Shimadzu MOC63u Instruction Manual
  1. Manuals
  2. Brands
  3. Shimadzu Manuals
  4. Measuring Instruments
  5. MOC63u
  6. Instruction manual

Shimadzu MOC63u Instruction Manual

Moisture analyzer
Hide thumbs Also See for MOC63u:
Table of Contents

Advertisement

Quick Links

Presented By
Dallas
Ft Worth
Austin
Houston
NicolScales.com
800.225.8181
Contact Us
Nicol Scales & Measurement is an ISO Accredited Calibration
Company that has provided calibration, repair and sales of all types
of weighing and measurement products since 1931.

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the MOC63u and is the answer not in the manual?

Questions and answers

Related Manuals for Shimadzu MOC63u

Summary of Contents for Shimadzu MOC63u

  • Page 1 Presented By Dallas Ft Worth Austin Houston NicolScales.com 800.225.8181 Contact Us Nicol Scales & Measurement is an ISO Accredited Calibration Company that has provided calibration, repair and sales of all types of weighing and measurement products since 1931.
  • Page 2 After Measurement P.49 Turning Power Off P.50 Setting Measuring Conditions P.52 Changing Moisture Analyzer Settings P.63 Calibrating Moisture Analyzer P.73 When Connecting MOC63u to Peripheral Devices P.78 Using Windows Direct Function P.79 Control Moisture Analyzer from PC P.85 Printer Output (Option) P.91...
  • Page 3 • or missing information, should any be found, may not be corrected immediately. Shimadzu Corporation (the Company) owns the copyright to this instruction manual. Neither part nor the • entirety of this document may be transferred or reproduced without the prior written permission of the Company.
  • Page 4 Thank you for choosing the MOC63u, Shimadzu Moisture Analyzer. Shimadzu Corporation, with more than 90 years experience in manufacturing high precision balances, is confident in the high quality of the MOC63u moisture analyzer. The MOC63u provides prompt and accurate measurement of moisture contents. With...
  • Page 5 What You Can Do You can search the usage instructions for information about functions you want to try or learn about by aim. Various I want to measure moisture content! measuring Measuring Moisture Content page  I want to set measuring conditions in detail! methods Setting Measuring Conditions page 5 I want to measure data easily! Standard Drying Automatic Ending Mode page 5 I want to measure data by setting the time! Standard Drying Timed Ending Mode page 55 I want to measure samples that change largely with heat! Slow Drying Mode page 58 I want to measure liquid samples!
  • Page 6 Outputting I want to transfer the measured data to PC (Excel, etc.)! measurement Using Windows Direct Function page 79 results and I want to set the ID for each moisture analyzer unit to settings control several units! Setting the Moisture Analyzer ID page 7 I want to set sample codes for the moisture analyzer to control samples! Setting Sample Codes page 67 I want to set the date and time for the moisture analyzer to control the measurement date and time! Setting the Date and Time page 68 I want to print out measurement results! Printing Stored Measurement Data page 9 I want to print out the settings! Outputting the Moisture Analyzer Settings from a Printer page 9 Others I want to switch types of values to be referenced for measurement! Setting the Measurement Standard page 6 I want to restrict menu items to be displayed! Restricting the Menu Display page 69 I want to set the password! Setting the Password page 70 I want to clear measurement data from memory! Clearing Measurement Data from Memory page 105 I want restore the default settings of the moisture analyzer!
  • Page 7 Doing so may result in an electric If you believe the moisture analyzer may be shock or lead to abnormal operation. malfunctioning, contact an authorized Shimadzu representative. use the moisture analyzer with the specified power source and in the specified voltage environment.
  • Page 8 ! WaRNINg Do not attempt to measure samples Do not place anything on that may undergo dangerous chemical top of the heater cover. reactions when heated. Prohibitions Prohibitions Doing so may result in fire. Doing so may result in an explosion or release of toxic gas. Do not place flammable materials near the moisture analyzer.
  • Page 9 ! Caution Do not use the moisture analyzer in the following locations: Prohibitions Doing so may result in a malfunction. Where there is an air flow (near an air- • conditioner, air vent, door, window, etc.) Where temperatures change markedly •...
  • Page 10 "Safety Notes", (^ page 6) and follow the guidelines outlining correct operation procedures. Samples The samples measured with the MOC63u moisture analyzer are heated during the measurement. Measuring hazardous samples may lead to burn injuries or fire. ! CautION Do not measure the following hazardous samples.
  • Page 11 Handling the Moisture Analyzer During and Immediately after Measurement ! CautION Install the parts correctly Install the sample pan and pan supporter correctly. Instructions ^ "Installing Parts", page 35 Do not touch the sample pan and surrounding parts with bare hands during or immediately after measurement. The sample pan and surrounding parts become extremely hot immediately after measurement. Prohibitions Be sufficiently careful so as not to suffer a burn injury.
  • Page 12 Additional Notes ! CautION When the device will not be used for a long period of time, turn the power off and disconnect the power cable. Instructions ^ "Turning Power Off", page 50 after a power failure, turn the power switch on. If a power failure occurs, the power is automatically turned off.
  • Page 13 Warning labels on device WaRNINg Caution. Hot Do not touch the black grill or the observation window on the upper part of the heater cover. Doing so may result in a burn injury. Warning labels WaRNINg Caution. Hot Start your operation only after heated parts have completely cooled down. Doing so may result in a burn injury. Preventing measurement of flammable materials Do not measure flammable materials.
  • Page 14 WaRNINg Caution. High voltage Pull out the power cable from a receptacle when changing the heater. Otherwise, you may receive an electric shock. Warning labels * When the glass case is removed...
  • Page 15 How to Search for Desired Items There are various methods you can use to search for the function or operation you want to learn about in this instruction manual. You can search for the item on the cover page of the instruction manual. "Cover Page Index" You can search for the item based on what you want to do. "What You Can Do", page 4 You can quickly search the menu item for the function or procedure you "Menu Map", page 115 want to use.
  • Page 16 Sample page ( The following is a sample page to show the layout of this document. The content does not provide actual operations.) Linked to the cover page index (right pages only) Index Explanation of terms Describe terms used for MOC63u. Menu operation Reference Notes The following information will help you to use the device correctly. Continued on next page...
  • Page 17 after-Sales Service If this product does not operate normally, follow the guidelines in "Troubleshooting Guide" (^ P. 110) analyze and manage the problem. If the problem still persists, or a symptom occurs presumably caused by another failure, contact our service representative (details on back cover).
  • Page 18 MEMO...
  • Page 19 They will advise you regarding the equipment take-back. With your co-operation we are aiming to reduce contamination from waste electronic and electrical equipment and preserve natural resource through re-use and recycling. Do not hesitate to ask Shimadzu service representative, if you require further information. WEEE Mark...
  • Page 20 MEMO...

  • Page 21: Table Of Contents

    table of Contents table of Contents Introduction .......... What You Can Do .
  • Page 22 After Measurement ........9 Turning Power Off .
  • Page 23 Control Moisture Analyzer from PC ......85 Setup and Use of the Communication Tool ....... . .85 ■...
  • Page 24 MEMO...

  • Page 25: Before Measurement

    Be sure to check that the package contains all of the following parts and that all parts are undamaged. A number shown in [ ] indicates a quantity. If you find that any of the parts are missing, damaged, or deformed, contact an authorized Shimadzu sales representative. Sample pan [3] Pan supporter [1] Moisture Analyzer unit [1]...

  • Page 26: Names And Functions Of Parts

    Names and Functions of Parts The following explains the individual parts and components of the MOC63u moisture analyzer. Main Unit Front Observation window You can observe the condition of the sample (object) even when the heater is turned on Heater cover and the heater cover is closed. A heater is included in the heater cover. Close the heater cover before Set the pan supporter and measurement. sample pan on this, then place an object. Heater Used to dry samples (objects). Display panel Displays measurement...
  • Page 27 BEFORE MEaSuREMENt Names and Functions of Parts Rear Kensington security slot A mounting hole for anti-theft key. This Fuse holder slot complies with the If a fuse breaks, replace Kensington standard. it with a fuse in this fuse holder. Data I/O connector Used to connect a printer Power inlet (EP-80, EP-90, etc.) Connect the power cable to (^ page 91) supply power to the moisture analyzer. RS-232C connector (9-pin socket) uSB connector Used to connect the main Used to connect the main unit to a PC. unit to a PC via serial interface.

  • Page 28: Keyboard

    Keyboard The following explains the keys placed on the top of the moisture analyzer. Description Turns the power on or off. Calls the menu during the standby state (measurement display). Returns to the upper level of the menu tree. Shifts the digit to the left when the date and time, password, sample code, or ID is entered. Selects the menu item.

  • Page 29: Display Panel

    BEFORE MEaSuREMENt Names and Functions of Parts Display Panel Display Description Indicates the program No. (0 to 9) currently selected. For further information on how to select the program No., see steps 1 to 3 of "Selecting the Measurement Condition Program No." (^ page 52). When shown: Communicates with other equipment (printer, PC, etc.) via RS-232C, DATA I/O, or USB.
  • Page 30 Display Description The measurement is started. The temperature is rising. RAPID: Rapid drying mode ^ "Measuring Continues drying at the maximum Samples by Raising temperature after the temperature has Temperature Rapidly reached the maximum and it also reaches ∆ (RAPID: Rapid M (amount of change in moisture content drying mode)", per 30 seconds) set as the rapid drying...
  • Page 31 BEFORE MEaSuREMENt Names and Functions of Parts Display Description Indicates the time elapsed after the start of measurement. Indicates the temperature inside the heater cover during measurement. Indicates the measurement result display currently selected. For further information on changing the display, see "Setting the Measurement Standard"...
  • Page 32 Display Description Indicates the moisture analyzer status. Upper When shown: The heater cover is open. When flashing: You must close the heater cover currently open. When hidden: The heater cover is closed. Middle When shown: The heater cover is closed. When hidden: The heater cover is open.

  • Page 33: Installation

    Before Measurement Installation The following explains the process flow from installing the moisture analyzer to starting measurements. Determining Installation Location Measurement performance of the moisture analyzer depends largely on environments where the moisture analyzer is installed. To ensure safe and accurate measurements, follow the following precautions. ! CautION Do not use the moisture analyzer in the following locations: Where corrosive gas or inflammable...
  • Page 34 ! CautION Do not use the moisture analyzer in the following locations: The measurement result may be incorrect. Prohibitions Where there is an air flow (near an air- • conditioner, air vent, door, window, etc.) Where temperature changes extremely • Where vibration occurs •...
  • Page 35 Before MeasureMent Installation ! Caution Do not use the moisture analyzer in the following locations: Prohibitions Where dust, electromagnetic waves, or • magnetic fields are present Place the moisture analyzer on a rigid, stable, and flat table, or on the floor in the room. Instructions Placing the moisture analyzer on an unstable surface may cause personal injury or a malfunction.

  • Page 36: Installing Parts

    Installing Parts Take the following steps to install the moisture analyzer parts. Install the heater insulation plate. Sample pan Sample pan Install the heater insulation plate onto the case. Align the hole in the heater insulate plate with that in the pan supporter, and place the heater insulation plate on the case.

  • Page 37: Adjusting The Level Of The Moisture Analyzer

    BEFORE MEaSuREMENt Installation Adjusting the Level of the Moisture Analyzer This moisture analyzer unit maintains the level with three points on the bottom: One fixing point at the rear middle position, and two level screws on the front right and left positions. You can check the level gauge to determine the level. How to operate the level screws The height of the level screws can be changed by rotating it.
  • Page 38 Rotate the right and left adjusters until the air bubble in the level gauge appears at the lateral center. At this step, you can neglect the longitudinal position of the air bubble. Rotate the front right adjuster clockwise. When the air bubble is on the left Rotate the front left adjuster clockwise. When the air bubble is on the right Rotate the right and left adjusters at the same time until the air bubble in the level gauge appears at the longitudinal center.

  • Page 39: Preparing For Measurement

    Before Measurement Preparing for Measurement Turn on the power of the moisture analyzer before starting measurement. "Turning the Power On", page 38 When you use the moisture analyzer for the first time, we recommend the span calibration after installation. "The Span Calibration after Installing the Moisture Analyzer", page 40 Turning the Power On The following explains how to turn the power on.
  • Page 40 When the power switch is turned on, the version number (*1) is displayed and the internal system ! ! ! ! ! ! ! ! ! ! ! ! ! ! is checked automatically. Then, "oFF" appears on the display panel. (*1) The version number is subject to change ! V ! 1 .

  • Page 41: The Span Calibration After Installing The Moisture Analyzer

    BEFORE MEaSuREMENt Preparing for Measurements The Span Calibration after Installing the Moisture Analyzer After installing the moisture analyzer, we recommend you warm it up and perform span calibration to stabilize the moisture analyzer. The span calibration is possible between 10 and 60 grams, however, a 50-gram calibration weight is recommended. Turning the power on.
  • Page 42 Place a 50-gram calibration weight on the sample pan. ! ! 5 ! 0 . 0 ! 0 ! 0 ! ! ! 5 ! 0 . 0 ! 0 ! 0 ! When you use a weight other than 50 grams... If you use a weight other than the When the mass indication flashes, When the mass indication flashes, 50-gram one, reset the corresponding place the weight.

  • Page 43: Menu

    Before Measurement Menu Use the menu to configure measuring conditions for the MOC63u moisture analyzer, or to set the display and output of its measured values. How to Use the Menu The following describes how to use the menu. Press to call up the menu.

  • Page 44: How To Enter Data

    How to Enter Data Some menu items such as temperature, time, ∆M (Moisture change rate for 30 seconds), and password require input of values. Key operation Operation Temperature Password Upon date entry Input data Time Sample code Upon time entry ∆M In the password field: First and second The display value digits: Values 0 to 9,...

  • Page 45: Measure

    Measure Measuring Moisture Content You can call preset measuring conditions for measurement with the moisture analyzer. When you use the moisture analyzer for the first time, set measuring conditions. For further information on how to turn the power on, see "Turning the Power On"...
  • Page 46 Be sure that (the stability Check whether the stability mark is Check whether the stability mark is mark) is displayed, and adjust the displayed. displayed. zero point. ! ! ! 0 . 0 ! 0 ! 0 ! ! ! ! 0 . 0 ! 0 ! 0 ! [0. 0 00 ] Before adjusting the zero point, be sure that the pan supporter and an empty sample pan are placed.
  • Page 47 MEaSuRE Measuring Moisture Content Close the heater cover. The measurement starts automatically. If the measurement does not start automatically… Manual start is set for measurement. Press to start the measurement. Switching between automatic and manual start modes As the default setting, measurement start automatically after a sample is placed and the heater cover is closed. ! ! S ! T ! A ! R ! T ! ! S ! T ! A ! R ! T You can switch the mode to manual...

  • Page 48: To Obtain The Best Results

    Reset the measurement result. ! ! ! 4 . 9 ! 6 ! 4 ! ! ! 4 . 9 ! 6 ! 4 The water content indicator and measurement completed indicator relating to the measurement result disappear, and the mass after drying process appears.

  • Page 49: Aborting Measurement

    Measure aborting Measurement You can abort the measurement in process. Press during measurement. ! ! ! ! 0 . 9 ! 5 ! ! ! ! 0 . 9 ! 5 [AB RT] A long beep sound is heard, and "ABoRT" appears on the display.

  • Page 50: After Measurement

    after Measurement After the measurement of a sample is completed, dispose of the sample and cool off the heater to prepare for the next measurement. Open the heater cover. CautION The heater cover is hot during and immediately after measurement. Hold the handle when opening or Prohibitions closing the heater cover.

  • Page 51: Turning Power Off

    Measure turning Power Off The following explains how to turn off the power of the moisture analyzer. Press and hold until [oFF] ! ! ! 0 . 0 ! 0 ! 0 ! ! ! ! 0 . 0 ! 0 ! 0 ! appears on the display.
  • Page 52 MEMO...

  • Page 53: Detailed Measurement

    Detailed Measurement Setting Measuring Conditions There are four types of drying modes (standard drying, rapid drying, slow drying, and stepped drying) for measurement conditions. There are two types of ending modes (automatic ending and timed ending). Configure the temperature, time, or ∆M (amount of change in moisture content per 30 seconds) for all modes.

  • Page 54: Setting Temperature And The Amount Of Change In Moisture Content (∆M) As Measurement Conditions (Auto: Standard Drying Automatic Ending Mode)

    Select the program No. to save ! P ! R ! G ! - ! N ! ! ! P ! R ! G ! - ! N ! ! measuring conditions. [PRG- (n indicates the program No. currently selected.) ! ! ! ! N ! . 2 ! ! ! ! ! N ! .
  • Page 55 Detailed Measurement Setting Measuring Conditions Specify the temperature. ! ! ! ! 1 ! 2 ! 0 ! ! ! ! 1 ! 2 ! 0 (Temperature input.) Specify the temperature within the range from 50 °C to 200 °C in 1-degree increments. Specify ∆M. ! ! ! ! 0 .

  • Page 56: Setting Temperature And Time As Measuring Conditions (Time: Standard Drying Timed Ending Mode)

    Setting Temperature and Time as Measuring Conditions (TIME: Standard drying timed ending mode) Standard dry time ending mode dries a sample at the set temperature and, when the time set as the ending condition is reached, terminates the measurement automatically. Set the temperature and drying time. This mode is suitable for measurements to be completed within a limited time. Start the menu.

  • Page 57: Measuring Samples By Raising Temperature Rapidly (Rapid: Rapid Drying Mode)

    Detailed Measurement Setting Measuring Conditions Measuring Samples by Raising Temperature Rapidly (RAPID: Rapid drying mode) Rapid drying mode raises the temperature rapidly until the amount of change in moisture content per 30 seconds drops below the set value, then dries a sample at the set temperature. As the ending condition, you can select either the amount of change in moisture content per 30 seconds or the time.
  • Page 58 Specify the ending condition. [ M] [TIME] (∆M or time input.) As the ending condition, you can select either the amount of change in moisture content per 30 seconds or the time. If ∆M is selected, specify the value within the range from 0.01 % to 0.1 % in 0.01-percent ! ! ! ! ! ! M ! ! ! ! ! ! ! M ! increments.

  • Page 59: Measuring Samples By Raising Temperature Gradually (Slow: Slow Drying Mode)

    Detailed Measurement Setting Measuring Conditions Measuring Samples by Raising Temperature gradually (SLOW: Slow drying mode) Slow drying mode raises the temperature more gradually than measurements in normal conditions, taking about five minutes from the time the measurement begins until the temperature reaches the preset level. As the ending condition, you can select either the amount of change in moisture content per 30 seconds or the time.
  • Page 60 If ∆M is selected, specify the value within the range from 0.01 % to 0.1 % in 0.01-percent ! ! ! ! ! ! ! ! ! ! ! ! increments. ! ! ! ! 0 . 1 ! 0 ! ! ! ! ! 0 .

  • Page 61: Measuring Samples By Setting Temperature Step By Step (Step: Stepped Drying Mode)

    Detailed Measurement Setting Measuring Conditions Measuring Samples by Setting Temperature Step by Step (STEP: Stepped drying mode) In the Stepped Drying mode, you can set the drying temperature and time in one to three steps for measurement purposes. As the ending condition, you can select either the amount of change in moisture content per 30 seconds or the time. After measuring a sample by changing drying temperature in two or three steps, when the amount of change in moisture content per 30 seconds drops below the set value, or the time reaches the set value, the measurement terminates automatically.
  • Page 62 Specify the temperature of the second step. ! ! ! ! 2 ! 0 ! 0 ! ! ! ! ! 2 ! 0 ! 0 ! (Temperature input.) Specify the temperature within the range from 50 °C to 200 °C in 1-degree increments. Specify ∆M or the time of the second step.
  • Page 63 Detailed Measurement Setting Measuring Conditions Specify the ending condition. [ M] [TIME] (∆M or time input.) As the ending condition, you can select either the amount of change in moisture content per 30 seconds or the time. If ∆M is selected, specify the value within the range from 0.01 % to 0.1 % in 0.01-percent ! ! ! ! ! ! ! M ! ! ! ! ! ! ! ! M !

  • Page 64: Changing Moisture Analyzer Settings

    Changing Moisture analyzer Settings You can change the MOC63u moisture analyzer settings by setting a sample code or by setting a moisture analyzer ID. Setting the Measurement Standard You can select the values to be referenced for measurements. The following shows the denotation of symbols used for formulas calculating the measurement standard.
  • Page 65 Detailed Measurement Changing Moisture Analyzer Settings Either of the following is selectable for the minimum value to be displayed. For mass: 0.001 grams or 0.01 grams For others: 0.1 % or 0.01 % Start the menu. ! P ! R ! ! G ! R ! M ! P ! R ! ! G ! R ! M The menu opens.
  • Page 66 Select the minimum value to be displayed during measurement. (Unit selection) Press to display the step 1 screen. Press again to return to the standby state. Display selected in step 3 Selectable units ［M W］ ［D W］ [0.1] or [0.01] (in %) ［M D］ ［W D］ ［GRAM］ [0.001] or [0.01] (in grams) ! ! ! ! 0 .

  • Page 67: Setting The Method To Start Measurement

    Detailed Measurement Changing Moisture Analyzer Settings Setting the Method to Start Measurement Select the method to start measurement from the following two types. Easy: Place a sample and close the heater cover, and the measurement will start • automatically. You can quickly start the measurement without pressing Normal: Press to start the measurement manually.

  • Page 68: Setting Sample Codes

    Setting Sample Codes Set sample codes to identify the sample (object) from output measurement results. The sample code consists of four digits. The first and second digits allow "0 to 9", "- (hyphen)", "A to Z", or "_ (underscore)" to be entered, and the third and fourth digits only allow "0 to 9". Sample code "0000"...

  • Page 69: Setting The Date And Time

    Detailed Measurement Changing Moisture Analyzer Settings Setting the Date and Time Set the date and time to be output as a measurement result. Select from the following the format to output the date. Use two digits to enter the year. YYMMDD: Year, Month, Day • MMDDYY: Month, Day, Year •...

  • Page 70: Restricting The Menu Display

    Enter the hour and minute. (Hour and minute input.) Press to save the settings and move to the next item. Press to move to the next item. ! ! ! D ! A ! T ! E ! ! ! D ! A ! T ! E When the time does not need to be changed, press to return to the standby state...

  • Page 71: Setting The Password

    Detailed Measurement Changing Moisture Analyzer Settings Enter the password. ! P ! - ! 0 ! 0 ! 0 ! 0 ! P ! - ! 0 ! 0 ! 0 ! 0 (Password input.) (Repeat for four digits.) [ K] ! L ! ! C ! K ! E ! D ! L ! ! C ! K ! E ! D Press to shift the digit.
  • Page 72 Enter the password. ! P ! - ! 9 ! 9 ! 9 ! 9 ! P ! - ! 9 ! 9 ! 9 ! 9 (Password input.) (Repeat for four digits.) [ K] ! ! ! ! ! ! K ! ! ! ! ! ! K Press to shift the digit.

  • Page 73: Setting The Moisture Analyzer Id

    Changing Moisture Analyzer Settings Setting the Moisture Analyzer ID To use several MOC63u moisture analyzer units, set the moisture analyzer IDs, so that you can identify which unit is responsible for measured data when you check the data. The ID consists of four digits, and each digit allows "0 to 9", "- (hyphen)", "A to Z", or "_ (underscore)"...

  • Page 74: Calibrating Moisture Analyzer

    Installing the Moisture Analyzer" (^ page 40). Calibrating the Temperature (Option) To calibrate the temperature of the MOC63u moisture analyzer, the optional "Temperature Calibration Kit" is required. For further information on the temperature calibration kit, refer to the instruction manual attached to the kit.
  • Page 75 Detailed Measurement Calibrating Moisture Analyzer Open the heater cover of the moisture analyzer, take out the sample pan, and place holder of the temperature calibration kit assembled in step 1. Align the hole in the holder hole with that in the Windbreak. Close the heater cover, and check that the sensor probe fits the indentation in the heater cover. Start the menu. ! P ! R ! ! G ! R ! M ! P ! R ! ! G ! R ! M The menu opens.
  • Page 76 Select the temperature calibration ! ! ! ! C ! A ! L ! ! ! ! ! C ! A ! L ! from the menu. [CAL] [BAL] [TEMP] [100 ] ! ! ! T ! E ! M ! P ! ! ! T ! E ! M ! P To calibrate the temperature correctly ! ! ! ! 1 ! 0 ! 0 !
  • Page 77 Detailed Measurement Calibrating Moisture Analyzer When temperature indication ! ! ! ! 1 ! 0 ! 0 ! ! ! ! 1 ! 0 ! 0 (100 °C) flashes, enter the calibration temperature. (Temperature input.) Flashing indicates that the Flashing indicates that the temperature is stable. temperature is stable. After 15 minutes has elapsed, the temperature indication flashes. Enter the temperature (calibration temperature) ! ! ! ! ! ! 9 ! 5 ! ! ! ! ! ! 9 ! 5 indicated on the thermometer of the temperature...

  • Page 78: Output Of Calibration Record

    Output of calibration record Start the Menu. ! P ! R ! ! G ! R ! M ! P ! R ! ! G ! R ! M The menu opens. Select the temperature calibration record from the menu. ! ! ! ! C ! A ! L ! ! ! ! ! C ! A ! L ! [CAL] [BAL] [CAL.

  • Page 79: Connection To Peripherals

    CONNECtION tO PERIPHERaLS When Connecting MOC63u to Peripheral Devices When the MOC63u moisture analyzer is connected to a PC and a printer, the following functions are available: Display the moisture analyzer data in an application of the PC. ^ "Using Windows Direct Function", page 79 Control the moisture analyzer using command codes issued by the PC. ^ "Control Moisture Analyzer from PC", page 85 Output the measurement result and the settings of the moisture analyzer to a printer.

  • Page 80: Using Windows Direct Function

    However, the dedicate tools are required to use the Windows Direct Function on the Windows Vista or Windows 7 OS. For further information, refer to our Web site (http://www.shimadzu. com/products/balance/index.html). * The moisture analyzer may not operate normally in certain environments with Windows XP. In that case, optional tools may be required.
  • Page 81 ! ! ! ! W ! I ! N [WIN] Setting the Windows Direct Function on the Windows system The Windows Direct Function must also be set on the Windows system to allow data transmission between the Windows system and the moisture analyzer. For further information, refer to the following Web site: http://www.shimadzu.com/products/balance/index.html...

  • Page 82: Connecting The Windows System And The Moisture Analyzer

    Connecting the Windows System and the Moisture Analyzer The following two ways are available for connecting to the Windows system: "Connection via the RS-232C cable" (^ page 81) • "Connection via the USB cable" (^ page 82) • Connection via the RS-C cable Use the following procedure to connect the moisture analyzer to the Windows system (the PC) via the RS-232C interface cable.
  • Page 83 Connection to Peripherals Using Windows Direct Function Connection via the USB cable Use the following procedure to connect the moisture analyzer to the Windows system (the PC) using the USB cable. Turn the power off. ^ "Turning Power Off", page 50 Unplug the power cable from receptacle. Plug the USB cable into the USB connector at the rear of the moisture analyzer. Install the USB driver software on the PC by following the on-screen instructions. Connect the USB cable to the PC.

  • Page 84: Displaying The Measurement Result In The Windows System

    Displaying the Measurement Result in the Windows System Use the following procedure to display the measurement results in the Excel running on the Windows system. The results can also be displayed using the Notepad or other programs. Turn on the power switch of the moisture analyzer. ^ "Turning the Power On", page 38 Start the Excel on the Windows system.

  • Page 85: If The Windows Direct Function Does Not Work Well

    If the problem continues, contact an authorized Shimadzu representative. I have set the Windows Direct Function, but it does not work! Check the communication cable type (the Shimadzu’s genuine parts or a commercial cable) and check its connection status. If you are using a USB-to-serial port converter, the COM number may have been set to a number greater than 4.

  • Page 86: Control Moisture Analyzer From Pc

    To control the moisture analyzer from the PC, you need to setup and use the special communication tool. For further information on the communication tool, refer to the following Web site: http://www.shimadzu.com/products/balance/index.html Start the menu. ! P ! R ! ! G ! R ! M ! P ! R ! ! G ! R ! M The menu opens.
  • Page 87 Connection to Peripherals Control Moisture Analyzer from PC What are the WIN settings… Certain Windows settings are required to use the Windows Direct Function. For details, see "Enable the Windows Direct Function" ( page 79). Set the parity. ! ! P . N ! ! N ! E ! ! P . N ! ! N ! E (Select parity bit setting.) (Currently selected stop bit.) ! ! P .
  • Page 88 Set the handshaking. ! ! H ! S . H ! W ! ! H ! S . H ! W (Select a handshaking.) (Currently selected delimiter.) ! ! H ! S . S ! W ! ! H ! S . S ! W When you use the EP-80 or EP-90 printer, be sure to select the "HS.HW"...

  • Page 89: How To Use The Command Codes

    Connection to Peripherals Control Moisture Analyzer from PC How to Use the Command Codes You can use command codes to control the MOC63u moisture analyzer from the PC. The following explains how to use the commands. Command acceptance When the PC outputs a command, the "COM ERR" message may be displayed and the command may be rejected by the moisture analyzer according to its conditions.

  • Page 90: Command Code List

    Command Code List When controlling the MOC63u moisture analyzer from the PC, the following commands are available: Data output Command Function Single time output TEMP Temperature Single time output Key operations Command Function Command Function Command Function Press Press POWER Press Press Press Press...

  • Page 91: Cable Tie

    Connection to Peripherals Control Moisture Analyzer from PC Cable Tie IBM PC/AT, DOS/V, for AX series PC (D-sub9 pin) (straight cable ties) PC side MOC6u side...

  • Page 92: Printer Output (Option)

    (Option) Connect a printer to the MOC63u moisture analyzer to output the measurement and calibration results to the printer. Connecting a Dedicated Printer Any of the following printers can be connected to the DATA I/O port of the MOC63u moisture analyzer. EP-80 •...

  • Page 93: Setting The Printer Output Method

    Connection to Peripherals Printer Output (Option) Setting the Printer Output Method Use the following procedure to set up the measurement result output to the printer. Start the menu. ! P ! R ! ! G ! R ! M ! P ! R ! ! G ! R ! M The menu opens.

  • Page 94: Printing Stored Measurement Data

    You can select one of the following timings. Option Description Does not output data during measurement. 1SEC Outputs data every one second. 2SEC Outputs data every two seconds. 5SEC Outputs data every five seconds. 10SEC Outputs data every 10 seconds. 30SEC Outputs data every 30 seconds.

  • Page 95: Outputting The Moisture Analyzer Settings From A Printer

    ! ! ! 0 . 0 ! 0 ! 0 Press to return to the standby state. Outputting the Moisture Analyzer Settings from a Printer You can output the current settings of the MOC63u moisture analyzer to a printer. For further information on initializing the current settings, see "Initializing Moisture Analyzer Settings" (^ page 106).

  • Page 96: Output Data

    The following explains the calibration and measurement result output from the printer. When a printer and a PC are used as an output device, and the Windows Direct Function is set, the time measurement result is printed with a period instead of a colon. Measurement result output example Name of manufacture : Shimadzu Corporation Model : MOC6u Serial number...
  • Page 97 Connection to Peripherals Printer Output (Option) Span calibration output example Name of manufacture : Shimadzu Corporation Model : MOC6u Serial number : D00000000000 Device ID : 0000 (*1) Date : Oct. 19, 010 (*) Time : 1 7:0:06 (*) Weight used : 50.000 g (*) Balance weight reading before : 50.00 g calibration (Span calibration) Balance weight reading after : 50.000 g calibration (Span calibration) Span calibration completed Signature title *1 Variable value ^ "Setting the Moisture Analyzer ID", page 72 *2 Variable value ^ "Setting the Date and Time", page 68...
  • Page 98 Temperature calibration output example Name of manufacture : Shimadzu Corporation Model : MOC6u Serial number : D00000000000 Device ID : 0000 (*1) Date : Oct. 19, 010 (*) Time : 1 7:1:15 (*) Set temperature : 100 °C Temperature before calibration : 100 °C Temperature after calibration : 100 °C Set temperature : 180 °C Temperature before calibration : 181 °C Temperature after calibration : 180 °C Temperature calibration completed Signature title *1 Variable value ^ "Setting the Moisture Analyzer ID", page 72 *2 Variable value...

  • Page 99: Maintenance

    MaINtENaNCE Maintenance of Moisture analyzer CautION Unplug power cord from receptacle before servicing. If the power cord is being plugged into receptacle, you may be shocked during servicing. Instructions Start the service only after the heater and the heater cover have cooled down. If they are hot, you may burn yourself. Prohibitions Main unit Sample pan Wipe and clean the main body You can remove the sample pan with a soft cloth moistened with a from the moisture analyzer, and small amount of mild detergent. wash it in the water.

  • Page 100: Removing The Glass Case

    Removing the glass Case To clean the glass case, carefully remove it from the moisture analyzer. CautION Do not directly touch the heater or the sensor. Prohibitions Doing so may shorten the service life of the heater or result in malfunction. Open the heater cover. Loosen two setscrews shown by arrows. Use the SB2.5 (M3) hex wrench in the accessory kit.
  • Page 101 MaINtENaNCE Maintenance of Moisture Analyzer Maintenance of Moisture Analyzer Detach the glass case. Slide the glass case to remove it through the wider opening of the glass case hole. CautION Do not touch broken glass with your bare hands. Prohibitions If the glass case is broken, be sure to handle the broken glass carefully so that you do not get injured. glass case glass case Place the glass case on a flat surface and clean it...

  • Page 102: Installing The Glass Case

    Installing the glass Case After you have cleaned the glass case and replaced the heater, install them on the moisture analyzer. "Replacing Heater", page 102 Handle the heater leads carefully. Take care not to pinch the heater leads by the heater cover when installing the glass case. Open the heater cover.

  • Page 103: Replacing Heater

    MaINtENaNCE Replacing Heater When the heater has deteriorated or when the heating unit needs to be replaced due to the blow of lamp, replace the heater with a new one. Use the following heater replacement procedure. WaRNINg Pull out the power cable from a receptacle. Otherwise, you may receive an electric shock. Instructions WaRNINg Start the service only after the heater and the heater cover have cooled down.
  • Page 104 Remove the heater from the clips. Hold the prongs (indicated with circles in the figure at right) located on both sides of the heater, and detach them form the clips. Heater Heater Install a new heater. Clips Clips Heater 1 Install the heater using the clips. 2 Hold the 3 Plug in the cable with connector. cable supports. Install the heater using the clips. Hold the cable with cable supports.

  • Page 105: Replacing Fuses

    MaINtENaNCE Replacing Fuses CautION Before replacing fuses, turn the power switch of the moisture analyzer OFF, and remove the power plug from the socket. Instructions Otherwise you could sustain an electric shock. Do NOT use any fuse other than those specified. Doing so could cause a fire or short-circuit. Prohibitions When replacing fuses, be sure to use the fuse written in the "Accessories". Hook the fuse holder with a slotted screwdriver, and pull it toward you. Fuse holder Fuse holder Slotted screwdriver Slotted screwdriver...

  • Page 106: Clearing Measurement Data From Memory

    Clearing Measurement Data from Memory You can clear the measurement data from memory. Once cleared, it cannot be recovered. Start the menu. ! P ! R ! ! G ! R ! M ! P ! R ! ! G ! R ! M The menu opens.

  • Page 107: Initializing Moisture Analyzer Settings

    MaINtENaNCE Initializing Moisture analyzer Settings The moisture analyzer can be initialized to the factory defaults. All programs are initialized. Therefore, no specific program numbers can be initialized. Start the menu. ! P ! R ! ! G ! R ! M ! P ! R ! ! G ! R ! M The menu opens.

  • Page 108: Inspection

    Inspection Because the moisture analyzer may have an error due to its application and operating conditions, the customer needs to routinely and periodically check if the moisture analyzer maintains the required performance and functions normally. The customer should determine the actual inspection (including the inspection method and criteria) as the control criteria depend on the purpose of application and management of the moisture analyzer.

  • Page 109: Periodic Inspection

    The calibration certificate showing the JCSS logo for uncertainty can be issued (for the moisture analyzer only). We recommend that you consult our authorized service agency for actual inspection. For further information, refer to our Web site (http://www.shimadzu.com/products/balance/index.html). The following outlines the periodic inspection. Outline of periodic inspection (Example)
  • Page 110 MEMO...

  • Page 111: Troubleshooting Guide And Other Information

    OtHER INFORMatION troubleshooting guide If You Have a Problem. If the MOC63u moisture analyzer does not operate normally, check the following points: Phenomenon Possible cause actions taken The power cord is unplugged. Check the power supply and The switchboard is turned off.

  • Page 112: When These Messages Appear

    When These Messages Appear… When any of the following messages appears on the panel, take actions given. Message code Possible cause actions taken ABoRT Span calibration or Press to return to the standby Page 48 (Operation aborted) measurement was aborted. state. The error code appears and the CoM.ERR An unrecognizable command moisture analyzer enters the error...
  • Page 113 tROuBLESHOOtINg guIDE aND OtHER INFORMatION Troubleshooting guide Message code Possible cause actions taken Unplug the power cord, and then plug it in again. If the same ERR.0 The source voltage is abnormal. Page 38 message appears again, call a service representative. A large error in the zero point or the sensitivity of the pan.

  • Page 114: When Required

    When Required Specifications (main unit) Measurement format Evaporation weight loss method (Heat drying and weight loss method) Sample weight 0.02-60 g Weight 0.001 g Minimum display Moisture content 0.01 % External weight range for 10-60g span calibration Measurable quantities Moisture content (Wet Base and Dry Base), weight, solid content Sample weight: 2 g 0.15 % Repeatability...

  • Page 115: Accessories

    TRoubleshooTing guide and oTheR infoRmaTion When Required Accessories The part numbers and specifications given are subject to change without notice. Standard Accessories and Consumables List item Part number description Pan supporter 321-71598 Heater insulation plate 321-71736-01 Windbreak 321-71720 Power cable 240V (*1) 071-60825-51 2.4 meters long (RoHS), 250 V/10 A Fuse 240V...

  • Page 116: Menu Map

    Menu Map The Menu Map illustrates the menu system in an easy to understand form. You can access the desired menu item quickly. For further information on menu display and operations, see "Menu" (^ page 42). How to use the menu map Notation of Explanation of operation menu map Select a menu item by pressing Press...
  • Page 117 tROuBLESHOOtINg guIDE aND OtHER INFORMatION When Required Menu map Press in the standby state. Defaults Items displayed during menu restriction ø PR GRM PRG-N o ø ø Program No. Selection ^ P.52 – 9 ^ P.53 TIME ^ P.55 RAPID ^ P.56 SL W ^ P.58 STEP...
  • Page 118 HS. H W Handshaking HS. S W ^ P.87 HS. T IM HS. FF Delimiter ^ P.87 CR+LF C DE 0000 Sample code entry ^ P.67 0000 – ZZ99 DATE YYMMDD Date and time setup ^ P.68 L CK L CKED UNL CK ø...

  • Page 119: Index

    Index Index Symbol ERR ......111 Error ......110, 111 g O/T f .
  • Page 120 Measurement standard ... . .63, 95 Measurement time ....30 RAPID:Rapid drying mode ..29, 56 Measuring conditions .
  • Page 121 UNIT ..... . . 30, 64, 95 USB connector ....26, 82 Warming up .

Table of Contents

Save PDF