Buchi SpeedExtractor E-916 Operation Manual
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Buchi SpeedExtractor E-916 Operation Manual

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SpeedExtractor E-916 / E-916XL / E-914
Operation Manual
093218G en

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Summary of Contents for Buchi SpeedExtractor E-916

  • Page 1 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual 093218G en...
  • Page 2 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience; espe- cially in respect to structure, illustrations and technical detail. This manual is copyright. Information from it may not be reproduced, distributed, or used for competitive purpos- es, nor made available to third parties.

  • Page 3: Table Of Contents

    4.5.3 General information on buttons ......................29 4.5.4 Rear connections ...........................30 4.5.5 Side connections ...........................30 Putting into operation ..............................31 Installation site ..............................31 Electrical connections ............................32 Gas and solvent connections..........................33 Dehydration ................................34 Functional test ..............................34 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 4 8.1.4 The pump is not aspirating properly .....................79 8.1.5 Replacement of check valves ......................80 8.1.6 Precipitation in the outlet lines ......................81 8.1.7 Malfunctions of the rotating valves ....................82 8.1.8 Upgrading a 2-port mixer to a 4-port mixer ................82 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 5 Store the manual in the immediate vicinity of the instrument, so that it can be consulted at any time. No technical modifications may be made to the instrument without the prior written agreement of BUCHI. Unau- thorized modifications may affect the system safety or result in accidents.

  • Page 6: About This Manual

    1 About this manual About this manual This manual describes the SpeedExtractor E-916 / E-914 and provides all information required for its safe operation and to maintain it in good working order. It is addressed in particular to laboratory personnel and operators.

  • Page 7: Abbreviations

    Materials and chemicals Combination of tetrafluoroethylene and hexafluoropropylene FFPM Perfluoro caoutchouc PTFE Polytetrafluoroethylene Polyoxymethylene (commercialized as Delrin® by DuPont) PEEK Polyether ether ketone Tetrahydrofurane Miscellaneous firm ware quantity Temperature difference Pressure difference SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 8: Safety

    Use in conjunction with solvents that have a low self ignition point or contain peroxides, such as diethyl ether or THF. • Use of cells, seals, hoses, and tubes other than the originals from BUCHI. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 9: Safety Warnings And Safety Signs Used In This Manual

    Table of supplementary safety information symbols The reference list below incorporates all safety information symbols used in this manual and their meaning. Symbol Meaning General warning Electrical hazard Harmful to life-forms SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 10 Paragraphs starting with Note transport helpful information for working with the device/software or its supplementary. Notes are not related to any kind of hazard or damage. NOTE Useful tips for the easy operation of the instrument/software. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 11: Product Safety

    Risk of burns by hot heating block and extraction cells. • Do not touch hot parts or surfaces • Let the system and inserted extraction cells cool down safely • Do not move the instrument or parts of it when hot SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 12: Warning Labels On Housing And Assemblies

    Observe supplementary data sheets of all used chemicals. • Handle corrosives in well ventilated environments only. • Always wear protective goggles. • Always wear protective gloves. • Always wear protective clothes. • Do not use damaged glassware. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 13: Built-In Safety Elements And Measures

    The presence of extraction cells in the heating block is checked in the tightness test at the begin- ning of each extraction process. Seismic tie-down In earthquake-susceptible regions the instrument should be tied down by the ventilation slot on the rear of the instrument. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 14: General Safety Rules

    Modifications to the instrument are only permitted after prior consultation and with the written approval of the manufacturer. Modifications and upgrades shall only be carried out by an authorized BUCHI technical engineer. The manufacturer will decline any claim resulting from unauthorized modifications.
  • Page 15 2 Safety SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 16: Technical Data

    Check the scope of delivery according to the order number and your shipping note. NOTE For detailed information on the listed products, see www.buchi.com or contact your local dealer. Instrument configurations The SpeedExtractor is available in 21 different configurations differing in the number of positions (E-916: 6 positions, E-916XL: 6 position, E-914: 4 positions), the type of solvent mixer (2 ports or 4 ports), and the size of the extraction cells (E-916: 10 –...
  • Page 17 FEP waste tube 1/16", 0.5 m 053303 Solvent bottle 1 L 053203 Quartz sand 0.3–0.9 mm, 2.5 kg 037689 Extraction Record demo license 053074 053691 053690 11069547 Extraction cell carrier Solvent filter 044340 Turix wrench 044349 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 18 Supporting ring PEEK 053667 053666 11069769 Filter hook 053316 053038 053037 11069530 Plunger Syringe 60 mL 034882 Brush small 053256 Brush large 053257 053026 053030 11069534 Gripper extraction cell Bit wrench 052783 Extruder rod 11055284 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 19: Materials Used

    Extraction cells Stainless steel Lines to waste Needles Stainless steel Collection vials Glass Septa for vials Silicon, PTFE Collection unit Stainless steel, POM Pump PTFE, ceramic, stainless steel Protective shield Glass, POM SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 20 For indoor use only 5 – 40 °C Temperature Altitude up to 2000 m maximum relative humidity 80 % for temperatures Humidity up to 31 °C, and then linearly decreasing to 50 % at 40 °C Noise level <70 dB *Accessories SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 21 3 Technical data SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 22: Description Of Function

    6 samples. The SpeedExtractor E-916 can be used for 6 samples with a maximum volume of 40 mL. The SpeedExtractor E-916XL can be used for 6 samples with a volume of 60 mL. The SpeedExtractor E-914 can be be used for up to 4 samples with a limited maximum volume of 120 mL.
  • Page 23 To compensate the pressure a second needle connects the collection bottle with an exhaust joint situated on the rear of the instrument. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 24: Overview Of The Extraction Process

    Flushing with nitrogen to remove residual solvent (see section 6.4.2). • Unloading the heating block (see section 6.4.9). NOTE Preheating the instrument to the temperature of operation prior to loading it with the extraction SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 25: Schematic Representation Of The Process

    This is usually done to prepare the system for another run with a different solvent. For a thorough description of each step please refer to section 6.4. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 26: Controls And Connections

    • press three times: stops the process immediately, i.e. the system remains at the very position of the process For more information see section 6.4.8. e Selection knob to define values within the instru- ment software. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 27: Main Displays Of The Instrument

    D MENU involves all functions that are not directly involved in an extraction method but are typically used at start-up, during maintenance, and service, and for product information. These four main displays contain the following elements: SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 28 Editing an existing (or default) extraction method (see section 6.4.3). d Open an existing extraction method (see section 6.4.6). e Save a previously edited extraction method (see section 6.4.3). f Delete an existing extraction method (see section 6.4.3). SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 29 In this case a scroll bar on the right hand side indicates the presence of hidden lines. Move down with down button to get access to this informa- tion. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 30: General Information On Buttons

    Load the predefined solvents by replacing the first 10 entries of the list Move lift (heating block or rack) up Move lift (heating block or rack) down Stop moving the lift Skip an extraction step or stop the running leak test SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 31: Rear Connections

    Waste outlet for flushing with solvent or collecting extracts 4.5.5 Side connections a Nitrogen inlet b Solvent 1 c Solvent 2 d Optional (with 4-port mixer only): solvent 3 e Optional (with 4-port mixer only): solvent 4 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 32: Putting Into Operation

    Keep external vibrations away from the instrument • Safely attach the instrument to the bench in earthquake prone regions • Do not operate the instrument without the protection cover installed at the front SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 33: Electrical Connections

    Check for sufficient grounding NOTE • External connections and extension lines must be provided with a grounded conductor lead (3-pole couplings, cord or plug equipment). All used power cords must meet the input power requirements. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 34: Gas And Solvent Connections

    Risk of instrument damage by dry running instrument parts, especially valves. • Never run the instrument or parts of it without any solvent • Connect the EXHAUST and WASTE outlets on the back of the instrument accordingly. EXHAUST WASTE SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 35: Dehydration

    To make sure that the installation procedure has been carried out properly and the system is tight, carry out a leak test (see section 6.2.5) before putting the instrument into operation for the first time. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 36: Operation

    For further information regarding the vial change, see section 6.4.3. Further information about how to optimize the extraction process is given in section 6.4.7. BUCHI's SpeedExtractor Application booklet and Application notes give detailed information about method de- velopment and method parameters for a waste range of applications.

  • Page 37: Preparing The Instrument

    • with chlorinated organic solvents for 2 min with methanol • with acidic or basic solvents with pure organic solvents such as ethanol or distilled water See section 6.2.6 for a description of the flushing process. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 38: Modifying The Solvent List

    • To modify a name (e.g. Dichloromethane_1) open the EDIT menu, choose the corresponding charac- ters and press SELECT. Confirm the changes with ACCEPT. The modified name now appears on the same position as previously Dichloromethane. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 39: Preheating The Instrument

    Do not touch hot parts or surfaces • Do not move the instrument or parts of it when hot NOTE Never preheat the instrument when the system is closed. Always equilibrate the instrument with vacant positions first. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 40: Activating/Deactivating Positions

    All extraction positions are deactivated by default. It is possible to activate all positions together or each individually. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 41: Leak Test

    (see section 6.2.3 and 6.4.1). • Activate all positions (see section 6.2.4). • Place empty collection vials into the collection rack and put it on the instrument as described in section 6.4.1. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 42 The measured pressure remains on the display. The evaluation of leak tests is described later in this section. Standard leak test The reference settings are used for the standardized leak test. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 43 The overall pressure should not rise until the difference between overall pressure and position pressure(s) reached min. 25 bar. After this the overall pressure is al- lowed to rise and to follow the position pressure(s). SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 44: Flushing The Instrument

    In contrast to flushing during extraction (see section 6.4.2), the flow rate is not reduced in the FLUSH SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 45: Activating The Ecomode

    • Open EXTRACTION  PREHEAT. Move down to ECOMODE with the corresponding function button and activate it using the selection knob. There is no need to confirm with ON. By simply ticking it the ECOMODE is already activated. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 46: Preparing The Sample

    For critical samples it is therefore recommended to use a smaller cooling unit instead (P/N 053682). Exchange of the cooling unit, however, requires an authorized service technician. Please contact BUCHI or your local dealer. 6.3.2...

  • Page 47: Extraction Cell Selection

    (P/N 053209) using the plug screw tool d (P/N 053607). Make sure that the concave surface of the plug screw points to the cell. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 48 This prevents the sample from clogging in case of swelling and thereby guarantees uniform flow. Differently packed extraction cells usually require different amounts of solvent, because the dead volume and back pressure are different. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 49 Use the brushes for that purpose. Any remaining sample or grain of sand reduces the lifetime of the cup seals and the extraction cells significantly. In case of proper operation the seals last for 100 extraction runs. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 50: Extraction Process

    The collection tray must be placed properly on the instrument to start a method. It is not possible to start a run in the absence of the tray. Make sure to always fill the collection tray with empty collection vials. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 51: Stages Of An Extraction Cycle

    • Heat-up time (heat-up of sample, solvent and cell) In the time period between the tightness test and hold step the pressure is increased step-by-step SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 52: Creating New Methods

    As a rule of thumb it is recommended to set the temperature approximately 20 – 30 °C over the boiling point and the pressure to 100 bar. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 53 • The EDIT button allows you to directly modify the solvent name without changing the solvent list. Press ACCEPT to confirm the changes and switch back to the EDIT METHOD display with the left arrow. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 54 • The time of the flush with solvent and flush with gas can be entered by turning the selection knob. It is mandatory to flush the system with gas for at least 1 min (E-916) or 2 min (E-914) respectively. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 55: Summary Of Operating Parameters

    Size of the collection bottle. There are different vials avail- 60, 150, 220, 240 mL, able from BUCHI: flat bottom narrow neck vials (60, 240 mL) / unspecified, waste round bottom open neck vials (220  m L) / Analyst vials (150  m L) (default: 240 mL)
  • Page 56 The solvent used in the last cycle is (default: 1 min) also used for the flush. FLUSH WITH GAS Time flushing with nitrogen. 1, 2 – 30 min (default: 3 min) SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 57: Example Of An Extraction Method

    All saved methods (up to 100) are stored in a numbered table. Select the desired method and press OK. The name of the method now appears in the title of the main display. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 58: Optimize A Process

    0-1 bar. For more detailed information about method development and optimization, please consider BUCHI's SpeedExtractor Application booklet and BUCHI's Application and Technical Notes. Please contact your sales person or BUCHI for these documents.

  • Page 59: Start, Pause, Stop And Abort Extraction

    (or a methanol/acetone/hexane mixture) for 5 – 15 min, and then put them in a dishwasher or oven. Do not exceed 300 °C for the latter. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 60: Creating A Report (Optional)

    PDF or CVS format. For more information regarding the SpeedExtractor Record software, please refer to the corresponding manual on the free trial CD (valid for 60 days) which is part of the scope of delivery (P/N 053074). SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 61 6 Operation SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 62: Maintenance

    Flushing the lines • If the next extraction method involves a different type of solvent, flush the lines thoroughly with the new solvent as described in section 6.2.6. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 63: Periodic Maintenance

    Proceed in reverse order to install the new seal. Make sure that the spring of the seals always points to the extraction cell. Perform a leak test to check the tightness of the system (see section 6.2.5). SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 64: Tube Connections And Needles

    To reduce any dead volume and potential sources of contamination, make sure that the ferrule is always flush with the end of the tube. The pointed end of the ferrule is oriented to the fitting. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 65 If there is constant leaking, inspect the tube and connector and replace them if necessary. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 66: Septum

    5 runs. Septum Vessel Corresponding septum Narrow-necked vials qty 100, P/N 049536 (60, 240 mL) Wide-necked vials qty 12, P/N 053677 (150, 220 mL) SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 67: Pump Maintenance

    ¼” spanner wrench while continuously pressing the capil- lary to the inside until the end of the capillary is firmly seated on the bottom of the opening bottom. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 68: Back Washing

    SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 69 7 Maintenance SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 70: Troubleshooting

    “Remedy”. More complicated malfunctions or errors are usually handled by a BUCHI technical engineer who has access to the official service manuals. In this case, please contact your local BUCHI customer service agent.
  • Page 71 Error 20 Vial lift motor blocked. Please The lift does not move at all most Contact BUCHI customer service. refer to user manual. probably due to a faulty v-belt or motor. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 72 Please refer to user NOTE manual. It is generally recom- mended to accommodate all positions to achieve best reproducible results. See also 6.2.4. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 73 Error 59 Nitrogen inlet pressure out of Nitrogen tank is not connected Check the pressure and connec- range. Please check nitrogen or empty. tion of the nitrogen tank. See supply. also section 5.3. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 74 Position X: Pressure out of range. The pressure sensor located Contact BUCHI customer service. Please refer to user manual. between the position valve and error 82 extraction cell is faulty and needs to be replaced. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 75: Handling And Resolving Blockages

    Secondly, the cell lift does not open when the process is finished to avoid splashing of the sample. There are different reasons why blockages can occur during extraction under high pressure and high temperature using the SpeedExtractor E-916 / E-914: inappropriate sample preparation, extraction parameters, or instrument configuration. Often a combination of these factors can cause blockages.
  • Page 76 The position is still tight, but the pressure will be decreased due to the larger volume now inside the cell. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 77 "//" indicates that it does not make sense to follow this way due to moving in circles. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 78 Start a flush into the collection vials (see section 6.2.6). If solvent flows into the vials, the cell (sample inside the cell, the filter or frit) was blocked. If solvent does not flow into the vial, the SpeedExtractor is blocked and further steps are necessary. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 79 If the SpeedExtractor is still blocked after this extraction it will be necessary to identify the blocked part. The flow test in the service menu allows locating the blockage within the instrument. See section 8.2.4. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 80: The Pump Is Not Aspirating Properly

    NOTE The syringe P/N 034882 is made of polypropylene and is therefore not compatible with halogenated solvents (i.e. dichloromethane) and acids. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 81: Replacement Of Check Valves

    • Attempt to clean the valves in acetone using ultrasound (or in another solvent), which dissolves the buffers you have been using. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 82: Precipitation In The Outlet Lines

    The alternative cooling unit (P/N 053682) must be installed by a BUCHI approved service technician. Please refer to your local dealer or BUCHI customer service.

  • Page 83: Malfunctions Of The Rotating Valves

    8.1.8 Upgrading a 2-port mixer to a 4-port mixer A BUCHI-approved service technician can retrofit a 2-port configuration with a 4-port mixer (P/N 053381). Please contact the local dealer or BUCHI customer service. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 84: Description Of The Service Menu

    A relative comparison of the pres- ging of the lines. sure makes it possible to quickly identify positions with possibly clogged lines, particle precipitation or capillary deformations. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 85: Checking The Valves

    Press CALIBRATE to move the valve back to its initial position. Pressing END shows the STATUS display with the current set- tings. Press END to go back to the SERVICE FUNCTIONS. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 86: Checking The Sensors

    Go to SERVICE FUNCTIONS  PUMP. Enter the flow rate us- ing the selection knob (1 – 50 mL/min). Press ON. The ACTUAL VALUE converges to the set value. If the ACTUAL VALUE remains 0, the pump is defective. Contact a BUCHI service engineer. The actual pressure is shown.

  • Page 87: Inspecting The Lines (Flow Test)

    A leak test must be carried out to ensure the tight- ness of the SpeedExtractor. If pressure builds up, a part inside the SpeedExtractor is blocked. Release the pressure manually and continue with test 4. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 88 Between lower seal holder Flow test: Heater in back and outlet valve: lower seal Test 4 position, beaker under- holder, cooling unit, capillary, neath outlet valve Not ok Top cover plate or before SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 89: Moving The Cell And Vial Lift

    (SN) and firm- ware version (FW) which are helpful in case of troubleshooting. Go back to the SERVICE FUNCTIONS with the left arrow. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 90: Customer Service

    Contacts for official BUCHI customer service offices are provided on the BUCHI website at: www.buchi.com. If your instrument malfunctions or you have technical questions or application problems, please contact one of these offices.
  • Page 91 8 Troubleshooting SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 92: Shutdown, Storage, Transport And Disposal

    Consult three further persons to transport the instrument • Do not drop the instrument or its transport box • Place the instrument on a stable, even and vibration-free surface • Keep limbs out of crushing zone SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 93: Disposal

    Follow valid regional and local laws concerning disposal. For help, please contact the local authorities. NOTE When returning the instrument to the manufacturer for repair work, please copy and complete the health and safety clearance form on the following page and enclose it with the instrument. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 94: Health And Safety Clearance

    Company name or stamp: Place, date: Name (print), job title (print): Signature: Health and Safety Clearance_20081110.doc_20081110 Version 1.0 Page 1/1 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 95 9 Shutdown, storage, transport and disposal SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 96: Spare Parts

    BUCHI. Always indicate the product designation and part number when ordering any spare parts. Use only genuine BUCHI consumables and spare parts for maintenance and repair, in order to ensure optimum system performance and reliability. Prior written permission of the manufac- turer should be obtained before any modifications are made to the spare parts used.
  • Page 97 Septa for narrow-necked vials 100 049536 n Collection vials, narrow-necked, 052672 flat bottom, 240 mL o Collection unit for E-916 053698 q Retaining plate for Syncore 11058339 Analyst R-12 vessels, for E-914 r Collection unit E-914 11058332 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 98 29.2/32 flange Accessories related to the SpeedExtractor E-914, mounted on the pedestal Item Order no. a Flask collection unit for longer 11058527 flasks, e.g. pear flasks b Polyvap R-6 collection unit 11058528 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 99 100 11058656 PTFE Accessories related to waste/solvent bottles Item Order no. a Safety cap for waste bottle, 7-port 1 11056948 b Safety cap, 2-port 11056949 c Solvent bottle with GL 45 cap 053203 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 100 11055334 Extraction thimble, cellulose, 80  m L 25 11059610 Extraction thimble, cellulose, 11055358 120 mL Extraction thimble, glass fiber, 11056633 40 mL Extraction thimble, glass fiber, 11059612 80 mL Extraction thimble, glass fiber, 11059611 120 mL SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 101 Suction tube, FEP, OD 1/8” 5 m 11055604 b 1/4 UNF-28 fitting 1/8”, green 053663 c 1/4 UNF-28 ferrules, green 053664 d Outlet capillary, metal, left* 053613 e Outlet capillary, metal, right* 053614 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 102 Further accessories Item Order no. a 4 port solvent mixer* 053381 b Small cooling unit for viscous 053682 samples* *Technician required for installation. Housing Item Order no. a Covering glass needle assembly 051322 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 103 /h, <10 mbar) with profes- sional vacuum controller, Woulff bottle and sec. condenser Recirculating Chiller F-105, 230 V 11056462 Recirculating Chiller F-105, 115 V 11056463 Recirculating Chiller F-108, 230  V 11056464 Recirculating Chiller F-108, 115 V 11056465 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 104 SpeedExtractor Quick Guide 093286 Software Product Order no. Product Order no. SpeedExtractor Record, demo 053074 Operation manual, software, EN PDF incl. on CD license SpeedExtractor Record license 053073 USB cable 2.0 A-B, 4.5 m 049226 SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
  • Page 105 10 Spare parts SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...

  • Page 106: Declarations And Requirements

    L’utilisation de cet appareil dans les zones résidentielles peut causer des interférences néfastes, auquel cas l’exploitant sera amené à prendre les dispositions utiles pour palier aux interférences à ses propres frais. SpeedExtractor E-916 / E-916XL / E-914 Operation Manual...
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