Agilent Technologies G1321A FLD Manuals

Manuals and User Guides for Agilent Technologies G1321A FLD. We have 1 Agilent Technologies G1321A FLD manual available for free PDF download: Reference Manual

Agilent Technologies G1321A FLD Reference Manual

Agilent Technologies G1321A FLD Reference Manual (334 pages)

Fluorescence Detector

Brand: Agilent Technologies | Category: Security Sensors | Size: 4.85 MB

Table of Contents

Table of Contents
5
1 Installing the Fluorescence Detector

14
- Site Requirements
  14
- Physical Specifications
  17
- Unpacking the Detector
  18
- Flow Connections to the Detector
  26
2 First Steps with the Fluorescence Detector

31
- Before You Start
  32
- Optimization Overview
  33
- Getting Started and Checkout
  34
3 Optimizing the Fluorescence Detector

61
- Optimization Overview
  62
- Design Features Help Optimization
  63
- Check Performance before You Start
  63
  - Finding the Best Wavelengths
    63
    
    A Real Example
    64
    
    Finding the Best Signal Amplification
    65
    
    Changing the Xenon Flash Lamp Frequency
    67
    
    Lamp Life Savings
    67
    
    Selecting the Best Response Time
    69
    
    Reducing Stray Light
    70
  - Status Indicators
    73
  - Status Indicators
    74
    
    Detector Status Indicator
    75
    
    Power Supply Indicator
    75
    
    Error Messages
    76
    
    Time-Out
    77
    
    Remote Time-Out
    78
    
    Shutdown
    78
    
    Leak
    79
    
    Synchronization Lost
    79
    
    Leak Sensor Open
    81
    
    Leak Sensor Short
    82
    
    Compensation Sensor Open
    83
    
    Compensation Sensor
    84
    
    Fan Failed
    85
    
    Motor Errors
    86
    
    Lamp Cover Open
    88
    
    FLF Board Not Found
    89
    
    ADC Not Calibrated
    90
    
    A/D Overflow
    91
4 Troubleshooting and Test Functions

73
- Flash Lamp Current Overflow
  91
  - Flash Trigger Lost
    93
- Wavelength Calibration Failed
  94
- Wavelength Calibration Lost
  94
  - Flow Cell Removed 103 no
    95
  - Peaks
    96
  - Wavelength Verification and Calibration
    96
- Check of Raman Band of Water
  99
  - The Wavelength Calibration Procedure
    105
    
    Preparation of the Flow Cell
    105
    
    Preparation of the Glycogen Calibration Sample
    105
    
    Wavelength Calibration
    106
    
    Verification
    107
  - Test Functions
    107
    
    Lamp Intensity Test
    108
    
    Lamp Intensity History
    109
    
    Dark-Current Test
    110
    
    Excitation and Emission Grating Resistance History
    111
  - Raman ASTM Signal-To-Noise Test
    112
    
    Using the Built-In Test Chromatogram
    114
    
    Using the Built-In DAC Test
    116
5 Repairing the Fluorescence Detector

119
- Introduction into Repairing the Fluorescence Detector
  120
- Overview of the Repairing of the Fluorescence Detector
  123
- Simple Repairs
  124
  - Exchanging a Flow Cell
    124
  - How to Use the Cuvette
    127
    
    Correcting Leaks
    128
    
    Flow Cell Flushing
    128
    
    Replacing Leak Handling System Parts
    129
    
    Exchanging Internal Parts
    130
    
    Removing the Covers
    132
- Removing the Rear Foam
  133
  - Exchanging the Lamp
    135
    
    Exchanging the EX-Condenser
    142
    
    Replacing the Lamp Cover Window
    147
    
    Exchanging the Processor Board
    151
    
    Exchanging the Fan
    154
    
    Exchanging the Leak Sensor or Leak Panel
    157
    
    Replacing the EM-Condenser or Cutoff-Filter
    160
    
    Replacing the Mirror Assembly
    164
  - Replacing the Slits
    170
- Removing the Optical Unit
  172
- Exchanging the Power Supply
  191
- Replacing Status Light Pipe
  194
- Installing the Optical Unit
  195
  - Replacing the Foams and Covers
    198
- Assembling the Main Cover
  201
- Replacing the Interface Board
  203
  - Repla I G the Dete Tor's Fir Are
    203
6 Identifying Parts and Materials

205
- Overview of Main Assemblies
  205
- Overview of Main Assemblies
  206
  - Optical Unit Assembly
    208
  - Lamp Cover Parts
    210
  - Control Module
    211
  - Sheet Metal Kit
    212
  - Plastic Parts
    213
  - Foam Parts
    214
  - Power and Status Light Pipes
    215
- Leak Parts
  216
- Cuvette Kit
  217
- Spare Parts
  218
  - Accessory Kit
    218
  - Cable Overview
    220
    
    Analog Cables
    222
    
    Remote Cables
    225
    
    BCD Cables
    231
    
    Auxiliary Cable
    232
    
    CAN Cable
    233
    
    External Contact Cable
    234
  - RS-232 Cable Kit
    235
- LAN Cables
  235
7 Introduction to the Fluorescence Detector

237
- Introduction to the Detector
  238
- How the Detector Operates
  239
  - Raman Effect
    241
  - Optical Unit
    242
    
    Reference System
    247
  - Analytical Information from Primary Data
    248
    
    Fluorescence Detection
    248
    
    Of Raw Data
    249
    
    Electrical Connections
    251
  - Instrument Layout
    253
  - Early Maintenance Feedback (EMF)
    254
    
    EMF Counters
    254
    
    Using the EMF Counters
    255
8 Theory of Operation

257
- Electronics
  258
- Detector Main Board (FLM)
  259
- Detector Frontend Board (FLF)
  262
  - FLF Board Revisions
    265
    
    How to Retrieve the FLF Board Revision
    266
  - Detector Lamp Supply Board (FLL)
    267
  - Firmware Description
    268
    
    Firmware Updates
    268
  - Raw Data Conversion to Fluorescence (LU) Units
    269
    
    Data Flow for Chromatographic Output
    271
    
    Data Flow for Spectral Output
    272
    
    Spectra Acquisition Modes
    274
- Optional Interface Boards
  274
  - BCD Board
    275
  - LAN Communication Interface Board
    276
  - Interfaces
    277
  - Analog Signal Output
    278
    
    GPIB Interface
    278
    
    CAN Interface
    279
    
    Remote Interface
    279
- Setting the 8-Bit Configuration Switch
  282
  - GPIB Default Addresses
    283
  - Communication Settings for RS-232C Communication
    284
    
    Resident Settings
    286
- The Main Power Supply Assembly
  286
9 Introduction to the Control Module

289
10 Specifications

313
- Performance Specifications
  314
- General Safety Information
  319
  - Safety Information
    319
- Lithium Batteries Information
  321
  - Radio Interference
    323
  - Sound Emission
    324
  - UV-Radiation (UV-Lamps Only)
    325
  - Solvent Information
    325
- A Safety Information
  328

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