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Summary of Contents for Buchi Melting Point M-560
- Page 1 Melting Point M-560 Operation Manual 093251G en OM_093251_M-560_en_G.indd 1 12.07.2018 09:21:10...
- Page 2 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience; espe- cially in respect to structure, illustrations and technical detail. This manual is copyright. Information from it may not be reproduced, distributed, or used for competitive purpos- es, nor made available to third parties.
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Page 3: Table Of Contents
No technical modifications may be made to the instrument without the prior written agreement of BUCHI. Unauthorized modifications may affect system safety or result in accidents. This manual is copyrighted. Information from it may not be reproduced, distributed, or used for competitive purposes, nor made available to third parties. - Page 4 11.1 FCC requirements (for USA and Canada) ..... . . 45 Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 3...
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Page 5: About This Manual
1 About this manual About this manual This manual describes the Melting Point M-560 and provides all the information required for its safe operation and to maintain it in good working order. It is addressed in particular to laboratory personnel and operators. -
Page 6: Safety
2 Safety Safety This section highlights the safety concept of the Melting Point M-560 and contains general rules of behavior and warnings about hazards concerning the use of the product. The safety of users and personnel can only be ensured if these safety instructions and the safety- related warnings in the individual sections are strictly observed and followed. -
Page 7: Warning Notices Used In This Manual
2.5.2 Other hazards WARNING Certain solvents within or in the vicinity of the Melting Point M-560 can form peroxides and/or are highly inflammable. • Always be aware of the explosion risk when working with hazardous substances or with substances of unknown composition. -
Page 8: Safety Measures
Modifications to the instrument are permitted only after prior consultation with and written approval from the manufacturer. Modifications and upgrades should be carried out only by an authorized BUCHI technical engineer. The manufacturer reserves the right to decline any claim resulting from unauthorized modifications. -
Page 9: Technical Data
3 Technical data Technical data This section introduces the reader to the Melting Point M-560 and its main components. It contains technical data, requirements and performance data. Scope of delivery Check the scope of delivery according to the order number. - Page 10 A) Boiling point tubes, 10 units 019697 B) Boiling point capillaries, 10 units 051850 User management activation code 11066387 Compaction wire 036721 Operation Manual: English 93251 German 93252 French 93253 Italian 93254 Spanish 93255 Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 9 12.07.2018 09:21:12...
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Page 11: Optional Accessories
Melting point capillaries, 1000 units 001759 Mortar and pestle, agate 041867 Compact keyboard German (CH) 029509 Compact keyboard English (USA) 029508 Serial dot matrix printer (including ribbon, 11055438 paper roll, and cables) Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 10 12.07.2018 09:21:14... -
Page 12: Technical Data Overview
019007 B) Boiling point capillaries, 100 units 051890 Protective cover 051935 Technical data overview Table 3-4: Technical data of the Melting Point M-560 Melting Point M-560 √ Manual melting point determination √ Manual boiling point determination Automatic melting point determination –... -
Page 13: Materials Used
3 Technical data Table 3-4: Technical data of the Melting Point M-560 Melting Point M-560 ±0.5 °C Accuracy of boiling point at 1.0 °C/min up to 400 °C Repeatability of boiling point at 1.0 °C/min ±0.3 °C Temperature gradients, °C/min 0.1, 0.2, 0.5, 1, 1.5, 2, 2.5, 3, 5, 10, 20... -
Page 14: Description Of Function
The boiling point is determined by the “Siwoloboff” method. The Melting Point M-560 can be used to determine the boiling point of a small amount of liquid. The heating block has one insert available for boiling point tubes (outside left). The moment of boiling is determined visually. -
Page 15: Controls And Connections
PS/2 connection for keyboard c RS 232 connection for serial printer d USB connection: required for service e Housing cooling fan f Heating block cooling fan PS/2 RS232 Fig. 4.2: Rear view Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 14 12.07.2018 09:21:15... -
Page 16: Putting Into Operation
5 Putting into operation Putting into operation This section describes the installation of the Melting Point M-560 and gives instructions for initial start- NOTE Inspect the instrument for damage during unpacking. If necessary, prepare a status report imme- diately to inform the postal company, railway company, or transport company. Keep the original packaging for future transport. - Page 17 • Press the glass holder down. Accessories • Place the melting point capillaries in the hole of the housing. The second hole is a reservoir for used capillaries. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 16 12.07.2018 09:21:16...
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Page 18: Power Connection
Calibration NOTE Before use it is recommended to calibrate the apparatus. Use supplied calibration substances only. Calibration is carried out in accordance with section 6.4 of these operating instructions. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 17 12.07.2018 09:21:17... -
Page 19: Operation
Operation This section explains the operating elements and possible operating modes. It gives instructions on how to operate the Melting Point M-560 properly and safely. ATTENTION Before use it is recommended to calibrate the apparatus. Use supplied calibration substances only. -
Page 20: Display During A Process Or In Menus
Working area shows: • items to select • samples during measurement • specific information in connection with the current menu c Functions selectable by the keys below. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 19 12.07.2018 09:21:17... -
Page 21: Entering Text
• ENTER = right softkey • Alt = center softkey • Esc = left softkey • In the method menu: To navigate quickly to a method name press the initial letter. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 20 12.07.2018 09:21:18... -
Page 22: Melting Point Determination
6.2.1 Sample preparation NOTE Use only capillaries from BUCHI. They are precise and adequate for this kind of operation. Other capillaries have other dimensions and wall thicknesses. Using others may result in results that are incorrect. Each sample has to be prepared. -
Page 23: Determination Without Pre-Registered Melting Point Method
Next. press Next. knob, and press Save. NOTE Insert samples only when the start temperature is reached (as soon as prompted). Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 22 12.07.2018 09:21:18... - Page 24 • To register additional temperature stamps, manu- ally press the SET button for the related sample. Each button can be pressed three times. Registered temperature stamps are displayed in green. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 23 12.07.2018 09:21:18...
- Page 25 The last result is stored in the device until a new measurement is started or the instrument is switched off. • After turning back to idle, the last result can be checked again by pressing Result. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 24 12.07.2018 09:21:19...
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Page 26: Creating A Method
• Delete: Deletes the parameters. method. • Rename: Changes the method name. NOTE FOR USER MANAGEMENT Methods can only be started in the user level. All other actions are not possible. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 25 12.07.2018 09:21:19... -
Page 27: Adjusting Parameters During A Determination
The result is printed out if a printer is connected. Printout a Instrument type b Determination parameters c Manual pressed results d General information e Signature of person making the determination Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 26 12.07.2018 09:21:19... -
Page 28: Boiling Point
6 Operation Boiling point NOTE For exact boiling point determination, use boiling point tubes and capillaries from BUCHI only. If other glass parts are used, incorrect or no results may be obtained. Use the following items: Product Order number A) Boiling point tubes, 10 units... - Page 29 “Barometric the setting “Sample ID pressure request” (see 6.5). request” (see 6.5). • Insert sample and press START to begin the deter- mination. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 28 12.07.2018 09:21:20...
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Page 30: Creating A Method
• Adjust the parameters by CHANGED (a) for the pressing Edit. Adjusting the temperature gradient. parameters does not affect the saved method. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 29 12.07.2018 09:21:20... -
Page 31: Printout
Boiling temp. = Temperature sample boiled. Boiling point = Boiling temp. corrected according entered barometric pressure. If a barometric pressure of 1013 mbar is entered boiling temperature and boiling point results are equal. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 30 12.07.2018 09:21:20... -
Page 32: Calibration
NOTE The instrument is calibrated using melting point standards. The calibration is valid for boiling points as well. The calibration procedure is recommended to be performed with the BUCHI calibration substances, in the BUCHI calibration set mode. Use the calibration set (11055018). This calibration set contains the melting point standards listed below. - Page 33 • The Print key is used to print out the data. • Back exits this menu. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 32 12.07.2018 09:21:21...
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Page 34: Printout
Thus, the value indicated for the Average might deviate from the value you calculate on the basis of the temperature values on the printout, as there is just one position after the decimal point. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 33... -
Page 35: User Calibration
6.4.2 can be performed with the user calibration mode. 6.4.5 Verification To verify the calibration, proceed as follows: • Measure all standards (BUCHI recommends using the verification set (11055019) but it is also possible to use your internal standards. NOTE The verification is not a guided process. - Page 36 Whether or not it is possible to change parameters (start temperature, stop temperature and temperature gradient) during a determination. Calibration interval 0–36 months: default 12 months. BUCHI recommends calibration or verification after 12 months using the calibration set and the verifica- tion set. Sample ID request enabled: After the start of determination, the sample ID window is displayed.
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Page 37: Test Protocol
The instrument can only be started in the administrator mode if the correct password is entered. 6.5.1 Test protocol a Power supply voltage b Signature of person carrying out the test Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 36 12.07.2018 09:21:23... -
Page 38: Sysinfo Protocol
6 Operation 6.5.2 SysInfo protocol a Setting parameters b Calibration correction values c Date of factory tests Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 37 12.07.2018 09:21:23... -
Page 39: User Management
Table 6-7: PC settings Baud rate: 19200 Parity: Data bit: Stop bit: No PC software is supplied to receive the XML data. Picking up the data is the customers responsibility. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 38 12.07.2018 09:21:23... -
Page 40: Maintenance
• Prior to any maintenance work on the instrument, switch off the power supply. ATTENTION Use only genuine BUCHI consumables and spare parts for any maintenance and repair work in order to assure continued system performance and reliability. Any modifications to the spare parts used should be carried out only with the prior written permission of the manufacturer. - Page 41 • If glass parts of a melting point capillary are stuck in a hole of the metal heating block, use the cleaning tool as shown in the picture. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 40 12.07.2018 09:21:23...
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Page 42: Troubleshooting
“Remedy”. More complicated malfunctions or errors are usually handled by a BUCHI technical engineer who has access to the official service manuals. In this case, please contact your local BUCHI customer service agent. -
Page 43: Setting The Printer Baud Rate
Contacts for official BUCHI customer service offices are available on the BUCHI website at: www. buchi.com. If malfunctions occur on your instrument or you have technical questions or application problems, please contact one of these offices. -
Page 44: Shutdown, Storage, Transport, And Disposal
To dispose of the instrument in an environmentally friendly manner, a list of materials is given in section 3.3, please ensure that the components are separated and recycled correctly. Please follow current regional and local laws concerning disposal. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 43 12.07.2018 09:21:24... -
Page 45: Spare Parts
Spare parts This section lists spare parts, accessories and optional extras, including all of the relevant order information for ordering from BUCHI. Always state the product designation and part number when ordering any spare parts. To ensure optimum system performance and reliability, use only genuine BUCHI consumables and spare parts for maintenance and repair. -
Page 46: Declarations And Requirements
L’utilisation de cet appareil dans les zones résidentielles peut causer des interférences néfastes, auquel cas l’exploitant sera amené à prendre les dispositions utiles pour palier aux interférences à ses propres frais. Melting Point M-560 Operation Manual, Version G OM_093251_M-560_en_G.indd 45 12.07.2018 09:21:25... - Page 47 T +52 55 9001 5386 F +66 2 862 08 54 F +971 4 313 2861 latinoamerica@buchi.com bacc@buchi.com middleeast@buchi.com www.buchi.com/es-es www.buchi.com/th-th www.buchi.com We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com OM_093251_M-560_en_G.indd 46 12.07.2018 09:21:26...
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