MicroCal VP-ITC User Manual page 85

11. Lower the upper Syringe Clamp so that it is flush to the top of the syringe holder.
12. Tighten the set-screw of the upper Syringe Clamp so that the disk is fixed to the syringe
glass.
13. Raise the syringe by carefully prying up on the upper Syringe Clamp until it is
approximately 3 mm higher than the top of the syringe holder.
14. Loosen the set-screw of the upper Syringe Clamp so that the clamp is free to slide up and
down on the outer diameter of the glass bore. Lower the Syringe Clamp all the way down
so that it is again flush to the top of the syringe holder.
15. Tighten the set-screw of the upper Syringe Clamp and your syringe height is now fixed at 3
mm from the bottom of the sample cell.
Reassemble the Pipette
Please refer to Section
pipette with the new syringe
1.6 Pipette Assembly (page 9), for instructions on how to reassemble the
Section 5: Instrument Maintenance
75