry Filter Assembly with R250 Regulator N9306067 Replacement Filter Element (for Air Dryer Filter Assem- bly)
Page 230 Maintenance Table 5-13. Organic Sample Introduction Kit (Part No. N0770420) Part No. Description 09902207 O-Ring (for Torch Adapter - inside) 09921028 O-Ring - Metric (for seal Spray Chamber to Injector Adapt- N0770358 Low Flow GemCone Nebulizer N0770614 Cap for either the Baffled or Unbaffled Cyclonic Spray Chamber N0772005 Quartz Torch (3 Slot)
Page 231 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description 00472020 MEINHARD Nebulizer (Type A, General purpose) 00472022 MEINHARD Nebulizer (Type C, High dissolved solids) 00473194 O-Ring (for Nebulizer Seal on N0680504 End Cap) 00473539 Knurled Screw used on End Cap 00473550 Solvent Flex Pump Tubing, 0.76mm ID, Black/Black (Sample tubing)
Page 232 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description 09903730 Nipple, 1/16 to 1/8 09904845 Cooling Water Filter 09904846 Replacement Cooling Water Filter Cartridge (for 09904845 Water Filter) 09904991 Drain Bottle (Carboy 15 Liter) 09908265 Polyethylene Tubing, Sample Capillary 09908585 PVC Pump Tubing, 1.14mm ID, Red/Red (Drain tubing) 09908587...
Page 233 Solvent Flex Pump Tubing, 1.14mm ID, Red/Red (Drain Tub- ing) 09923383 Cap Sleeve 0.406 in. Brown Vinyl 09936225 ICP-OES Instrument Maintenance Log Book 09936877 Hardware Guide Optima 8000 09936889 Unpacking Instructions Optima 8000 09985708 PTFE Tubing 0.031 x 0.016 09985723 1/8 in. OD Teflon Tubing 09985729 PVC Tubing 1.5mm ID...
Page 234 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0680504 End Cap for GemCone Nebulizers N0681574 MEINHARD Nebulizer (Type K, Reduced flow and organics) N0690271 Drain Bottle Cap Assembly N0690274 Argon Supply Hose N0690275 Nitrogen Supply Hose N0690360 Peristaltic Pump Head Assembly with Stainless Steel Rollers N0690670...
Page 235 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0770336 Quick Disconnect Tubing Assembly for GemCone Nebulizer N0780131 Quartz Torch N0770341 Water Supply Hose N0770342 Water Drain Hose N0770343 Long Torch (for organics and high dissolved solids) N0770346 Arm Lifting Assembly N0770348...
Page 236 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0770602 Tool Assembly Injector Seal N0770603 Injector Adapter Assembly (includes O-Rings but not injector) N0770605 Cyclonic Spray Chamber with Cap for Aqueous Solutions N0770608 External Spray Chamber Mount for use with high-volatility organic solutions N0770609 Stand for Dual View Torch Assembly...
Page 237 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0774077 Unifit Drain Connector with Tubing for Cyclonic Spray Chambers (1.3mm OD x 0.75mm ID x 700mm LG) N0774080 UniFit Drain Connector with Tubing for Cyclonic Spray Chambers (1/16in. OD x 0.75mm ID x 700mm LG) N0775014 Quartz Injector, 2.0mm ID, 141mm LG N0775220...
Page 238 Maintenance Table 5-15. All Replacement Parts by Part Number Part No. Description N0775348 MicroMist Nebulizer (0.7 L/min. Ar flow rate, 0.1 mL/min. uptake rate) N0775349 MicroMist Nebulizer (0.7 L/min. Ar flow rate, 0.05 mL/min. uptake rate) N0775356 Cyclonic Spray Chamber (O-Ring Free) N0775358 Eluo Nebulizer Cleaner N0776006...
Page 239: Ordering Supplies, Accessories, And Replacement Parts
4mm Liquid-End Connector Ordering Supplies, Accessories, and Replacement Parts Every day you count on PerkinElmer to provide you with solutions that deliver reliable performance, control operating costs and maximize operational time. Our complete portfolio of consumables, parts, supplies, training and service helps you meet both routine and demanding measurement challenges.
Page 240 If you are located within the U.S., call toll free 1-800-762-4002, 8 a.m. to 8 p.m. EST. Your order will be shipped promptly, usually within 24 hours. If you are located outside of the U.S., call your local PerkinElmer sales or service office.
Page 241: Chapter 6: Troubleshooting
Troubleshooting...
Page 242 A Word on Troubleshooting We recommend that you consult the troubleshooting information included here before you call a PerkinElmer service engineer. The Troubleshooting chapter contains suggestions to help you determine systematically whether instrument problems are due to improper analytical techniques, improper selection of instrument parameters, or malfunction of the instrument.
Page 243: Troubleshooting
Troubleshooting What the Performance Checks Measure The tests in this section allow the operator to measure performance aspects of the instrument. If you are experiencing problems with your results, these tests can pinpoint the cause of the problem. The tests include the following: •...
Page 244: Troubleshooting
Troubleshooting Sodium Bullet Test To run the sodium bullet test: 1. For aqueous analyses, aspirate a 1000 mg/L solution of sodium. For organic analyses, aspirate an appropriate organic blank. 2. Examine the plasma through the viewing window in the sample compartment door.
Page 245: Performance Problems
Do the pump rollers bind or not roll easily? Are there grooves in the pump rollers? On the PerkinElmer pump, the pump head may be removed for cleaning. The pump head may also be replaced. A pump head with stainless steel rollers is available. See Removing the Pump Head on the Peristaltic Pump on page 224.
Page 246 Troubleshooting Nebulizer and Spray Chamber Is there leakage around the end cap? Is there leakage from the spray chamber drain? Is fluid accumulating in the torch? Make sure the end cap is on securely. If you cannot get a secure fit, the end cap O ring may need to be replaced.
Page 247 Troubleshooting Purge Window Is the purge window cloudy or dirty? Rinse with deionized water and dry with a soft cloth. Or, replace if necessary. Do not touch the window. If oils from the skin are deposited on the window, this can cause inaccurate results.
Page 248 Troubleshooting Performance Problems: Troubleshooting Table Table 6-1. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action RSD (Relative The sample introduction Refer to Cleaning the Sample Standard Deviation) system may not be set up Introduction System on page 144. greater than 1%. correctly or may require maintenance.
Page 249 Troubleshooting Table 6-1. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action Cannot obtain You may not be comparing the Refer to the Winlab32 Software Guide suggested BEC value appropriate BEC value for the on the WinLab CD for details. wavelength you are using.
Page 250 Troubleshooting Table 6-1. Performance Problems: Troubleshooting Table Problem Possible Cause(s) Corrective Action Results Standard solutions may have Rerun proven standards. erroneously low been improperly made. Blank solution may be Remake the blank solution. Acidify the contaminated or not matrix- blank if the sample matrix is acidified. matched to the standards.
Page 251 Troubleshooting Table 6-1. Performance Problems: Troubleshooting Table Cannot get suggested The sample introduction Refer to Chapter 4, Maintenance. detection limits system may not be set up correctly, or may require maintenance. The BEC may be high. Run the BEC test. Refer to the Winlab32 Software Guide on the WinLab CD for details.
Page 252: Plasma Ignition And Stability Problems
Troubleshooting Plasma Ignition and Stability Problems Plasma Ignition Problems Possible reasons for unsuccessful ignition follow. Correct the problem, if possible, and then try to ignite the plasma again. • If the plasma will not light check the ignitor. Open the door to the sample compartment.
Page 253: Plasma Stability Problems
Troubleshooting flows on for approximately two minutes. Then turn off the pump and try to reignite the plasma again. • Optics Interlock. Check that the optics is centered over the torch. Problems with ignition may be due to the optics having been bumped out of the correct position.
Page 254: Printing Problems
Troubleshooting • Be sure that the injector you are using is recommended for the types of solvents you are using. The quartz injector, 1.2 mm i.d., is recommended for typical organic analyses. The alumina injector, 0.85 mm i.d., should be used with volatile organic solvents, for example, methanol.
Page 255 Check the rollers in the pump head to Rollers may be stuck. see if they roll freely. Tubing may be worn. Replace tubing. Pump makes excessive A mechanical problem may Call a PerkinElmer service engineer. noise have occurred.
Page 256 Troubleshooting Autosampler Problems Table 6-4. Autosampler Problems Problem Possible Cause(s) Corrective Action Autosampler does not There may be a GPIB Use the Instrument Diagnostics respond communication problem. window to reset the autosampler. The software may not be In the System menu, click on configured for the autosampler Configure Autosampler.
Page 257: Troubleshooting Form
Troubleshooting RF Generator/Sample Introduction System Troubleshooting Form Fill out the following form before you contact PerkinElmer service. Troubleshooting Form General: Instrument Serial Number: Site: Date: Sample Introduction Configuration: Nebulizer Type:CROSS FLOW / LF GEMCONE / MEINHARD Spray Chamber Type:SCOTT / CYCLONIC / BAFFLED CYCLONIC Injector Type:QUARTZ / ALUMINA Injector Bore (mm):0.8 / 1.2 / 1.6 / 2.0 / 3.0...
Page 258: Instrument Environment
Troubleshooting Operating Conditions: RF Power:W Plasma Gas Flow:/min Aux Gas Flow:l/min Nebulizer Gas Flow:l/min Sample Uptake Rate:ml/min Sample Compartment Heater:C Torch Position:mm Distance between Injector tip and Aux Tube:mm Instrument Environment: Lab Temperature:C C Vent Distance from Exhaust:mm Line Voltage:V Line FrequencyHz Chiller Temperature Setting: C...
Page 259 Troubleshooting Common Setup Problems: Glassware bottomed out in torch body (Glassware Holder):Yes/No Glassware aligned with notch in torch body (Glassware Holder):Yes/No Copper tape covering igniter spark hole:Yes/No Igniter finger contacting copper tape:Yes/No Ground rod located near end of glassware but outside of glasswareYes/No Fiber Optic located over glassware and is not melted or recessed:Yes/No Torch position appropriate for sample type:Yes/No Aqueous = -3, Organics = -3, High Solids = -1...
Page 260 Troubleshooting Troubleshooting Tasks Performed: Did the plasma light:Yes/No Did the plasma stay lit after ignition:Yes/No Plasma went out after pump turned on:Yes/No Plasma went out after how long of operation: Plasma went out with Warm Wet Plasma (neb on, pump on, heat on):Yes/No Plasma went out with Cold Wet Plasma (neb on, pump on, no heat):Yes/No Plasma went out with Dry Plasma (neb on, no pump):Yes/No Plasma went out when injector capped off:Yes/No...
Page 261 Troubleshooting Figure 6-2 Normal Plasma at -3mm position Figure 6-3 Rounded Plasma due to sample or air getting around the outside (typ- ically subtle air leak)
Page 262 Troubleshooting Figure 6-4 Aux Gas too high, Air Leak, or Spray Chamber Temperature too high Figure 6-5 Injector too far forward Figure 6-6 No Aux Gas (Torch may be glowing)
Page 263 Troubleshooting Figure 6-7 Air Leak or Spray Chamber Temperature too high Figure 6-8 Thin Plasma due to leak in Plasma Gas Line...
Page 264: Error Messages
Error Messages...
Page 265: Error Messages
The following messages are listed numerically by error code. No Error There is no error. No corrective action is needed. Vds out of The drain to source Contact PerkinElmer Service. voltage voltage across the tolerance power FET transistor window is out of the Tolerance window.
Page 266: Error Messages
In this case, the RF Oscillator Assembly must be replaced. Contact PerkinElmer Service. Ids 2 out of The drain to source Contact PerkinElmer Service. level 2 current across the window power FET transistor 2 is out of the level 2...
Page 267 Failed to set AUX to Check argon supply, argon pressure, AUX set AUX a value specified in flow tubing and connections. If this does not flow to the AUX Setting correct the problem, contact PerkinElmer specified Flow Controls Service. level window.
Page 268 Torch not Torch interlock Contact PerkinElmer Service. installed switch not satisfied. Door open Door ajar or not Close the RF door to correct this error sensed closed. message. If closing the door does not clear this error message, contact PerkinElmer Service.
Page 269 Neb flow attain the nebulizer tips for blockage. Check the argon lines from flow. Pneumatics board for crimping. If this does not correct the problem, contact PerkinElmer Service. Failed to The instrument has Check the argon lines for crimping. If this...
Page 270 Ignition and Stability Problems on page detecting but the plasma is not 255for more information. If this does not plasma on. The fiber optic correct the problem contact PerkinElmer during will do a hardware Service. ignition shutdown. Not used...
Page 271 If it is being pushed out of the than the other plasma induction plates correct the air leak or transistor. Both AUX flow. If this does not correct the transistors should problem, contact PerkinElmer Service. have an equal current within tolerance limits. +24 V This fatal message Contact PerkinElmer Service.
Page 272 Ignition and Stability Problems on page plasma detecting the plasma 255for more information. If this does not but the plasma is not correct the problem contact PerkinElmer Service. Ids 1 not 0 Drain to source Contact PerkinElmer Service. current across the...
Page 273 (<10 L/m) Control Dialog into the instruments. If this does not solve the window is too low, or problem, contact PerkinElmer Service. not enough inlet pressure and flow to sustain the plasma gas flow.
Page 274 Check the water valve. The valve maybe stuck on frozen open or the flow switch may need to be replaced. If the solid-state relay is on and the water is on, the flow sensor could be stuck on flow. Contact PerkinElmer Service.
Page 275 Error Messages Error Parameters for the Contact PerkinElmer Service. reading ignite command for post-ignite the power setting are power invalid. setting Error Parameters for the Contact PerkinElmer Service. reading ignite command for post-ignite the AUX flow are AUX flow invalid.
Page 276 Otherwise the instrument is fully heater off heater is now off. functional. Contact PerkinElmer Service to have the nebulizer compartment heater repaired.
Page 277 Index coolant recommended daily checks Acid Digestions electrical requirements Adjusting the Sampling Probe Height 102, 103 filling Air Filters filters general maintenance requirements maintenance starting periodic checks Coil, RF RF generator, changing see RF Coil spectrometer, changing Computer Alignment configuration and setup torch viewing position Connections Argon...
Page 278 Index Dissolving Solid Samples Fusion Mixtures in organics using acids Gas Cylinders Drain handling 141, 255 daily checks identification periodic checks storing safety practices Gas Supply tubing, connecting replacement parts Drain Tubing Gases adjusting connecting, instructions connecting connections at back of instrument 214, 221 installing Hardware Settings...
Page 279 Index general information daily checks moving the instrument end cap, removing Quick-Change Adjustable Torch Module end cap,replacing fuses 126, 129 shipping list GemCone nebulizer summary GemCone nebulizer, cleaning Installation Kit GemTip Cross-Flow nebulizer items included general system Instrument Handling nebulizer 142, 143 Instrument Parameters periodic checks...
Page 280 Index concentric glass nebulizer, maintenance Optics Interlock concentric glass, cleaning checking concentric glass, installing Optimization Cross-Flow nebulizer argon tip, removing Organic Vapors checking Cross-Flow nebulizer sample tip, removing Organics and plasma stability Cross-Flow nebulizer spray pattern, check- checking Cross-Flow nebulizer, disassembling Perchloric Acid daily checks Performance Checks...
Page 281 Index Plasma Induction Plates replacing purge windows Plasma Parameters torch module recommendations Replacement parts by part number Plasma Torch RF Control Electronics periodic maintenance RF Generator Pneumatic Requirements RF Power laboratory requirements RF Radiation Printer safety practices configuration and setup troubleshooting problems with Safety Information Pump Tubing...
Page 282 Index Sample Compartment monochromator description transfer optics Sample Introduction System wavelength correction autosampler Spray Chamber cleaning checking 154, 177 description cleaning inspection of description nebulizer end cap,removing peristaltic pump inspecting Quick-Change Adjustable Torch Module maintenance torch periodic checks 148, 176 Sample Preparation removing Sample Tubing...
Page 283 Index Torch Module part numbers Torch Viewing Position Alignment Procedure 121, 144 Transfer Optics Troubleshooting autosampler problems general information performance problems performance problems, table plasma ignition problems plasma stability problems printing problems pump problems Ultraviolet Radiation safety practices Viewing Warnings symbols used on instrument Waste Disposal Procedures Water Filter...
Page 285 PerkinElmer, Inc. 710 Bridgeport Avenue Shelton, CT 06484-4794, U.S.A. Internet: http://www.perkinelmer.com email: info@perkinelmer.com PerkinElmer is a registered trademark of PerkinElmer, Inc.

PerkinElmer OPTIMA 8000 Customer Hardware And Service Manual

Chapter 1: Safety Practices

Chapter 2: Preparing Your Laboratory

Chapter 3: System Description

Chapter 4: Installation

Chapter 5: Maintenance

Chapter 6: Troubleshooting

Quick Links

Troubleshooting

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Summary of Contents for PerkinElmer OPTIMA 8000