PerkinElmer OPTIMA 8000 Spectrometer Manuals

Manuals and User Guides for PerkinElmer OPTIMA 8000 Spectrometer. We have 1 PerkinElmer OPTIMA 8000 Spectrometer manual available for free PDF download: Customer Hardware And Service Manual

PerkinElmer OPTIMA 8000 Customer Hardware And Service Manual

PerkinElmer OPTIMA 8000 Customer Hardware And Service Manual (285 pages)

ICP OPTICAL EMISSION

Brand: PerkinElmer | Category: Laboratory Equipment | Size: 3.15 MB

Table of Contents

Table of Contents
5
Customer Service
13
Safety and Regulatory Information
14
Using this Guide
25
Documents to Help You
25
How this Guide Is Organized
26
- Using the Index
  27
- A Word on Troubleshooting
  27
Chapter 1: Safety Practices

29
- Introduction
  30
- Laboratory Guidelines
  30
  - General
    30
  - Environmental Conditions
    31
  - Pollution Degree
    31
  - Handling of the Instrument
    31
  - Laboratory Ventilation
    31
- Instrument Safety Practices
  32
  - Safety Interlocks
    32
  - Radio Frequency Radiation
    33
  - Ultraviolet Radiation
    33
  - Electrical Safety
    33
  - High Temperatures
    35
  - Hot Exhaust Gases
    35
  - Safe Use of Drain Systems
    36
  - Waste Disposal Procedures
    36
- WEEE Instructions for Perkinelmer Products
  37
- Safe Handling of Gas Cylinders
  38
- Sample Preparation
  42
  - Dissolving Solid Samples in Organics
    42
  - Dissolving Solid Samples Using Acids
    43
  - Acid Digestions
    44
  - Fusion Mixtures
    46
- Decontamination and Cleaning
  46
  - Decontamination
    46
  - Cleaning the Instrument
    47
- References
  48
Chapter 2: Preparing Your Laboratory

49
- Environmental Conditions
  50
- Exhaust Vent Requirements
  50
- Cooling Water Requirements
  56
  - Optima 8000
    57
  - Argon
    59
  - Purge Gas
    59
  - Shear Gas
    60
  - Regulator
    60
Chapter 3: System Description

62
- Introduction
  63
  - Transfer Optics
    65
  - Monochromator
    67
  - Detector
    69
  - Wavelength Correction
    72
- ICP Source
  73
  - RF Generator
    73
  - RF Control Electronics
    75
- Sample Introduction System
  75
  - Sample and Torch Compartments
    75
  - Quick-Change Adjustable Torch Module
    75
  - Nebulizers
    76
  - Nebulizer Heater (Optional)
    79
  - Peristaltic Pump
    80
  - Autosampler
    80
- Switches and Controls
  80
  - Main On/Off Switch
    80
  - Interlocks
    80
  - Software Controls
    81
- Connections to Electrical, Gas, and Cooling Water Supplies
  83
- System Initialization
  85
- Technical Data
  86
  - General
    86
  - ICP Plasma Generator System
    86
  - Gas Flow Controls
    87
  - Sample Introduction System
    87
  - Optical System
    88
Chapter 4: Installation

89
- Installation Summary
  90
- Setting up the Computer and Printer
  91
- Moving the Instrument
  91
- Connecting the Gases and Cooling Water
  92
  - Connecting the Gases
    92
- Connecting the Polyscience Chiller
  96
- Connecting the System Components
  103
- Installing the Quick-Change Adjustable Torch Module
  106
  - Connecting the Nebulizer (NEB) Tubing
    110
- Installing the Autosampler
  112
  - Fitting and Connecting the Autosampler Sampling Probe
    116
  - Adjusting the Sampling Probe Height
    118
- Setting the Torch Viewing Position
  120
- Switching on the System
  121
- Setting Instrument Parameters
  122
- Shipping List
  125
  - Maintenance
    126
  - Maintenance
    128
Chapter 5: Maintenance

136
- Introduction
  137
- Daily Checks
  137
  - Daily Cleaning
    137
  - Argon Supply
    137
  - Purge Gas Supply
    138
  - Shear Gas Supply
    138
  - Chiller
    138
  - Vent
    138
  - Torch and Plasma Induction Plates
    138
  - Nebulizer
    139
  - Peristaltic Pump and Drain
    139
- Periodic Checks
  140
  - Torch Assembly and Plasma Induction Plates
    140
  - Purge Viewing Window/Tubes
    140
  - Nebulizer
    140
  - Spray Chamber
    141
  - Peristaltic Pump
    141
  - Drains
    141
  - General System Maintenance
    141
  - Torch Viewing Position Alignment
    142
  - Performance Checks
    142
  - Cleaning the Sample Introduction System
    142
- Quick-Change Adjustable Torch Module
  144
  - Plasma Torch
    144
  - Plasma Induction Plates
    145
  - Removing the Scott Spray Chamber
    146
  - Removing the Injector
    146
  - Removing and Disassembling the Torch
    148
  - Cleaning the Torch
    151
  - Replacing the Torch
    152
  - Replacing the Torch on the Mount
    157
  - Replacing the Spray Chamber
    162
  - Connecting the Nebulizer (Neb) Tubing
    162
  - Replacing the Plasma Induction Plates
    164
- Windows
  166
  - Removing and Cleaning the Windows
    166
  - Removing the Windows
    166
  - Cleaning the Windows
    168
  - Replacing the Radial Window
    168
  - Replacing the Axial Window
    170
  - Replacing and Adjusting the Shear Gas Nozzle
    172
  - Adjusting the Position of the Shear Gas Nozzle
    173
- Scott-Type Spray Chamber
  174
- Cyclonic Spray Chamber
  176
  - Installing the Cyclonic Spray Chamber
    176
  - Etching the Cyclonic Spray Chamber
    181
- Nebulizers
  183
- Gemtip Cross-Flow Nebulizer
  185
- Gemcone Nebulizer
  199
- Concentric Glass Nebulizer
  204
  - Installing the Concentric Nebulizer
    204
  - Cleaning the Concentric Glass Nebulizer
    207
- Mira Mist Nebulizer
  209
  - Sample Capillary Tubing
    209
  - Gas Line
    210
  - Sample Introduction / Maximizing Stability
    210
  - Cleaning the Nebulizer
    210
- Peristaltic Pump
  211
  - Replacement Pump Tubing
    211
  - Installing the Sample and Drain Tubing
    212
  - Installing the Sample Tubing
    213
  - Connecting the Drain Tubing Assembly
    216
  - Installing the Drain Tubing
    219
  - Adjusting the Pump Tubing
    220
  - Cleaning the Pump
    221
  - Removing the Pump Head on the Peristaltic Pump
    222
  - Drain
    222
- General System Maintenance
  224
  - Cleaning the Instrument
    224
  - Air Filters
    224
  - Changing the RF Generator Air Filter
    224
  - Changing the Spectrometer Air Filter
    225
  - Changing the Neon Lamp
    226
  - Chiller and Filters
    226
  - Fuses
    227
- Replacement Parts: General
  228
  - Ordering Supplies, Accessories, and Replacement Parts
    239
Chapter 6: Troubleshooting

241
- Troubleshooting
  243
- Troubleshooting
  244
- Performance Problems
  245
  - Checking the Sample Introduction System
    245
- Plasma Ignition and Stability Problems
  252
  - Plasma Ignition Problems
    252
  - Plasma Stability Problems
    253
- Printing Problems
  254
  - Troubleshooting Form
    257
  - Instrument Environment
    258
  - Error Messages
    264
  - Error Messages
    265
  - Error Messages
    266

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