Related Manuals for Shimadzu TOC-V CPH
Summary of Contents for Shimadzu TOC-V CPH
- Page 1 SHIMADZU TOC-V Series TOTAL ORGANIC CARBON ANALYSER Short-User Manual TOC-V CPH/CPN TOC-Control V Version 2.00...
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Page 2: Table Of Contents
Table of Content TOC-Control V Main Menu 1. Measurement 1.1 Sample Table Editor 1.2 H/W Settings 1.3 Online Manual Administration 2.1 System Administrator 2.2 Audit Trail 2.3 User Authentication 2.4 Others Sample Table Editor 1. Create a calibration curve 2. Create a method 3. -
Page 3: Toc-Control V Main Menu
Main Menu Parameter Action/Description STARTPROGRAMSTOC-Control V TOC-Control V or Start TOC-Control V Main Menu double-click on the TOC-Control V icon (Desktop) Measurement Sample Table Editor - to create and edit methods, calibration curves and sample measurement sequences. Parameter Action / Description Click on the “Sample Table Editor”... - Page 4 User Name of current user is automatically entered, if entered it cannot be edited Date of Creation Current date is automatically entered and cannot be edited Comment Enter additional system information (optional) Instrument Setup Wizard-2 : Instrument Options Parameter Action / Description Select “Combustion”...
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Page 5: Online Manual
Instrument Setup Wizard-5 : SSM parameters Parameter Action / Description SSM TC Furnace ON Select this option to heat the TC furnace of SSM SSM IC Furnace ON Select this option to heat the IC furnace of SSM Instrument Setup Wizard-6 : Communication parameters Parameter Action / Description Com Port... -
Page 6: System Administrator
System Administration 2.1.1 System Policy - to check the security functions, activation of them is done during the installation 2.1.2 S/W Validation to verify that the TOC-Control V program files have not been modified since installation Audit Trail 2.2.1 Log Browser - to open the audit trail database (please refer to the Administration Manual) 2.2.2 Add a Log Event to add an event to the Log Browser... -
Page 7: Others
Password Enter the password for the new account. The limits for password (required item) length and complexity can be changed. Please refer to the Administration Menu Confirm Password Enter the password again. (required item) Company, Department, Enter additional information of user if required Position, Tel, email User Level Select a radio button to establish the user level... -
Page 8: Sample Table Editor
Sample Table Editor Start the TOC-Control V from the Windows Start menu, and click the Sample Table Editor or click the short cut “Sample Table Editor” on the desktop. Sample table Editor with open Sample Table and Sample Window Explanation of the Windows design: 1: Menu bar 2: Tool bar for the file 3: Tool bar for the instrument... -
Page 9: Create A Calibration Curve
1. Create a Calibration Curve File A Calibration Curve File is used to generate a calibration curve. This file includes standard solution concentration and measurement parameters Click “New” in the Calibration Curve tab of the file viewer or Select “File” – “New” – “Calibration Curve” Calibration Curve Wizard –1 System Information Parameter Action/Description... - Page 10 Calculation Method Select the calculation method to be used for the calibration curve. Point to point The point to point curve fit draws a straight line between adjacent data points and considers each line segment to be a separate calibration line governed by its own equation. Linear regression A linear regression statistically determines the line that best fits the pattern of all data points.
- Page 11 Calibration Curve Wizard –6 Additional Settings Parameter Action/Description Use default settings Select this option to use the default values for peak detection. Min. integration time Enter the minimum time the instrument signal will continue to be detected Max. integration Enter the maximum time the instrument signal will be detected when no peak is found Correlation Coeff.
- Page 12 Overview about several possibilities to create a Calibration Curve: Wizard -2 Calibration points are Edit calibration curve Calibration curve Calibration curve according to Calibration curve distributed uniformly over point manually according to USP/EP type concentration range DIN 38402/P-51 Normal calibration curve, data Normal calibration Special calibration curve: Special calibration curve:...
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Page 13: Create A Method
2. Creating a Method A Method is a file used to set the analysis parameters used for measuring unknown samples. Click “New” in the Method tab of the file viewer or Select “File” – “New” – “Method” Method Wizard –1 System Information Parameter Action/Description System... - Page 14 Expected Conc. Range Enter the maximum expected concentration. A range value is automatically entered based on the selected calibration curve No. of Injections Enter the minimum/maximum number of injections for the samples SD Max Enter the maximum standard deviation and coefficient of variance CV Max that is acceptable for the injections.
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Page 15: Create A Sample Run
3. Create a Sample Run Click “New” in the Sample Table tab of the file viewer or Select “File” – “New” – “Sample Table” Parameter Action/Description System Select the instrument Comment Enter a comment (512 characters minimum) 3.1 Editing the Sample Table Insert the sample measurement parameters into the Sample Table a) Insert the calibration curve (Standard solutions) into the Sample Table Drag the calibration curve file from the Calibration Curve tab of the file viewer or... - Page 16 Right-click in the left cell in the row where multiple samples are to be inserted. Select “Insert” – “Multiple Samples” Sample Group Wizard –1 Sample Source - enter the parameter source for the sample Parameter Action/Description Method to create the sample group using measurement parameters of an existing method file Enter the desired method or select the method using the Browse button...
- Page 17 Sample Group Wizard –4 Calibration Curve Check Select the control samples to be inserted with the calibration curves Parameter Action/Description Control Sample selection Select the control sample to be attached to the calibration curve. These parameters can be entered for each calibration curve selected in Sample Wizard 4.
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Page 18: Schedule File
4. Schedule File 4.1 Creating a new Schedule A schedule is a stored file which contains measurement parameters for multiple samples, including the specific sequence of analyses. The saved content of the file can be called up as desired, and loaded into a sample table. Editing of a schedule file in the format of a sample table is conducted using the same operations as in a sample table. -
Page 19: Vial Number
5. Vial number After inserting the samples in the sample table, the vial number of vials to be sampled I the ASI-V must be associated with the samples Open a complete sample table and click the Vial setting button Parameter Action/Description Table The sample table displays the row, sample name and attribute of the... -
Page 20: Analysis
III. Analysis Connecting to the Instrument Open the Sample Table to be used and click the [Connect] button of the Tool bar Click “Use Settings on PC” Start of analysis (standby - function) - Click [Start] button of the Tool bar - Define the Standby option Parameters Action/Description... -
Page 21: Sample Window
Sample Window - During Measurement Click the [Sample Window] button on the Tool bar Parameters Action/Description Graph Current Peak Displays the peak profile of the highlighted injection. All Peaks Displays all injection peaks for the selected sample Calibration Curve Displays calibration curve (for calibration standards only) This function is not available during real-time analysis. -
Page 22: Edit Mode
Editing the Sample Table during analysis The sample table can be edited during analysis by changing to the Edit Mode. This mode allows the following operations to be conducted in the sample table in the same way as when analysis is not being conducted During analysis, select “Instrument”...
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