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Endress+Hauser analytik jena PlasmaQuant 9200 Operating Manual
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Endress+Hauser analytik jena PlasmaQuant 9200 Operating Manual

Endress+Hauser analytik jena PlasmaQuant 9200 Operating Manual

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Operating Manual
PlasmaQuant 9200

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Summary of Contents for Endress+Hauser analytik jena PlasmaQuant 9200

  • Page 1 Operating Manual PlasmaQuant 9200...
  • Page 2 Manufacturer Analytik Jena GmbH+Co. KG Konrad-Zuse-Straße 1 07745 Jena / Germany Phone: +49 3641 77 70 Fax: +49 3641 77 9279 Email: info@analytik-jena.com Technical Service Analytik Jena GmbH+Co. KG Konrad-Zuse-Straße 1 07745 Jena / Germany Phone: +49 3641 77 7407 Fax: +49 3641 77 9279 Email: service@analytik-jena.com For a proper and safe use of this product follow the instructions.
  • Page 3 PlasmaQuant 9200 Table of contents Table of contents 1 Basic information ..............................About this manual ............................Intended use ..............................2 Safety ..................................Safety labeling on the device ........................... Requirements for the operating personnel..................... Safety instructions for transport and commissioning..................Safety instructions for operation ........................Safety instructions for the operation of compressed gas containers and compressed gas systems....
  • Page 4 Table of contents PlasmaQuant 9200 Device faults and analytical problems ......................55 7 Maintenance and care of the emission spectrometer ..................58 Maintenance overview ............................. 59 Cleaning the dismantleable torch........................60 Replacing the glass body..........................63 Maintenance of the one-piece torch ....................... 65 Cleaning the nebulizer............................
  • Page 5 PlasmaQuant 9200 Basic information Basic information About this manual This user manual describes the following device models: PlasmaQuant 9200 ¡ ¡ PlasmaQuant 9200 Elite The models are combined in the following text. Any differences between the models are explained in the relevant section. The device is intended to be operated by qualified specialist personnel who must ob- serve all instructions given in the operating manual.
  • Page 6 Basic information PlasmaQuant 9200 Intended use The optical emission spectrometer with inductively coupled plasma (ICP-OES) is used in a chemical analysis laboratory for the analysis of liquid, mainly aqueous samples, to de- termine concentrations of up to 75 elements up to the trace range. The device may only be used for the processes described in the user manual.
  • Page 7 PlasmaQuant 9200 Safety Safety For your own safety and to ensure error-free and safe operation of the device, please read this chapter carefully before commissioning. Observe all safety instructions listed in this manual, as well as all messages and instruc- tions displayed by the control- and analysis software on the monitor.
  • Page 8 Safety PlasmaQuant 9200 The responsible body at the installation site is accountable for compliance with safety and occupational health regulations. The responsible body must meet the following re- quirements: ¡ Provide information about national regulations on work safety and accident preven- tion and observe them during operation of the device.
  • Page 9 PlasmaQuant 9200 Safety Safety instructions for operation Safety circuits The plasma compartment is shielded by the housing and the UV and EMC protective glass, as well as the metal grille on the plasma compartment door in such a way that high-frequency radiation and UV radiation are reduced to a safe level.
  • Page 10 Safety PlasmaQuant 9200 The device is designed so that the plasma compartment protrudes beyond the sampling compartment with the sample feed system. When working on the sample feed system, there is a risk of bumping your head on the plasma compartment or the open plasma compartment door.
  • Page 11 PlasmaQuant 9200 Safety The device meets the requirements for interference emission in accordance with EN ¡ 55011 Group 1, Class A. Electrical and electronic assemblies are shielded from interference emission by metal components. Strong interference from other devices may disrupt the image of the plasma camera. A visual inspection of the plasma on the device is therefore recommended.
  • Page 12 Safety PlasmaQuant 9200 Shut off the gas supply to the device before performing maintenance. Only leave the ¡ gas supply open if expressly required by the operating instructions. ¡ Use only original spare parts, wear parts and consumables. These have been tested and ensure safe operation.
  • Page 13 PlasmaQuant 9200 Function and design Function and design Design The device is used to determine the elemental content in liquid, usually aqueous sam- ples. A special sample feed system is used to extend the measuring range to organic so- lutions. The device essentially consists of the following components: ¡...
  • Page 14 Function and design PlasmaQuant 9200 The sample tray is held in place by two pins and can be removed if necessary. Fig. 2 Device with removable sample tray Easy maintenance The device has a modular design. Maintenance and wear parts are easily accessible. For example, you can replace the water filter on the rear of the device yourself and/or flush it regularly in accordance with the maintenance instructions.
  • Page 15 PlasmaQuant 9200 Function and design 3.1.1 Plasma compartment The plasma compartment is shielded by the housing and the UV protective glass, as well as the metal grille on the plasma compartment door in such a way that high-frequency radiation is reduced to a safe level. At the same time, the plasma compartment can still be accessed for maintenance pur- poses via the plasma compartment door.
  • Page 16 Function and design PlasmaQuant 9200 Plasma gas Auxiliary gas Sample aerosol in the nebulizer gas Fig. 5 Schematic diagram of the torch with gas flows 1 Induction coil 2 Outer tube 3 Inner tube 4 Injector Mount the plasma torch or torch with the holder (shuttle) on the guide rail of the me- chanical height adjustment.
  • Page 17 PlasmaQuant 9200 Function and design The outer tube is exposed to high thermal loads. With the demountable torch, you can replace the parts individually. However, during assembly, you must ensure that the indi- vidual parts are gas-tight and check that the injector is seated correctly. You clean the one-piece torch as a whole.
  • Page 18 Function and design PlasmaQuant 9200 Fig. 8 Spray chamber and nebulizer 1 Spray chamber 2 Waste hose connection 3 Fork clamp 4 Plastic nut 5 Nebulizer 6 Sample tube connection 7 Gas connection (argon) The waste bottle for collecting the sample solutions is included. The plastic bottle (poly- ethylene, 2 liters) has a screw cap with holes for the hoses.
  • Page 19 PlasmaQuant 9200 Function and design Fig. 9 Rear of the device 1 Interfaces 2 Power switch, power connection 3 Exhaust connection 4 Ventilation grille 5 Inspection hatch (customer service only) 6 Gas connections (bottom: argon, top: oxygen) 7 Water filter 8 Cooling water connection Fig. 10 Interfaces 1 COM 2: Autosampler...
  • Page 20 Function and design PlasmaQuant 9200 Fig. 11 Gas connections 1 Connection for oxygen (additive gas) 2 Argon connection The device draws in ambient air for air cooling from below at the rear of the device. En- sure that the air can flow freely. Gases Argon is used as a gas for the torch and nebulizer and for purging the spectrometer.
  • Page 21 PlasmaQuant 9200 Function and design Fig. 12 Switching the device on and off 1 Standby switch 2 Manual plasma deactivation switch 3 Power switch, power connection Type plate The type plate is located on the rear of the device. A label with the device serial number is also affixed to the inside of the plasma compartment door.
  • Page 22 Function and design PlasmaQuant 9200 The Teledyne Cetac ASX-560 autosampler and the smaller Cetac ASX-280 are suitable for aqueous solutions and have an integrated purge station. They can be equipped with various sample racks. The Cetac XLR-860 autosampler can hold up to 720 samples. The Cetac Oils 7400 autosampler enables the automatic feed of oils and coolants.
  • Page 23 PlasmaQuant 9200 Installation and commissioning Installation and commissioning Installation conditions 4.1.1 Installation location requirements The emission spectrometer may only be operated in closed rooms. The location must have the quality of a chemical laboratory (indoor use). ¡ Avoid direct sunlight and radiation from heaters onto the device. If necessary, pro- vide air conditioning.
  • Page 24 Installation and commissioning PlasmaQuant 9200 Operating voltage 200 to 240 V AC ±10 % Frequency 50/60 Hz Power connection Device connection: ¡ C19 input socket Mains connection cable: CEE 7/7 (EU) ¡ NEMA 6-20 (due to 240 V, NEMA L6-20 plug) ¡ (USA, Canada) Connection cable with open ends, e.g. Japan ¡...
  • Page 25 PlasmaQuant 9200 Installation and commissioning Extraction output 3.5 m³/min (min.), 5.5 m³/min (max.) Optimal: 4.0 to 4.5 m³/min Adapter using flexible aluminum pipe Pipe diameter: 125 mm Pipe length: 1000 mm 4.1.5 Recirculating chiller The HF generator is cooled by the cooling circuit of the external recirculating chiller. Please observe the information provided in the recirculating chiller' s operating instruc- tions.
  • Page 26 Installation and commissioning PlasmaQuant 9200 4.1.6 Device layout and space requirements The emission spectrometer is a compact device designed for table-top operation. The re- quired space depends on all components that make up the measuring station. Components of the measuring station: Autosampler ¡...
  • Page 27 PlasmaQuant 9200 Installation and commissioning 932 mm 600 mm Fig. 13 Space requirements (viewed from the front) 125 mm 280 mm 809 mm 530 mm Fig. 14 Space requirements (view from above)
  • Page 28 Installation and commissioning PlasmaQuant 9200 Installing the sample supply system The sample feed systems, the torch and the nebulizer with spray chamber, as well as the autosampler, must be installed by the customer during maintenance work. CAUTION Risk of injury A risk of injury due to broken glass is present when handling glass parts.
  • Page 29 PlasmaQuant 9200 Installation and commissioning } Push the torch upwards on the rail until it engages over the holder with the spring pin (1) on the height adjustment. The height adjustment is factory set so that the zero point on the scale corresponds to the optimum setting for standard applications.
  • Page 30 Installation and commissioning PlasmaQuant 9200 Pump hose Inside diameter Designation (stopper) Sample supply 0.762 mm/0.03 inch black/black Waste 1.143 mm/0.045 inch red/red Adjust the contact pressure on the pump hose as follows: } Loosen the screw on the lever so that no liquid is conveyed. } Slowly tighten the screw until liquid begins to flow through the hose.
  • Page 31 PlasmaQuant 9200 Installation and commissioning Fig. 16 Connection panel on the right side of the sampler 1 DIP switch 2 "HOST" connection (to the basic device) 3 Power switch 4 Fuse holder 5 Power connection Note: DIP switch 5 is set to "ON". Only the aforementioned connections are required for the use of the sampler together with the basic device.
  • Page 32 Installation and commissioning PlasmaQuant 9200 Installing the sampler NOTICE Risk of damage to the sensitive electronics ¡ Only connect the sampler to the electrical grid after installation. } Place the tray on the automatic sampler foot, and place the base plate for holding the sample racks on that.
  • Page 33 PlasmaQuant 9200 Installation and commissioning } Connect the pump hose for the purging solution to the lower intake con- nection (1a) of the purging vessel. Place the pump hose over the hose block from above and clamp it between two stoppers. Connect the intake hose for purging solution to the other end of the hose (1b).
  • Page 34 Installation and commissioning PlasmaQuant 9200 Installing other accessories 4.4.1 Coupling the Teledyne Cetac ASX-560 autosampler to the Cetac ASXPress Plus switching valve When delivered together with the emission spectrometer, the accessories are commis- sioned with the base device. The user only needs to carry out the installation themselves if they order the accessories separately and the accessories are delivered later.
  • Page 35 PlasmaQuant 9200 Installation and commissioning } Connect the control unit and autosampler to the electrical mains. Teledyne Cetac ASX-560 Power con- nection Communication ca- bles Valve assembly Power connection Cetac ASXPress Plus Control unit Fig. 19 Diagram: Connections between PC and accessories } Connect the switching valve to the autosampler and emission spectrometer using the following hoses: –...
  • Page 36 Installation and commissioning PlasmaQuant 9200 When the autosampler and switching valve are connected (without dilution system), the Dashboard software controls the switching valve. Control of the switching valve is not integrated in the ASpect PQ software. For operation of the autosampler and switching valve without dilution system: } Install the Dashboard software;...
  • Page 37 PlasmaQuant 9200 Installation and commissioning Connecting autosampler and } Connect the autosampler and dilution system via the following interfaces and con- dilution system nect to the electrical network: Fig. 22 Connect autosampler and dilution system Connections on the rear of the autosampler: 1 Power supply for autosampler 2 USB interface to PC (via hub) (via dilution system)
  • Page 38 Installation and commissioning PlasmaQuant 9200 Fig. 24 Hose connections on the dilution system 1 Connection to the storage bottle with di- 2 Syringe pump lution solution 3 Connection to the waste bottle 4 Connection to storage bottle with rins- ing liquid (for vortex mixer vessel) 5 Connection to vortex mixer vessel 6 Connection to autosampler needle (placed on the autosampler)
  • Page 39 PlasmaQuant 9200 Installation and commissioning Time Measure Software command Installation of the dilu- Insert the syringe into the Move syringe to removal ¡ tion system syringe pump of the dilution position When changing the sy- system. ¡ ringe To do this, move the syringe piston to the ½...
  • Page 40 Installation and commissioning PlasmaQuant 9200 Fig. 26 Connect autosampler and dilution system Connections on the rear of the autosampler: 1 Power supply for autosampler 2 USB interface to PC (via hub) (via dilution system) 3 Vortex cable (to dilution system) Connections on the rear of the dilution system: 4 Power supply for dilution system 5 Connection for power supply to au- tosampler...
  • Page 41 PlasmaQuant 9200 Installation and commissioning Fig. 28 Connection to control computer via hub 1 Connection of the USB cables from au- 2 Hub tosampler, dilution system, and switch- ing valve 3 USB cable to the PC 4 Power supply to hub } Connect the dilution system to the autosampler and Cetac ASXPress Plus switching valve using the following hoses: Fig. 29...
  • Page 42 Installation and commissioning PlasmaQuant 9200 Fig. 30 Connect the hoses to the switching valve 1 Switching valve 2 6-port valve with labeled hose connec- tions Software support for commis- The control of the autosampler, dilution system, and switching valve is integrated into sioning and maintenance the ASpect PQ software.
  • Page 43 PlasmaQuant 9200 Installation and commissioning Time Measure Software command Commissioning the dilu- Rinse the syringe pump, Prime syringe and vortexer ¡ tion system after instal- tubes, and vortex mixer ves- lation or maintenance sel with rinsing solution. After changing the dilu- Remove air bubbles from the ¡...
  • Page 44 Installation and commissioning PlasmaQuant 9200 Fig. 32 Install temperature-controlled spray chamber 1 Transfer tube 2 Temperature-controlled spray chamber 3 Argon hose 4 Nebulizer 5 Sample hose 6 Waste hose 7 Power cable 8 USB cable (to the PC) } Place the temperature-controlled spray chamber (2) in the sampling compartment of the emission spectrometer.
  • Page 45 PlasmaQuant 9200 Installation and commissioning 4.4.5 Installing the argon humidifier Fig. 33 Installing the argon humidifier 1 Gas inlet: Argon hose from ICP-OES 2 Bypass valve (ON/Bypass) 3 Gas outlet: Argon hose to nebulizer 4 Glass vessel with membrane coil } Assemble the argon humidifier as described in the enclosed data sheet. Be careful not to damage the membrane coil.
  • Page 46 Installation and commissioning PlasmaQuant 9200 4.4.6 Installing the inline filter Fig. 34 Installing the in-line filter 1 Sample hose to nebulizer 2 Filter block with hose connectors 3 Pump hose for sample } Insert the in-line filter into the hose path such that the arrow on the filter block points in the direction of flow (i.e.
  • Page 47 PlasmaQuant 9200 Installation and commissioning 4.4.7 Installing the kit for internal standard (KIS) The KIS is suitable for the analysis of samples in which the matrix has an influence on the measurement. If the standards and samples have a different viscosity, for example, this may influence the measurement result.
  • Page 48 Operation PlasmaQuant 9200 Operation Switching on the spectrometer and igniting the plasma CAUTION Risk of poisoning due to ozone and nitrous gases ¡ Switch on exhaust unit prior to igniting the plasma. ¡ Leave the exhaust unit switched on during operation. To ensure safe plasma operation, the device monitors the following conditions using safety circuits.
  • Page 49 PlasmaQuant 9200 Operation } Check the filling level of the waste bottle and empty the bottle if there is not enough reservoir available for analysis. } For manual operation without an autosampler, immerse the sample aspiration tube in the wash solution. No air must follow during the plasma ignition process. } Start the ASpect PQ program.
  • Page 50 Operation PlasmaQuant 9200 } Confirm the query to turn off the purge gas for the detector with Yes if you want to turn off the purge gas. If you are only interrupting work for a short time (up to 30 min) or are working in the UV range, do not turn off the purge gas.
  • Page 51 PlasmaQuant 9200 Operation Starting a measurement routine In preparation for a measurement, create a method and a sequence or use one of the prepared worksheets. If necessary, prepare a sample ID containing additional sample information such as dilu- tions. Prepare the samples for measurement, e.g., on the autosampler tray. Start measurement } Switch on the PC.
  • Page 52 Troubleshooting PlasmaQuant 9200 Troubleshooting Fault messages in the software NOTICE Risk of device damage Contact customer service in the following cases: ¡ The troubleshooting measures described do not eliminate the error. ¡ The error occurs repeatedly. ¡ The error message is not featured in the following list or the list refers to customer service for troubleshooting the error.
  • Page 53 PlasmaQuant 9200 Troubleshooting Error code/error message 3871: No cooling water available (detector cooling)! Cause Remedy ¡ The recirculating chiller is not switched ¡ Switch on the recirculating chiller ¡ Check the cooling water flow at > 0.85 l/ ¡ The cooling water flow is too low 3872: CCD cooling is inactive! Cause Remedy...
  • Page 54 Troubleshooting PlasmaQuant 9200 Error code/error message 4010: Plasma shut-down because cooling water temperature too high (out)! Cause Remedy ¡ The cooling water flow is too low ¡ Determine the coolant flow, replace the ¡ The cooling temperature setting at the coolant recirculating chiller is too high ¡...
  • Page 55 PlasmaQuant 9200 Troubleshooting Error code/error message 5204: Status: Plasma error! Cause Remedy ¡ Device communication error ¡ Restart the device (and PC if relevant) ¡ The step motor for grating, prism, shut- ¡ Inform service ter is faulty 5206: Status: One or more safety interlocks are open! Cause Remedy ¡...
  • Page 56 Troubleshooting PlasmaQuant 9200 Adjustment on the analyte channel Adjust the x/y offset of the method pa- ¡ ¡ rameter in thePlasma|Optimize plasma view position window (see on- line help or software manual) Leak in the sample feed system (e.g., in Check the sample and pump hoses and ¡...
  • Page 57 PlasmaQuant 9200 Troubleshooting The measured value is too high Cause Remedy ¡ Error in calibration ¡ Check the calibration solutions ¡ Matrix-related spectral overlay, mea- ¡ Select another undisturbed analysis line surement is performed on a peak shoul- ¡ Perform spectral correction (correction model) Contamination/carry-over Find and remedy the cause for contami-...
  • Page 58 Maintenance and care of the emission spectrometer PlasmaQuant 9200 Maintenance and care of the emission spectrometer The operator may not undertake any service or maintenance work to this device and its components other than that specified in these instructions. Observe the information in the "Safety instructions" section for all maintenance work. Compliance with the safety instructions is a prerequisite for the error-free operation of the device.
  • Page 59 PlasmaQuant 9200 Maintenance and care of the emission spectrometer Maintenance overview Basic device Maintenance interval Maintenance task Daily and after mainte- Check the filling level of the wash solution bottle, replenish ¡ nance Check the filling level of the waste bottle, empty ¡...
  • Page 60 Maintenance and care of the emission spectrometer PlasmaQuant 9200 Maintenance interval Maintenance task Replace the glass body of the demountable torch if it is ¡ cracked. Replace the one-piece torch completely if it is dam- aged. Autosampler Maintenance interval Maintenance task Daily and after mainte- ¡...
  • Page 61 PlasmaQuant 9200 Maintenance and care of the emission spectrometer CAUTION Risk of injury A risk of injury due to broken glass is present when handling glass parts. ¡ Handle glass parts with extreme caution. ¡ Wear non-slip glass handling gloves that allow a firm and secure grip. Clean the torch in case of visible soiling (deposits or scaling).
  • Page 62 Maintenance and care of the emission spectrometer PlasmaQuant 9200 } Unscrew the torch from the carriage on the rail guide. } Remove first the outer and then the inner tube carefully from the holder in a twisting motion.  CAUTION! The quartz tubes are very fragile and are firmly mounted in the ground glass connector of the holder.
  • Page 63 PlasmaQuant 9200 Maintenance and care of the emission spectrometer } Insert the outer tube into the glass body with a twisting motion. Make sure that the ground joint seal is tight. } Reinstall the torch. Replacing the glass body The glass body of the demountable torch only needs to be replaced if it is cracked. When cleaning the torch, check the glass body for contamination by particles or solvents.
  • Page 64 Maintenance and care of the emission spectrometer PlasmaQuant 9200 } The glass body is correctly aligned when the two slanted bores for the ar- gon inlet are centered in the openings on the back of the holder. } Check the O-rings. Renew worn O-rings. } Insert the three O-rings and carefully press them onto the glass body.
  • Page 65 PlasmaQuant 9200 Maintenance and care of the emission spectrometer } Push the O-ring about 1 cm onto the injector. } Push the injector into the holder with a twisting motion. } Screw the connecting piece onto the holder as far as it will go. This will seal and adjust the injector properly.
  • Page 66 Maintenance and care of the emission spectrometer PlasmaQuant 9200 CAUTION Risk of injury A risk of injury due to broken glass is present when handling glass parts. ¡ Handle glass parts with extreme caution. ¡ Wear non-slip glass handling gloves that allow a firm and secure grip. Cleaning the one-piece torch You need to clean the torch if it is visibly dirty.
  • Page 67 PlasmaQuant 9200 Maintenance and care of the emission spectrometer } Insert the torch into the holder as far as it will go. Align the torch so that the gas inlet opening of the torch is centered in the gas connection of the holder, see arrow.
  • Page 68 Maintenance and care of the emission spectrometer PlasmaQuant 9200 } Screw the gas connection into the holder so that it is flush with the sur- face of the holder.  NOTICE! Danger of glass breakage! Do not screw in the gas connec- tion any further under any circumstances.
  • Page 69 PlasmaQuant 9200 Maintenance and care of the emission spectrometer Fig. 41 Nebulizer cleaning tool 1 Nebulizer 2 Nebulizer holder 3 1st red O-ring 4 Syringe WARNING Risk of methanol poisoning Methanol is poisonous if inhaled, swallowed or on skin contact. The liquid and its vapors are highly flammable.
  • Page 70 Maintenance and care of the emission spectrometer PlasmaQuant 9200 Cleaning and decontaminating the sampling compartment and the plasma compartment The responsible body at the installation site is in charge of carrying out suitable decon- tamination should the device become contaminated externally or internally with dan- gerous substances.
  • Page 71 PlasmaQuant 9200 Maintenance and care of the emission spectrometer CAUTION Risk of burns from the induction coil and torch Plasma is extremely hot. The induction coil and torch are still very hot after the plasma has been extinguished. Contact with the hot surfaces can cause burns. ¡...
  • Page 72 Maintenance and care of the emission spectrometer PlasmaQuant 9200 } Select 3 lines, one line each in the low UV range, in the medium and in the high wavelength range. } For a QC sample, determine the intensities at these 3 wavelengths and record the re- sults in a QC card or a table.
  • Page 73 PlasmaQuant 9200 Maintenance and care of the emission spectrometer Maintaining the horizontal The horizontal window is used for radial observation. window } Before cleaning: Extinguish the plasma via the ASpect PQ software by clicking on in the toolbar. Alternatively, use to open the Plasma window and click on Plasma off.
  • Page 74 Maintenance and care of the emission spectrometer PlasmaQuant 9200 Checking the gas system for leaks Check for leak tightness weekly and whenever the device has been disconnected from the gas supply system. For this purpose, close the shut-off valve of the gas supply system and check the pressure at the downstream manometer.
  • Page 75 PlasmaQuant 9200 Maintenance and care of the emission spectrometer 7.10 Replacing the air filter The air inlet filter is located in a drawer on the front of the device. Check the filter monthly and replace it if heavily soiled. Check the underside of the filter for dirt. A heavily soiled filter can reduce heat dissipation from the device.
  • Page 76 Maintenance and care of the emission spectrometer PlasmaQuant 9200 Fig. 44 Video: Cleaning the water filter under running water (available in the on- line help) 7.12 Maintenance on the ASPQ 3300 autosampler 7.12.1 Replacing the cannula and sample hose The autosamplers are delivered with a cannula to which the sample tube is attached. Cannula and sample tube are always replaced at the same time.
  • Page 77 PlasmaQuant 9200 Maintenance and care of the emission spectrometer Fig. 45 Replacing the cannula and sample tube of the autosampler 1 Connecting piece (attachment to the 2 Sealing cone holder) 3 Banjo bolt 4 Connecting piece (attachment to the holder) 5 Cannula with sample tube (one piece) 7.12.2 Replacing the pump hoses of the purging pump CAUTION Risk of chemical burns during hose replacement...
  • Page 78 Maintenance and care of the emission spectrometer PlasmaQuant 9200 Fig. 46 Purging vessel and pump on the sampler 1a Intake connection for purging solution 1b Purging solution hose on the purging vessel 2a Waste connection on the purging vessel 2b Hose to the waste container 3 Clamping bracket 4 Clamping lever with spring 5 Pump speed controller...
  • Page 79 PlasmaQuant 9200 Maintenance and care of the emission spectrometer } Replace defective power fuses. Only use T 5 A H 250 V. 5 x 20 mm type fuses. } Insert the fuse into the clip marked with an arrow (see image). } Connect the power cable and the serial connection (HOST) to the sampler. } Switch on the sampler via the power switch.
  • Page 80 Maintenance and care of the emission spectrometer PlasmaQuant 9200 – Switch off the recirculating chiller. – On the recirculating chiller, disconnect the cooling water return flow connection and hold the tube in the receptacle (bucket). – Switch the recirculating chiller back on and allow it to run until the flow of cooling water ends and only mist comes out.
  • Page 81 PlasmaQuant 9200 Transport and storage Transport and storage Preparing the device for transport } Switch on the device and start the control software. } Remove cooling water from the system: – Start the wizard to replace the cooling water in the control software. –...
  • Page 82 Transport and storage PlasmaQuant 9200 Observe the guide values and adhere to the legally mandated limits for lifting and ¡ carrying loads without auxiliary means. ¡ Observe the installation conditions at the new location. Transport When transporting the device, observe the safety instructions in the "Safety instructions" section.
  • Page 83 PlasmaQuant 9200 Transport and storage } Switch on the device and start the control software on the PC. See also 2 Installation and commissioning [} 23] Installing the recirculating chiller NOTICE Risk of damage to the device due to incorrect operation of the recirculating chiller ¡...
  • Page 84 Disposal PlasmaQuant 9200 Disposal Most waste produced via analysis is in the form of aqueous solutions. Aside from metal and heavy metal ions, these primarily contain various mineral acids used in sample preparation. For safe disposal of this waste, all solutions must be neutralized with an alkaline so- lution such as a diluted sodium hydroxide solution.
  • Page 85 PlasmaQuant 9200 Specifications Specifications 10.1 Technical data 10.1.1 Basic device technical data PlasmaQuant 9200 Elite Monochromator Echelle grating double monochromator with a focal length of F= 400 mm and variable gap; pre-monochromator with quartz prism, wavelength selection via additional reflected neon radiator Wavelength range 160 to 900 nm Wavelength accu-...
  • Page 86 Specifications PlasmaQuant 9200 Signal evaluation Spectrally resolved Spectra of 20 to 200 pixels width Analytic data Sample type Liquid Type of nebulizer Concentric nebulizer Spray chamber Cyclone chamber Power supply Operating voltage 200 to 240 V AC ±10 % Frequency 50/60 Hz Power connection Device connection: C19 input socket ¡...
  • Page 87 PlasmaQuant 9200 Specifications Air pressure 0.7 bar to 1.06 bar Max. permissible altitude 2000 m Storage Temperature: -40 °C to +70 °C Use drying agent Protection type IP 20 Degree of contamination Extraction Material Heat-resistant and corrosion-resistant (recommended: V2A steel) External pipe diameter 125 mm Extraction output 3.5 m³/min (min.), 5.5 m³/min (max.) Optimal: 4.0 to 4.5 m³/min Adapter using flexible aluminum pipe Pipe diameter: 125 mm...
  • Page 88 Specifications PlasmaQuant 9200 Supply voltage / frequency 110 V / 60 Hz 230 V / 50/60 Hz Typical average power con- 2900 VA sumption Cooling performance 3000 VA at 25 °C Mass (empty) 92 kg Silent version (optional), ≤ 57 dB(A) sound pressure level ¡ Length of the water tub- ¡...
  • Page 89 PlasmaQuant 9200 Specifications Racks 3 (sample vessels), 2 (special cups) Purging bottle 2 l 10.1.5 Technical data for other accessories Autosampler Teledyne Cetac ASX-560 Dimensions 580 mm x 620 mm x 550 mm (W x H x D) Mass 12 kg Cetac ASX-280 Dimensions 360 mm x 620 mm x 550 mm (W x H x D) Mass 8.1 kg Cetac XLR-860...
  • Page 90 Specifications PlasmaQuant 9200 10.2 Guidelines and standards Compliance with the following guidelines and regulations applicable to the product is declared: Low Voltage Directive – 2014/35/EU ¡ EMC Directive – 2014/30/EU ¡ ¡ RoHS Directive – 2011/65/EU Applied harmonized standards are: EN 61010-1:2010+A1:2019 ¡...
  • Page 91 PlasmaQuant 9200 List of figures List of figures Fig. 1 Emission spectrometer with open plasma compartment .................. 13 Fig. 2 Device with removable sample tray ........................14 Fig. 3 Transporting the device............................14 Fig. 4 The plasma compartment ........................... 15 Fig.
  • Page 92 List of figures PlasmaQuant 9200 Fig. 39 Animation: Cleaning the one-piece torch, including replacing the sealing rings (available in the online help)..................................66 Fig. 40 Video: Cleaning the nebulizer (available in the online help)................68 Fig. 41 Nebulizer cleaning tool............................69 Fig.

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