Agilent Technologies 5975 Series Manuals

Manuals and User Guides for Agilent Technologies 5975 Series. We have 4 Agilent Technologies 5975 Series manuals available for free PDF download: Operation Manual, Operating Manual, Hardware Installation, Site Preparation Manual

Agilent Technologies 5975 Series Operation Manual (192 pages)

Series MSD

Brand: Agilent Technologies | Category: Laboratory Equipment | Size: 5.89 MB

Table of Contents

5
- Series MSD Operation Manual for Masshunter
  9
1 Introduction

11
- Introduction
  12
  - 5975 MSD Version
    12
  - Abbreviations Used
    13
  - The 5975 Series MSD
    15
  - CI MSD Hardware Description
    17
  - Important Safety Warnings
    19
    
    Electrostatic Discharge Is a Threat to MSD Electronics
    19
    
    Many Internal Parts of the MSD Carry Dangerous Voltages
    19
    
    Many Parts Are Dangerously Hot
    20
    
    The Oil Pan under the Standard Foreline Pump Can be a Fire Hazard
    20
  - Hydrogen Safety
    21
    
    GC Precautions
    21
    
    Dangers Unique to GC/MSD Operation
    22
    
    Hydrogen Accumulation in an MSD
    22
    
    Precautions
    24
  - Safety and Regulatory Certifications
    26
    
    Information
    26
    
    Symbols
    27
    
    Electromagnetic Compatibility
    28
    
    Sound Emission Declaration
    28
  - Cleaning/Recycling the Product
    29
  - Liquid Spillage
    29
  - Moving or Storing the MSD
    29
2 Installing Gc Columns

31
- Columns
  32
  - Conditioning Columns
    32
    
    Conditioning Ferrules
    33
    
    Tips and Hints
    33
- Installing GC Columns
  34
3 Operating in Electron Impact (Ei) Mode

51
- Operating in Electron Impact (EI) Mode
  52
4 Operating in Chemical Ionization (CI) Mode

101
- Operating in Chemical Ionization (CI) Mode
  102
  - General Guidelines
    102
  - The CI GC/MSD Interface
    103
  - To Operate the CI MSD
    105
  - To Switch from the EI Source to the CI Source
    106
  - To Pump down the MSD in CI Mode
    107
  - To Set up the Software for CI Operation
    108
  - To Operate the Reagent Gas Flow Control Module
    110
  - To Set up Methane Reagent Gas Flow
    114
  - To Use Other Reagent Gases
    117
  - To Switch from the CI Source to the EI Source
    121
  - CI Autotune
    122
  - To Perform a PCI Autotune (Methane Only)
    124
  - To Perform an NCI Autotune (Methane Reagent Gas)
    126
  - To Verify PCI Performance
    128
  - To Verify NCI Performance
    129
  - To Monitor CI Mode High Vacuum Pressure
    130
5 General Maintenance

133
- Before Starting
  134
- Maintaining the Vacuum System
  139
- To Replace the Primary Fuses
  140
- To Remove the EI Ion Source
  142
- To Disassemble the EI Source
  144
- To Clean the EI Source
  146
- To Assemble an EI Source
  149
- To Replace a Filament in an EI Source
  152
- To Reinstall the EI Ion Source
  154
- To Replace the Electron Multiplier Horn
  156
6 CI Maintenance

159
- General Information
  160
- To Set up Your MSD for CI Operation
  161
- To Install the CI Ion Source
  162
- To Install the CI Interface Tip Seal
  164
- To Remove the CI Source
  165
- To Disassemble the CI Source
  167
- To Clean the CI Source
  169
- To Assemble the CI Source
  171
- To Replace a Filament in a CI Source
  173
  - A Chemical Ionization Theory
    175
  - Chemical Ionization Overview
    176
  - Positive CI Theory
    178
  - Negative CI Theory
    185

Agilent Technologies 5975 Series Operating Manual (164 pages)

MSD For OpenLAB CDS

Brand: Agilent Technologies | Category: Laboratory Equipment | Size: 12.43 MB

Hardware User Information
4
Introduction
9
5977B Series MSD Version
10
Abbreviations Used
11
The 5977B Series MSD
13
MSD Hardware Description
15
Important Safety Warnings
16
Hydrogen Safety
19
- GC Precautions
  19
- Precautions
  21
Safety and Regulatory Certifications
23
Intended Use
26
Cleaning/Recycling the Product
26
Accidental Liquid Spillage
26
Moving or Storing the MSD
26
To Replace the Primary Fuses
27
Installing 7890/7820/6890/6850 GC Columns
29
Columns
30
To Install a Capillary Column in a Split/Splitless Inlet
32
To Condition a Capillary Column
35
To Install a Capillary Column in the GC/MS Interface Using the Self-Tightening Column Nut
36
To Install a Capillary Column in the GC/MS Interface Using a Standard Column Nut
41
- Nut
  41
To Install the Interface Tip Seal
44
To Calibrate Column Flow Linear Velocity
46
The GC/MSD Interface for a 7890B Series GC
49
Intuvo 9000 GC Column Maintenance
51
Columns
52
To Replace an Intuvo GC Column
55
To Replace an Intuvo 9000 GC Gasket
59
To Install a Column Guard or Jumper Chip
60
To Replace the 9000 GC/MS Tail
64
To Condition an Intuvo Capillary Column
68
To Install the Interface Tip Seal
70
The GC/MS Interface for a 9000 Series GC
72
Operating in EI Mode
75
Operating the MSD from the DS
76
Operating the MSD from the GC Control Panel
77
Configuring the MSD through the Web User Interface (WUI)
81
- To Change the Network Settings of the MSD
  81
Operating the 5975/5977 MSD from the Local Control Panel (LCP)
84
- Modes of Operation
  84
- LCP Status Messages
  86
- To View System Status During Startup
  87
Emodule Mini Display Readout
91
Front Panel Instrument Status LED
91
The GC/MSD Interface
92
Before You Turn on the MSD
94
Pumping down
95
Controlling Temperatures
95
Controlling Column Flow
95
Venting the MSD
96
Set MS Analyzer Temperatures
97
Enable the GC/MS Interface and Oven
99
View MSD Temperatures and Vacuum
100
To Run an Autotune
102
To Open the MSD Covers
103
Vent the MSD
104
To Pump down the MS
106
To Move or Store the MSD
109
General Maintenance
111
Before Starting
112
Maintaining the Vacuum System
116
Maintaining the Analyzer
117
To Open the Analyzer Chamber
119
To Remove the EI HES
121
To Connect/Disconnect Wiring to the EI HES
123
To Disassemble the EI HES
124
To Clean the EI HES
127
To Assemble the EI HES
130
To Remove the EI HES Filaments
135
To Install the EI HES Filament
137
To Install the EI HES
138
To Remove the EI XTR, SS, or Inert Source
139
To Connect/Disconnect Wiring from the EI XTR, SS, and Inert Sources
140
To Disassemble the EI SS or EI Inert Source
141
To Disassemble the EI XTR Source
144
To Clean an EI XTR, SS, or Inert Source
147
To Assemble an EI SS or Inert Source
151
To Assemble the EI XTR Source
154
To Replace a Filament in an EI XTR, SS, or Inert Source
157
To Install the EI XTR, SS, or Inert Source
159
To Replace the Electron Multiplier Horn
160
To Close the Analyzer Chamber
162

Agilent Technologies 5975 Series Hardware Installation (60 pages)

Mass Selective Detectors

Brand: Agilent Technologies | Category: Security Sensors | Size: 6.08 MB

Table of Contents
3
1 General Information

8
- Introduction
  8
- Important Safety Warnings
  10
- Safety and Regulatory Certifications
  13
  - Information
    13
  - Symbols
    14
  - Electromagnetic Compatibility
    15
  - Sound Emission Declaration for Germany
    15
- Cleaning
  16
- Recycling the Product
  16
- Customer Responsibilities
  17
- Before You Start
  18
- Other Documentation
  19
2 Installation

21
3 Checklists

45
- Installation Checklist
  46
- Customer Familiarization Checklist
  53
  - Topics Not Included in Familiarization
    53
  - Hardware Overview
    54
  - System Operation
    54
- MSD Chemstation Software Overview
  54
- MSD Chemstation Software Autotune Descriptions
  54
- Methods
  55
- Data Acquisition
  55
- Data Analysis
  55
- Sequence
  56
- MSD Chemstation Maintenance
  56
- EI Instrument User Maintenance
  56
- Troubleshooting (Diagnostics)
  57
- Tune Charts
  57
- Additional Support Information
  57

Agilent Technologies 5975 Series Site Preparation Manual (44 pages)

Mass Selective Detectors

Brand: Agilent Technologies | Category: Computer Accessories | Size: 1.71 MB

Table of Contents
3
1 General Information

6
- Instrument Identification
  6
  - 5975 MSD Versions
    6
- Important Safety Warnings
  7
- Hydrogen Safety
  9
- Chemical Safety
  10
- Safety and Regulatory Certifications
  11
  - Information
    11
  - Symbols
    12
  - Electromagnetic Compatibility
    13
  - Sound Emission Declaration
    13
- Cleaning
  14
- Recycling the Product
  14
2 Site Preparation

15
- Overview
  16
  - Customer Responsibility
    16
  - Agilent Responsibility
    17
  - Other Documentation
    19
- Space and Weight Requirements
  20
- Communications Requirements
  22
  - Telephone
    22
  - Site LAN Network
    22
- Electrical Requirements
  23
  - Voltage Ranges of Major Components
    23
  - Power Configurations
    24
  - Power Requirements
    25
  - Power Plugs and Cord
    26
  - Other Electrical Considerations
    27
- Air Conditioning and Environmental Requirements
  28
  - Temperature, Humidity, and Altitude
    28
  - Airborne Dust
    29
  - Exhaust Venting
    29
  - Fume (Exhaust) Hood
    30
- Carrier and Reagent Gas Requirements
  31
  - Regulators, Tubing, and Fittings
    32
- Laboratory Supply Requirements
  33
  - Cleaning Solvents
    33
  - Data System Supplies
    33
  - Spare Parts and Consumables
    34
- Receiving the System
  37
  - Delivery and Unloading
    37
  - Inspecting for Damage
    37
  - Storage
    38
  - Unpacking
    38
- Installation and Verification
  39
  - Installation
    39
  - Verification
    39
  - Sensitivity Specifications
    40

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3 Operating in Electron Impact (Ei) Mode

4 Operating in Chemical Ionization (CI) Mode

5 General Maintenance

6 CI Maintenance

Agilent Technologies 5975 Series Operating Manual (164 pages)

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