Conditioning Ferrules; Tips And Hints - Agilent Technologies 5977C Series Operating Manual

2 Installing 8890 GC Columns

Conditioning ferrules

Column bleed is most common in new or poorly crosslinked columns. It is much
worse if there are traces of oxygen in the carrier gas when the column is heated.
To minimize column bleed, all capillary columns should be conditioned before
they are installed in the GC/MSD interface.
Conditioning ferrules
Heating ferrules to their maximum expected operating temperature a few times
before they are installed can reduce chemical bleed from the ferrules. Thermal
cycling ferrules to their maximum operating temperatures, prior to running your
application, will help reduce leaks from the assembly.

Tips and hints

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If you are using hydrogen as a carrier gas or for the JetClean system, the hydrogen
WAR N IN G
gas flow must be off before turning off the MSD power. If the foreline pump is
off, hydrogen will accumulate in the MSD and an explosion may occur. Read
"Hydrogen Safety"
Always wear safety glasses when handling capillary columns. Avoid
WAR N IN G
puncturing your skin with the end of the column.
5977C GC/MSD Operating Manual
The column installation procedures for the 5977C Series MSDs may be
different from that for previous MSDs. Using the procedure from another
instrument may not work, and may damage the column or the MSD.
Always use carrier gas that is at least 99.9995% pure.
Because of thermal expansion, new ferrules may loosen after heating and
cooling a few times. Check for tightness after two or three heating cycles or
use the self tightening column nuts.
Always wear clean gloves when handling columns, especially the end that
will be inserted into the GC/MSD interface.
on page 22 before operating the MSD with hydrogen gas.
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