Buchi Rotavapor R-220 Pro Operation Manual
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Buchi Rotavapor R-220 Pro Operation Manual

Buchi Rotavapor R-220 Pro Operation Manual

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Rotavapor
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R-220 Pro
Operation Manual
11593893E en

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  • Page 1 Rotavapor ® R-220 Pro Operation Manual 11593893E en...
  • Page 2 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience; espe- cially in respect to structure, illustrations and technical detail. This manual is copyright. Information from it may not be reproduced, distributed, or used for competitive purpos- es, nor made available to third parties.

  • Page 3: Table Of Contents

    Connection eld at the rear-side ........28 Connection of the Rotavapor R-220 Pro to the Recirculating Chiller F-325 and ..
  • Page 4 Table of contents 5.13 Heating bath setup for 2×1800 W heating element ......54 5.13.1 Water as heating transfer medium........56 5.13.2 Heating transfer media with high boiling point .

  • Page 5: About This Manual

    No technical modi cations may be made to the instrument without the prior written agreement of BUCHI. Unauthorized modi cations may a ect the system safety or result in accidents. Technical data are subject to change without notice.

  • Page 6: Safety

    2 Safety Safety This chapter highlights out the safety concept of the instrument and contains general rules of behavior and warnings from direct and indirect hazards concerning the use of the product. For the users' safety, all safety instructions and safety messages in the individual chapters shall be strictly observed and followed.

  • Page 7: Safety Warnings And Safety Signals Used In This Manual

    2 Safety Safety warnings and safety signals used in this manual DANGER, WARNING, CAUTION and NOTICE are standardized signal words for identifying levels of hazard seriousness of risks related to personal injury and property damage. All signal words, which are related to personal injury are accompanied by the general safety sign. For your safety it is important to read and fully understand the below table with the di erent signal words and their de nitions! Sign Signal word...
  • Page 8 2 Safety Explosive gases, explosive environment Harmful to life-forms Hot item, hot surface Device damage Inhalation of substances Explosive substances Flammable substances Fragile items / content Warning, heavy item Environmental pollution hazard Do not dispose of in household trash R-220 Pro Operation Manual...
  • Page 9 2 Safety Use of water is mandatory (non-standard symbol) Wear protective mask Wear laboratory coat Wear protective goggles Wear protective gloves Heavy weight, lifting requires more than one person Additional user information Paragraphs starting with NOTE transport helpful information for working with the device / software or its supplementaries.

  • Page 10: Product Safety

    2 Safety Product safety Safety warnings in this manual (as described in section 2.4) serve to make the user alert and to avoid hazardous situations emanating from residual dangers by giving appropriate counter measures. However, risks to users, property and the environment can arise when the instrument is damaged, used carelessly or improperly.

  • Page 11: Warning Labels On Housing

    2 Safety NOTICE Risk of instrument short-circuits and damage by liquids. • Do not spill liquids over the instrument or its component parts • Wipe o any liquids instantly • Ensure a safe positioning of the evaporating ask for storage •...

  • Page 12: Personal Safety Measures

    2 Safety 2.5.3 Personal safety measures Always wear personal protective equipment such as protective eye goggles, protective clothing and gloves when working with the instrument. Wear inhalation protection when working with hazardous solvents and all kind of respirable material or material of unknown composition. WARNING Death or serious poisoning by contact or incorporation of harmful media at use.

  • Page 13: General Safety Rules

    Modi cations to the instrument are only permitted after prior consultation with and with the written approval of the manufacturer. Modi cations and upgrades shall only be carried out by an authorized BUCHI technical engineer. The manufacturer will decline any claim resulting from unauthorized modi - cations.

  • Page 14: Technical Data

    3 Technical data Technical data This chapter introduces the reader to the instrument and its speci cations. It contains an overview of available glassware con gurations, technical data, requirements and performance data. Available system con gurations and dimensions 1750 1200 R-220 Pro Operation Manual...

  • Page 15: Typical Example Applications And Accessories

    Concentration of large volumes Inlet valve Recrystallization Drying Vapor duct with frit NOTE For large scale continous evaporation BUCHI o ers the R-220 Pro in continous version with a highly automated re ll and product receiving process. R-220 Pro Operation Manual...

  • Page 16: Technical Data

    3 Technical data Technical data R-220 Pro R-220 Pro R-220 Pro R-220 Pro Essential Continuous High Performance Dimensions (W x D x H) 1200 x 710 x 1750 1100 x 560 x 1700 1200 x 600 x 1750 1200 x 710 x 1800 Weight 100 kg 85 kg...
  • Page 17 3 Technical data R-220 Pro R-220 Pro R-220 Pro R-220 Pro Essential Continuous High Performance Heating bath medium Water Water (4200 W heater) Heating bath medium Water (6300 W heater) Heating capacity Ambient to 180 °C Ambient to 180 °C Ambient to 180 °C (3600 W heater) Heating capacity...
  • Page 18 3 Technical data Display Bath temperature 1 °C steps Cooling temperature (option) 1 °C steps Vapor temperature 1 °C steps Set rotation speed 1 rpm steps Set bath temperature 1 °C steps Actual vacuum 1 mbar steps Set vacuum 1 mbar steps Materials Housing Stainless steel 1.4301 (AISI 304)

  • Page 19: Description Of Function

    4 Description of function Description of function This chapter explains the basic working principle of the Rotavapor ® R-220 Pro. It also shows how the instrument is structured and provides a general functional description of its assemblies. Functional principle of a Rotavapor ®...
  • Page 20 4 Description of function Safety reserve Cooler with cooling medium Optimal condensation zone range (~ 80% cooler height) Rotation drive for evaporating ask Evaporating solvent Condensated solvent Heating bath with heating liquid Evaporation area The solvent is heated by means of a heating bath. The turbulent mixing inside the rotating evaporating ask results in an increased evaporation rate.

  • Page 21: Rotavapor Front-Side

    4 Description of function Rotavapor ® front-side Various glassware con gurations are available for the Rotavapor ® R-220 Pro. Condenser(s) Manual inlet valve Distribution piece Evaporating ask Shut o tap Receiving ask Draining valve R-220 Pro Operation Manual...

  • Page 22: Tubing Scheme

    4 Description of function Tubing scheme      R-220 Pro Operation Manual...
  • Page 23 4 Description of function Vacuum / gas circuit Vacuum pump (recommended type: For most applications a vaccum is used to signi cantly reduce Vacuum Pump V-600) the boiling point of the liquid content inside the evaporating ask. 2 + 3 Aeration / inert gas inlet at the The aeration valves at the optional vacuum controller and Vacubox...

  • Page 24: Cooling Water Routing

    4 Description of function 4.3.1 Cooling water routing General memory aid for cooling water routing Independent of the number of coolers, the water inlet has to be connected in ascending order starting with the cooler closest to the receiving vessel. The water output is always the upper connector! Example: Output (sink or chiller re ux)

  • Page 25: Vaccum Routing

    4 Description of function 4.3.2 Vaccum routing General memory aid for vacuum routing Independent of the installed glassware setup the vacuum pump has to be connected at the end of the cooling path. Depending on the used setup this can either be subsequently at or after the last condenser.
  • Page 26 4 Description of function Example 2: Connection to Vacubox Vapor temp. sensor Connection to vacuum source End of cooling path Vapor path R-220 Pro Operation Manual...

  • Page 27: User Interface Front-Side

    4 Description of function User interface front-side Interface I-300 Pro (see separate Operation Manual of the I-300 Pro) Turning knob to adjust rotational speed and bath temperature ON / OFF switch Button Functionality Set the bath temperature, change value with the turning knob Heater: Switches the heating bath ON / OFF ON/OFF...

  • Page 28: Connection Eld At The Rear-Side

    4 Description of function Connection eld at the rear-side        R-220 Pro Operation Manual...
  • Page 29 It must be installed in serial after the cooling water source. See Operation Manual of the BUCHI COM bus sockets with power over bus connector. Suit- connected device(s)! able BUCHI devices: Vacuum pump, vacuum controller, chiller Cooling water ow sensor (optional).
  • Page 30 4 Description of function Position Drawing Description Cooling water temperature sensor. Must be looped-in between  cooling water source outlet and cooler/cooler assembly of the Rotavapor ® Vacubox. For a detailed description see I-300 Pro operation  manual. See master drawing for appearance ...

  • Page 31: The Vacuum Pump V-600

    4 Description of function Connection of the Rotavapor ® R-220 Pro to the Recirculating Chiller F-325 and the Vacuum Pump V-600  Communication link between Rotavapor® R-220 Pro and Recirculating Chiller F-325. Communication link between Rotavapor ® R-220 Pro and Vacuum Pump V-600. Vacuum tubing between Rotavapor ®...

  • Page 32: Placement Of The Automatic Sensor

    4 Description of function Placement of the automatic sensor  Location of the temperature sensor Connection of the automatic sensor to the VacuBox (connection port: VT/AS). Cooling water inlet into the automatic sensor (connection port: IN). Cooling water ow from the automatic sensor to the condenser ...

  • Page 33: Putting Into Operation

    Put the instrument on a stable, horizontal surface. Consider the maximum product dimensions and weight. Obtain the environmental conditions as described in section 3.2, technical data. Installation on the dedicated mobile trolley (order no. 041257) or the BUCHI Recirculating Chiller F-325 is also possible.

  • Page 34: Electrical Connections

    5 Putting into operation NOTICE Risk of instrument damage by liquids or mechanical shocks. • Do not spill liquids over the instrument or its components • Do not move the instrument when it is loaded with sample liquid • Do not drop the instrument or its components •...
  • Page 35 5 Putting into operation NOTICE Risk of instrument damage by wrong mains supply. • External mains supply must meet the voltage given on the type plate • Check for su cient grounding R-220 Pro Operation Manual...

  • Page 36: Sensor Setup And Adjustments

    5 Putting into operation Sensor setup and adjustments Sensor setup menu These instructions are valid for the setup menu of the cooling water sensor and level sensors connected at the rear connection eld. Lift Keep the "LIFT UP" button pressed while switching on the Rotavapor ®...

  • Page 37: Level Sensors

    5 Putting into operation 5.3.1 Level sensors Description of function: The capacitive level sensors are recommended for setups with two receiving asks to achieve unin- terruptible evaporation over a longer period and for larger product volumes. The sensitivity of the capacitive level sensors must be adjusted to safely detect the liquid level between di erent products.

  • Page 38: Cooling Water Ow Sensor

    5 Putting into operation 5.3.2 Cooling water ow sensor The switching threshold of the ow sensor can be adjusted by shifting the sensor element up and down. CW Flow Adjustment instructions • Make sure the ow sensor is installed in an upright position! Loosen the locking screw a. •...

  • Page 39: Foam Sensor

    5 Putting into operation 5.3.3 Foam sensor Description of function: A foam sensor is highly recommended whenever heavily foaming products are in use. When foam formation is detected by the sensor, the aeration valve of the Rotavapor ® will be opened for an instant, causing the foam to collapse.
  • Page 40 5 Putting into operation Adjustment instructions • Make sure the foam sensor is installed correctly. Remove the white plastic screw a to get access to the sensor adjustment screw. • Allow su cient foam formation. • As soon as the foam touches the sensor housing, the LED at the sensor must switch active, causing the aeration valve to open for an instant.

  • Page 41: Vapor Temperature Sensor

    5 Putting into operation 5.3.4 Vapor temperature sensor Description of function: Enables the vapor temperature reading at the Rotavapor display. ® Vapor temperature sensor VAPOR TEMP. Installation instructions: Turn the ring nut a of the sensor to fasten and tighten the temperature sensor. Insert the sensor plug at the "VAPOR TEMP."...

  • Page 42: Cooling Water Temperature Sensor

    5 Putting into operation 5.3.5 Cooling water temperature sensor Description of function: Enables the cooling water temperature reading at the Rotavapor display. ® Condenser output Cooling water temperature sensor Sensor socket CW TEMP. To sink / chiller input Installation instructions: Use hose clamps to install the sensor at the hosing between condenser output and sink or chiller input.

  • Page 43: Setting Up The Support Rod(S)

    5 Putting into operation Setting up the support rod(s)  Install the retaining bracket at the housing. Fasten the Torx screw with included tool. Premount the headless screw with a few turns at the side thread of the bracket. Remove the blind plug from the blind hole at the foot of the Rotavapor ®...

  • Page 44: Condenser Clamps

    5 Putting into operation Condenser clamps Flat spring Turn the lever counterclockwise to loosen / open the clamp. It is not necessary to completely open the clamp! Pull the support o-ring onto the rod. Shift the opened clamp with the at spring side onto the rod until it touches the o-ring.

  • Page 45: Easyclamps

    5 Putting into operation EasyClamps EasyClamps can be found at glassware connections. EasyClamps can be cleaned assembled or dissassembled in an ultrasonic bath, e.g. with a soapy detergent if cleaning is necessary. Stage 1 Turn counterclockwise to loosen the thumb nut Stage 2 Type: DN45 Type: DN 25...

  • Page 46: Inlet Valve

    5 Putting into operation Inlet valve The inlet valve allows continous feeding and manual aeration (e.g. at foam formation) of the evapo- rating ask. The feeding throughput is manually adjustable via the thumbscrew. NOTE The PTFE seal element inside the valve is a standard spare part and can be exchanged easily accor- ding to the drawing below.

  • Page 47: Glassware And Con Gurations

    5 Putting into operation Glassware and con gurations All original glassware parts and accessories are of superior quality. However, glassware is generally fragile and must be handled with appropriate care to achieve a long lifetime and safe use. Every glassware part must be inspected visually prior to use to ensure safe and proper functionality. Visually inspect glassware for: •...
  • Page 48 5 Putting into operation It is recommended to install a glassware setup starting with the distribution piece at the gearbox. All other parts will subsequently be aligned towards the Rotavapor ® via the distribution piece. The drawing below shows an example installation of a complex setup. For other setups proceed adaptive (e.g.

  • Page 49: Single Receiver

    5 Putting into operation 5.11 Single receiver Outlet of glassware con guration Shut-o tap EasyClamp (DN 25) Branching piece EasyClamp (DN 25) Aeration screw cap Receiving ask EasyClamp (DN 25) Draining valve R-220 Pro Operation Manual...
  • Page 50 5 Putting into operation Preparational steps: • Install the appropriate glassware con guration between the gearbox and the branching piece • Install the support ring at the support rod on a low position • Install the shut-o tap at the branching piece Main installation: Connect the ball joint of the branching piece to the glassware con guration outlet.
  • Page 51 5 Putting into operation Outlet of glassware con guration Shut-o tap Branching piece 1 Branching piece 2 Aeration screw cap Receiving ask EasyClamp (DN 25) Draining valve Preparational steps: • Install the appropriate glassware con guration between the gearbox and the ‘branching piece 2’ •...
  • Page 52 5 Putting into operation Place the rst receiving ask on the support ring . ➥ Keep the receiving ask upright with one hand. ➡ Adjust the support ring until the ball joint between the receiving ask and the branching piece is seated without tension. Fixate the support ring in this position.

  • Page 53: Heating Bath Lling Level

    5 Putting into operation Install the draining valves with two EasyClamps (DN 25). 2× 5.12 Heating bath lling level The optimal lling level of the heating transfer medium in the bath ensures maximum evaporation performance and safe handling. Depending on the evaporating ask size, the level has to be adjusted. Filling procedure •...

  • Page 54: Heating Bath Setup For 2×1800 W Heating Element

    5 Putting into operation 5.13 Heating bath setup for 2×1800 W heating element The heating element holder is labelled with the heating power data. The heating bath of the 2×1800 W version can be lled with di erent kinds of liquid heating transfer medium. Depending on the maximum heating bath temperature for the target application, a suitable medium must be used.
  • Page 55 5 Putting into operation Basic heating transfer medium requirements • Do not use media which are corrosive against the heating bath and its subcomponents or the evaporating ask. E.g. add a su cient amount of borax when deionized water is used! •...

  • Page 56: Water As Heating Transfer Medium

    5 Putting into operation 5.13.1 Water as heating transfer medium With the heating bath in lowest position, install the level drain output tube with a level di erence of > 5 cm towards the sink to ensure safe draining. Fixate all tube connections with hose clamps! NOTICE Risk of damage caused by heating transfer mediums.

  • Page 57: Heating Transfer Media With High Boiling Point

    5 Putting into operation Level drain with Ø 12 mm hose connector, let into sink. Draining tap with Ø 12 mm hose connector, let into sink. Heating and cooling water source. If a water tap is used, the optional cooling water shut-o tap is recom- mended.

  • Page 58: Heating Bath Setup For 4.2 And 6.3 Kw Heating Element

    5 Putting into operation 5.14 Heating bath setup for 4.2 and 6.3 kW heating element The heating element holder is labelled with the heating power data. For the 4.2 and 6.3 kW versions only water must be used as heating transfer medium. Because of the enormous heat input there is a risk of smoke formation and re when using other heating transfer media than water! How to set the maximum setpoint temperature Limiting the maximal temperature set-point to a value below 100 °C can help to eliminate processing...
  • Page 59 5 Putting into operation Basic heating transfer medium requirements Do not use water which is corrosive against the heating bath and its subcomponents or the evapo- rating ask. E.g. add a su cient amount of borax when deionized water is used! DANGER Risk of re by use of ammable heating transfer media.

  • Page 60: Attaching And Removing Evaporating Asks

    5 Putting into operation 5.15 Attaching and removing evaporating asks Evaporating asks are available in di erent types and sizes to meet all kinds of application require- ments. However, the maximal load on the rotational ange must not exeed 20 kg! CAUTION Risk of minor or moderate injury by heavy weight of the evaporating ask.
  • Page 61 5 Putting into operation   Push down the unlock rocker at the left half of the snap ange. Open the snap ange completely and carefully take away the evaporating ask. Using the ask handler The handler can increase the level of safety when placed on top of the heating bath at ask exchange.

  • Page 62: Adjusting The Snap Ange

    5 Putting into operation NOTICE Risk of instrument damage by wrong mains supply. • External mains supply must meet the voltage given on the type plate • Check for su cient grounding 5.16 Adjusting the snap ange System tightness is essential when working with a Rotavapor ®...

  • Page 63: Installation And Usage Of A Shut-O Tap

    5 Putting into operation NOTE Perform the adjustment in single-turn steps only. Inbetween, check for proper tension with the empty evaporating ask. 5.17 Installation and usage of a shut-o tap The shut-o tap provides a three stage valve mechanism with a spring-loaded seal stamp. This prestressing assures safe seal under normal conditions.

  • Page 64: Removing The Interface For Remote Control

    5 Putting into operation 5.18 Removing the interface for remote control  • Tilt the I-300 Pro display towards you a. • Remove the I-300 Pro display b from the holder c. • You can ll the space with a blind cover (see chapter 10.5 "Optional equipment and upgrade parts") For reinstallation proceed in reverse order.

  • Page 65: Final Installation Check

    5 Putting into operation CAUTION Risk of injury when remote controlling Rotavapor® R-220 Pro without visual contact • Keep visual contact to the Rotavapor® R-220 Pro to ensure that no-one is attempting to operate the device while it is being remote controlled 5.19 Final installation check After installation has been completed and before performing the rst distillation make sure the instal-...

  • Page 66: Operation

    6 Operation Operation This chapter gives examples of typical instrument applications and instructions on how to operate the instrument properly and safely. See also section 2.5 “Product safety” for general warnings. NOTE Operation of the interface is explained in the operation manual of the Interface I-300 Pro. Evaporation in three steps a Preparational steps •...

  • Page 67: Optimal Distillation Conditions

    6 Operation Optimal distillation conditions To achieve optimal distillation conditions, all distillation energy supplied by the heating bath must be removed by the condenser. The physical cooling capacity of the condenser must not be exeeded in order to avoid steam emission by overpressure inside the assembly! NOTE: A temperature gradient of 20 °C between 'heating bath →...

  • Page 68: Solvent Table

    6 Operation Solvent table Molar mass Evaporation energy Boiling point Density in Vacuum in mbar for Solvent Formula in g / mol in J / g at 1013 mbar g / cm boiling point at 40 °C Acetone 58.1 0.790 n-amylalcohol, n-pentanol 88.1 0.814...

  • Page 69: Maintenance And Repairs

    Such training and knowledge can only be provided by BUCHI. Addresses of o cial BUCHI customer service o ces are given on the BUCHI website under: www.buchi.com. If malfunctions occur on your instrument or you have technical questions or applica- tion problems, contact one of these o ces.

  • Page 70: Regular Service And Checks

    7 Maintenance and repairs Regular service and checks To maintain the system in good working order the checks described in this section should be performed regularly. Defective or worn out parts must be exchanged directly to ensure safe use and optimal e ciency.

  • Page 71: Snap Ange Coupling, Ask Seal And Vapor Duct

    7 Maintenance and repairs Heating bath Use a commercially available decalci cation agent to dissolve residues of calcium and other minerals in the bath. Subsequently rinse the bath thoroughly! All housing parts must be completely dried before the system can be connected to mains again! WARNING Death or serious burns by electric current at cleaning.
  • Page 72 7 Maintenance and repairs Use the seal tool (order no. 20075) to unlock the metal reed and free the snap ange.  Carefully pull o the snap ange from the metal reed locking. For reinstallation plug the coupling back onto the ange. The metal reed snaps into locking position with a noticable click sound.
  • Page 73 7 Maintenance and repairs Removal / installation of the vapor duct With the ask seal removed, the (glass) vapor duct can easily be pulled out. At reinstallation, the keyway at the vapor duct end must be aligned to the spring loaded notch at the gearbox to lock rota- tion between the drive and the duct.

  • Page 74: Distribution Head Seal And Vacuum Seal

    7 Maintenance and repairs Distribution head seal and vacuum seal Removal of the seal holder Remove the snap ange coupling and the ask seal rst. Pull out the vapor duct by hand. Loosen the EasyClamp (DN70) and take o the distribution head (glass part). Subsequently, completely remove the EasyClamp from the gearbox.
  • Page 75 7 Maintenance and repairs Installation of the seal unit Place the vacuum seal onto the seal holder with the ring-shaped metal insert facing upwards. Take the seal holder into both hands and gently push in the seal with both thumbs in several steps.

  • Page 76: Troubleshooting

    8 Troubleshooting Troubleshooting This chapter helps to resume operation after a problem has occurred with the instrument which does not require special technical training. It lists possible occurrences, their probable cause and suggests how to remedy the problem. The troubleshooting table below lists possible malfunctions and errors of the instrument. The operator is enabled to correct some of those problems or errors by him/herself.

  • Page 77: Error Messages And Their Remedy

    The error messages are shown in the rotational speed display. Errors which are not listed in the table are to be corrected by a BUCHI trained technician who has access to o cial service manuals. In this case, please refer to your local BUCHI customer service agent.
  • Page 78 8 Troubleshooting Errors and their remedy Error Additional error indicator on display Possible cause Remedy E01 Heating bath icon ashes. Bath temp. sensor not connected or • Switch o the unit. Wait for the bath defective. to cool down a little before restart. Call service if problem is persistent.
  • Page 79 8 Troubleshooting E08 n.a. Shortcut at vacuum valve. • Unplug valve and restart system for causal research. • Exchange valve if defective. Call service if problem is persistent. Error Addition error indicator on display Possible cause Remedy E11 ‘SHIELD OPEN’ message Shield not closed at the time of •...
  • Page 80 8 Troubleshooting E14 ‘LEVEL 2’ message appears. Filling level reached. • Empty receiving vessel 2 and press the “Aerate” button to con rm the error message. • Check cable and plug of the ow sensor. • Exchange sensor if defective or run evaporation with user controlled lling level.
  • Page 81 8 Troubleshooting E33 Heating bath icon ashes. • Actual to set value di erence • Press “Aerate” button to con rm the is higher than 15 °C. error message. • Electronic malfunction. • Check set value for plausibility (e.g. set value below room temperature). If necessary, wait for the heating bath to cool down su ciently.

  • Page 82: Resettable Automatic System Fuses

    8 Troubleshooting Resettable automatic system fuses Fuse ok F1 — F4 (12A, 250V) Fuse triggered Resetting a system fuse • Switch o the Rotapavor ® • Push in the fuse for reset • Switch on the Rotavapor ® NOTE Device fuses may be triggered occasionally due to voltage peaks under high system load. When fuses trigger frequently, inform your customer service! Do not try to repair the fuses! R-220 Pro Operation Manual...

  • Page 83: Shutdown, Storage, Transport And Disposal

    9 Shutdown, storage, transport and disposal Shutdown, storage, transport and disposal This chapter instructs how to shut down and disposal of the instrument. Information about storage and shipping conditions can also be found here. Storage and transport Switch o the instrument and remove the power cord. To disassemble the Rotavapor ®...

  • Page 84: Disposal

    9 Shutdown, storage, transport and disposal Disposal For instrument disposal in an environmentally friendly manner, a list of materials is given in chapter 3.3. This helps to ensure that the components can be separated and recycled correctly by a specialist for disposal. For disposal of liquids and consumables such as heating transfer media, see supplementary data sheets of these chemicals! You have to follow valid regional and local laws concerning disposal.
  • Page 85 9 Shutdown, storage, transport and disposal Health and Safety Clearance Declaration concerning safety, potential hazards and safe disposal of waste. For the safety and health of our staff, laws and regulations regarding the handling of dangerous goods, occupational health and safety regulations, safety at work laws and regulations regarding safe disposal of waste, e.g.

  • Page 86: Spare Parts

    This chapter lists spare parts, accessories and options including their ordering information. Only order spare parts and consumables from BUCHI to maintain the warranty status and to assure best performance and reliability of the system and a ected components. Any modi cations to the spare parts used are only allowed with the prior written permission of the manufacturer.

  • Page 87: Re Ux Glass Con Gurations

    10 Spare parts 10.1 Re ux glass con gurations Re ux con gurations are available with three di erent types of coolers attached to a common base of distribution piece and condensate cooler. Basic R-220 Pro Operation Manual...

  • Page 88: R' Con Guration

    10 Spare parts 10.1.1 'R' con guration 003577 027338 037287 005155 041155 041151 041159 041156 041131 041076 041060 041348 041373 041228 000794 027277 041130 041162 005155 027289 041130 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15 041131 EasyClamp DN 40, cpl.

  • Page 89: Rb' Con Guration

    10 Spare parts 10.1.2 'RB' con guration 037287 003577 027338 005155 041120 027824 041151 041156 041131 041076 041060 041348 041373 041228 000794 027277 041130 041162 005155 027289 041130 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15 041120 Glass holder Bullfrog...

  • Page 90: C' Con Guration

    10 Spare parts 10.1.3 'C' con guration 025979 025124 025981 003577 041079 027338 005155 041151 041156 025978 041131 041076 041060 041348 041373 041228 000794 027277 041130 041162 005155 027289 041130 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15 041060...

  • Page 91: Basic' Con Guration

    10 Spare parts 10.1.4 'BASIC' con guration 003577 027338 037287 005155 041155 041151 041159 041156 041131 041060 11056021 11055596 041076 11055696 11056022 041228 027277 041130 005155 027289 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15 041131 EasyClamp DN 40, cpl.

  • Page 92: Decending Glass Con Gurations

    10 Spare parts 10.2 Decending glass con gurations Decending con gurations are available with ve di erent types of cooler setups attached to a common base of distribution piece and y-piece. D2 HP R-220 Pro Operation Manual...

  • Page 93: D' Con Guration

    10 Spare parts 10.2.1 'D' con guration 041076 027150 041131 041131 041155 041151 041156 001165 027308 041348 000794 041131 037287 041335 001129 041228 003577 027277 027338 005155 041131 11055588 005155 027289 041130 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15...

  • Page 94: D2 Hp' Con Guration

    10 Spare parts 10.2.2 'D2 HP' con guration 041076 041131 11060823 11060824 041155 041131 041151 001165 041156 027308 041131 001129 041335 041228 027277 041337 000794 041348 041131 005155 041130 027289 003577 027338 005155 Artikelliste Bestell-Nr. Bezeichnung Bestell-Nr. Bezeichnung 000794 Screw cap SVL15 041131 Easy Clamp DN40, cpl.

  • Page 95: D2' Con Guration

    10 Spare parts 10.2.3 'D2' con guration 041076 041131 027150 041131 041155 041151 001165 041156 041159 027308 041131 041348 000794 041335 041228 027277 041131 11055588 005155 041130 027289 003577 027338 005155 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15...

  • Page 96: Db' Con Guration

    10 Spare parts 10.2.4 'DB' con guration 041076 027825 027837 041131 041120 041151 001165 041156 041131 041348 000794 025435 041335 041228 027277 001129 041131 005155 11055588 027289 041130 003577 027338 005155 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15...

  • Page 97: Db2' Con Guration

    10 Spare parts 10.2.5 'DB2' con guration 041076 027837 041131 041120 041155 041151 041151 041156 041156 001165 027825 041159 041131 041348 041335 000794 041228 11055588 027277 041130 005155 027289 003577 027338 005155 List of articles Order no. Part name Order no. Part name 000794 Screw cap SVL 15...

  • Page 98: Receiving Vessel Parts

    10 Spare parts 10.3 Receiving vessel parts Interchangeable receiver (double) Part name Order no. Receiving ask 10 l plg 037569 Branching piece 1 plg 041048 Branching piece 2 plg 11055585 for con guration R, RB and C Branching piece 2 plg 041049 for con guration D, D2, DB and DB2 Outlet valve, DN 25/2...

  • Page 99: Miscellaneous Parts

    10 Spare parts Interchangeable receiver D2 HP Part name Order no. Receiving ask 10 l plg 037569 Branching piece plg 041048 Outlet valve, DN25/2 041061 Shut-o tap, small, cpl. 041062 EasyClamp, DN25 041130 Pivoting clamp, cpl. 041151 Base for ask 041252 T-piece DN25 041445...
  • Page 100 10 Spare parts Inlet valve, cpl. 041348 PTFE bellow 041388 Glass body 041346 041388 Set of 5 SVL 15 seals 041946 11061551 Screw cap SVL 15 003549 041346 Connetion, PTFE 041354 Screw cap SVL 30 003223 041946 Seal SVL 30×18 000398 Support ring inlet valve 041147...
  • Page 101 10 Spare parts Snap ange coupling, cpl. 041112 041112 Set of 5× O-ring 64 x 5.0 041229 041229 EasyClamp element, DN 70 041135 PTFE coated silicone gasket 11056381 for DN 25 (set of 5) Small glassware joint ∅~ 30 mm 11056381 R-220 Pro Operation Manual...
  • Page 102 10 Spare parts PTFE coated silicone gasket 11056382 for DN 40 (set of 5) Large glassware joint ∅~ 47 mm 11056382 6 L evaporating ask 027470 10 L evaporating ask 027469 20 L evaporating ask 027468 10 L evaporating ask, amber 11069604 20 L evaporating ask, amber 11069605...

  • Page 103: Optional Equipment And Upgrade Parts

    10 Spare parts 10.5 Optional equipment and upgrade parts For more information about the following parts go to www.buchi.com or contact your local BUCHI representative. Optional parts Part name Order no. Safety shield for D, D2, R and C for...
  • Page 104 10 Spare parts Blind cover for Interface I-300 Pro 11064152 Manual ask handler 041400 Foam detector 11056083 Cooling water temp. sensor 11055988 Cooling water valve 041191 R-220 Pro Operation Manual...
  • Page 105 10 Spare parts Cooling water ow sensor 11055971 Automatic sensor for R-220 Pro 11064486 Level sensor (pluggable) 11056192 Aeration valve 11055929 R-220 Pro Operation Manual...
  • Page 106 T +971 4 313 2860 T +52 55 9001 5386 F +66 2 862 08 54 F +971 4 313 2861 latinoamerica@buchi.com bacc@buchi.com middleeast@buchi.com www.buchi.com/es-es www.buchi.com/th-th www.buchi.com We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...

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