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User Manuals: MicroCal VP-ITC Titration Calorimeter
Manuals and User Guides for MicroCal VP-ITC Titration Calorimeter. We have
1
MicroCal VP-ITC Titration Calorimeter manual available for free PDF download: User Manual
MicroCal VP-ITC User Manual (93 pages)
MicroCalorimeter
Brand:
MicroCal
| Category:
Laboratory Equipment
| Size: 5 MB
Table of Contents
Table of Contents
1
General
3
How to Use this Manual
3
How to Get Help from Microcal
4
This Section Is Arranged as Follows
11
Section 1: VP-ITC System Introduction
11
VP ITC - the Basics
12
Data Acquisition and Instrument Control
13
Suitable Laboratory Environment
14
VP-ITC Parts and Accessories
15
Setting up the VP-ITC Instrument
17
Pipette Assembly
19
The Thermovac
21
This Section Is Arranged as Follows
24
Software.
24
Section 2: Vpviewer and Origin Software
24
Vpviewer and Origin Software Overview
25
Powering up the VP-ITC Instrument
25
Vpviewer Main Window
27
ITC Controls Window
31
Thermostat/Calibration Window
36
Setup/Maintenance Window
37
Constants Window
40
Real Time Data Display in Origin
41
ITC Cell Status
43
This Section Is Arranged as Follows
45
Section 3: Running an ITC Experiment
45
Designing ITC Experiments
46
Using the Thermovac to Degas Samples
50
Cell Loading
51
Loading the Auto-Pipette
52
Choosing the Run Parameters
55
Carrying out Experimental Runs
56
Using the Thermovac for Cleaning the ITC Sample Cell
57
Cleaning Syringes
59
Section 4: Experimental Tutorials
60
Water-Water Baselines
61
Methanol Tutorial
70
Rnase-2'CMP Experiment Tutorial
73
This Section Is Arranged as Follows
74
Section 5: Instrument Maintenance
74
Cleaning the Cells and Pipette
75
Replacing Pipette Plunger Tips
78
Y-Axis Calibration
82
Replacing Injection Syringes & Height Adjustment
84
This Section Is Arranged as Follows
86
Section 6: Tips and Troubleshooting
86
User Tips and Faqs
87
Troubleshooting
88
A Note about Buffers
89
Selecting the Proper Stirring Rate
89
Estimation of Required Concentrations
90
Section 7: Additional Features
91
Extended Data Display
92
Customizing Vpviewer
92
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