WARNING sample gas is toxic, flammable, or corrosive. Check the sample line and all connections for leaks before powering up. Consult plant safety personnel for appropriate exhaust venting guidelines for specific sample gas type. vi | 5910 UHP Moisture Analyzer...
Achtung - Heiße Oberfläche Environmental Information (WEEE) This AMETEK product contains materials that can be reclaimed and recycled. In some cases the product may contain materials known to be hazardous to the environment or human health. In order to prevent the release of harmful substances into the environment and to conserve our natural resources, AMETEK recommends that you arrange to recycle this product when it reaches its “end of life.”...
CAUTION The various configurations of the 5910 Moisture Analyzer should not produce, or fall victim to, electromagnetic disturbances as specified in the European Union’s EMC Directive. Strict compli- ance to the EMC Directive requires that certain installation techniques and wiring practices are used to prevent or minimize erratic behavior of the Analyzer or its electronic neighbors.
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SPECIAL WARNINGS AND INFORMATION For Use of this Equipment in Class 1, Division 2 Hazardous Locations This equipment is designed to meet requirements for Class I, Division 2, Groups ABCD, or Non- Hazaradous areas only. Explosion Hazard - Substitution of Components May Impair Suitability for Class I, Division 2. WARNING Risque d’explosion - La substitution de composants peut rendre ce materiel inaccept- able pour les emplacements de Classe I, Division 2.
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Failure to adhere to this warning will result in erroneous results and possible damage to the analyzer. Save the original packaging received with this analyzer. It is an ap- proved 4G container in which you can ship the 5910 analyzer with the purifier installed. WARNING Do not make or break the RS-232 connection unless the area is known to be non-hazardous.
European Standards Information Manufacturer’s Name: AMETEK Process Instruments (ISO 9001 Registered 1995) Manufacturer’s Address: Process & Analytical Instruments Division 455 Corporate Boulevard Newark, DE 19702 Phone: 302-456-4400 Fax: 302-456-4444 EU Representative Address: Dr. Jurgen Gassen AMETEK Precision Instruments Europe GmbH...
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Process photometric analyzers, process moisture analyzers, and sampling systems are warranted to perform the intended measurement, only in the event that the customer has supplied, and AMETEK has accepted, valid sample stream composition data, process conditions, and electrical area classification prior to order acknowledgment.
5910 MOISTURE ANALYZER Overview The Model 5910 Moisture Analyzer measures trace concentrations of moisture in ultra- high purity gases such as air, oxygen, hydrogen, helium, argon, neon, nitrogen, and xenon using a quartz crystal microbalance sensor. Calibrated range is 0 to 150 parts-per- billion by volume (PPBV) with a trend indication for measured concentrations above the calibrated range.
One RS-232 or one RS-485 serial interface provide communication be- tween the analyzer and your recording or data acquisition equipment. The 5910 analyzer is configured, and analyzer parameters are set, by using either the analyzer display, keypad and function keys, or using an external PC.
Gas Flow Controlling the gas flow rate The 5910 Moisture Analyzer gas flow is controlled by a mass flow controller and a pres- sure regulator/orifice. The mass flow controller is located in the reference gas leg of the sample system. A microprocessor reads the total gas flow at the exhaust and adjusts the pressure regulator to maintain a constant total flow.
M a ss F lo w C o n tro lle r Reference Gas Flow. M F M = M a ss F lo w M e te r E xh a u st Figure 1-2. Flow during reference cycle. 1-4 | 5910 Moisture Analyzer...
Sample gas measurement (Figure 1-3) The sample gas enters the analyzer through the gas inlet and flows through the first dia- phragm valve (DV1). The flow then splits. One half of the sample gas continues through the “sample” leg. It passes through the pressure regulator which is computer-controlled.
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M a s s F lo w C o n tro lle r M F M = M a s s F lo w M e te r Sample Gas Flow Sample Gas Flow. E x h a u s t Figure 1-4. Zero reference gas flow. 1-6 | 5910 Moisture Analyzer...
∆ ƒ values until the next zero cycle. AMETEK recommends performing a zero every 24 hours for the first month of opera- tion. After this start-up period, the analyzer will have dried down sufficiently to NOTE increase the zeroing interval to 1 week.
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5900 analyzers is estimated to reach 10% (i.e., a 2 PPBV change at 20 PPBV) after 45 months of service. Even though the QCM-based moisture analyzers are extremely stable, AMETEK recom- mends that you check the calibration of the analyzer every three years. This performance check should be handled as part of the normal maintenance schedule for the equipment.
SPECIFICATIONS All specifications subject to change without notice. NOTE Compatible Gases Air, helium, argon, neon, hydrogen, oxygen, nitrogen, and xenon are compatible gases. Contact the factory to confirm compatibility with other gases. Read the Gas Compatibility Warning in the “Special Warnings and Information” sec- tion at the beginning of this manual for more information.
INSTALLATION AND START-UP Read this entire chapter before installing the 5910 analyzer. Failure to do so may impair protection against fire, electric shock and injury originally provided by this WARNING equipment. Do not use this analyzer in a manner not specified in this manual.
Analyzer Requirements Space Requirements The 5910 Moisture Analyzer requires an area 48 cm wide x 17.7 cm high x 50.9 cm deep (19” x 7” x 20”) plus clearance for analyzer connections and proper ventilation (Figure 3-1). It should be located as close to the sample tap as possible.
Indoor use only, IEC 529; IP40 Electrical Requirements The 5910 Moisture Analyzer can be installed in a general purpose area or NEC/CEC Class I, Division 2 hazardous area. It does not have an On/Off power switch so power must be applied though a circuit breaker switch at the AC source.
Refer to the “Special Warnings and Information” section in the beginning of this manual for information on sample gas compatibility. CAUTION RS-232 and RS-485 Connections (item 4 in Figure 3-2)- Do not Connect or Discon- nect when energized. WARNING 3-4 | 5910 Moisture Analyzer...
Op imal results are obtained with the sample line maintained at 60 °C. - Recommended sample gas input tubing is 1/4 inch OD, electropolished 316L VAR stainless steel (AMETEK #257707002 or equivalent). Exhaust pressure must be atmospheric. •...
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Serial wiring supplied by user. Analog Output 4-20 mA output to user recording equip- ment. Wiring supplied by user. Alarm Contacts Connections for: Data Valid, Concentra- tion Alarm and System Alarm. Wiring supplied by user. 3-6 | 5910 Moisture Analyzer...
Alarm & Alert Contacts Analog Output Figure 3-3. 5910 moisture analyzer interface board. Gas Connections (Figure 3-4) Install a main process shut-off valve and pressure regulator (recommended) at the sample tap. Locate the analyzer as close as possible to the sample source.
AMETEK service. Voltage selection The 5910 analyzer comes from the factory set to operate on 115 VAC. If you must switch the setting to 230 VAC (or back to the 115 VAC setting), follow the procedure below.
Power installation Your analyzer’s power cord must be terminated with an approved, grounded, male locking plug as per the NEC 501-3(b)6 or CEC 18-172, 174 (i.e. twist lock). This is the only power input configuration that complies with NEC and CEC regulations for use of a flex- ible mains power cord connection in Class 1, Division 2 hazardous locations.
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NEC 501-3(b). • The disconnect device must be close enough to the analyzer so the operator can reach it easily. • The disconnect device must be clearly marked as the power discon- nect for the analyzer. 3-10 | 5910 Moisture Analyzer...
LINE VOLTAGE RS-485 TERMINATOR FUSE ANALOG OUTPUT DATA CONC SYSTEM POWER VALID ALARM ALARM CONNECTOR Figure 3-6. 13 14 1 (L) (LINE) Remove 1 (L) and 2 (N) (NEUTRAL) 2 (N). Communication connections (Figure 3-8) Remove terminal cover. Connect the 4-to-20 mA analog output (13) and alarm and data valid terminals (14) on the interface board to the analyzer through the me- tallic signal conduit (2) (Figure 3-2) as per NEC 501-4b for hazardous locations.
Consult your safety specialist. WARNING Analyzer Set-Up Overview of Keypad The Model 5910 Moisture Analyzer keypad (Figure 3-10) is used to access menus and sub-menus and system values for the function keys, and to set-up your analyzer param- eters. Function keys Press one of the four function keys to access the main menu for that category as well as sub-menus and system values.
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Alarm & Alert Contacts Analog Output Figure 3-8. Communication connections on the 5910 analyzer interface board. To highlight an item, scroll through the menu items until the small arrowheads point to your choice as shown in Figure 3-11. Up and down arrow symbols displayed on the right-hand side of the screen indicate that there are more menu items above or below the currently displayed items.
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100 to 500 ohms Figure 3-10a. Self-powered 4-20 mA output connections. Meter 100 to 500 ohms Supply 24 Volts Figure 3-10b. Externally powered Meter 4-20 mA output connections. 3-14 | 5910 Moisture Analyzer...
Overview of Display The default display has four lines (Figure 3-12): Zero Alarm FUNCTION Range KEYS Figure 3-11. 5910 analyzer keypad. Config Cancel Enter Line 1 Sample concentration • Line 2 Status message • Line 3 Alarm message • Line 4 Alarm Value •...
You are ready to do an initial zero cycle. Procedure for speeding up the dry down period To decrease the time required to dry down the 5910 analyzer, follow this procedure: Make all gas connections and apply power to the analyzer. Allow the analyzer to warm up and run with the factory-default settings for a period of 6 to 12 hours.
At the end of this interval, set as follows: Zero Schedule Type to “Daily” 5.7 ppb Sampling . . . High Concentration 5.0 ppb Limit Figure 3-14. Default normal operation screen. Values are for example only. Zero Duration to 288 cycles (i.e., 12 hours) Zero Hour to 1 The exact menu location for each of these parameters can be found by referring to the Menu Map at the beginning of Chapter 4.
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The 5910 analyzer requires time to fully recover to normal operation after zeroing. During the recovery period, “Equilibrating” will be shown on line two of the display.
USER INTERFACE The user interface consists of the display screen on the front of the 5910 Moisture Ana- lyzer and the keypad. Using a combination of the function keys and the number, minus sign and decimal point, you can set the parameters for your analyzer.
Test Display Cancel Press Key Test Keypad Open Contacts Test Alarms Close Contacts Figure 4-2. 4 mA Output Menu map for 5910 Test Analog 12 mA Output 20 mA Output Moisture Analyzer. Test Serial Start Cancel 4-2 | 5910 Moisture Analyzer...
Zero Key Use the Zero Key to define on-demand zero settings. ZERO Hold Outputs Enable Disable Adjust Offset Enable Disable Start Zero Figure 4-3. Main menu for the Zero key. Quit Zero Hold Outputs Enable Select this function to hold the output at the last valid reading during a zero.
Main menu for Alarm key. High Limit Enter the high limit value in PPBV. Low Limit Enter the low limit value in PPBV. Enable Alarm Select “enable” or “disable” to activate the moisture concentration alarm relay. 4-4 | 5910 Moisture Analyzer...
Range Key Use the Range Key to define your 4-to-20 mA output setting. RANGE Maximum Conc Enter Value Minimum Conc Enter Value Figure 4-5. Main menu for Range key. Use this setting to scale the 4-to-20 mA output. The 4-to-20 mA output is proportional to the moisture concentration.
Select “on” or “off.” The default is ON. Enter Value Contrast 1 to 9 Font Back Light This is a factory-set parameter that identi- fies the type used for the display on Enter Value Font 0 or 1 the analyzer. 4-6 | 5910 Moisture Analyzer...
Communication Select communication setup. Node Address Enter the address for RS485 serial communications Config ( 0 - 240). Address 240 is reserved (see the “Special Addresses” section in Chapter 5 for details). Communication Baud Rate Node Enter Address Address Select the baud rate at which you transfer data (9600 or 19200).
Wednesday Month Enter Value Thursday Enter the 2-digit value for the month. Friday Saturday Hour Enter Value Hour Enter the value using the 24-hour Minute Enter Value clock. Minute Enter the 2-digit value for minutes. 4-8 | 5910 Moisture Analyzer...
Enter the zero period value in cycles. Duration One cycle is 2.5 minutes. AMETEK recommends performing a zero every 24 hours for the first month of opera- tion. After this start-up period, the analyzer will have dried down sufficiently to NOTE increase the zeroing interval to 1 week.
Test Analog Output Tests the analog output by allowing the user to set outputs to 4, 12 or 20 mA. Test Serial Communications Performs a “loop back” test and reports the result to the display. 4-10 | 5910 Moisture Analyzer...
SERIAL COMMUNICATIONS Protocol The protocol used for the 5910 Moisture Analyzer is a master/slave, command/response communication with the master initiating all transfers. The message format for transfers initiated by the master is seen in Figure 5-1. End Flag Node Address Data Figure 5-1.
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End Flag Figure 5-3. Message format for slave acknowledge. Response Code The message format for slave failure response is seen in Figure 5-4. End Flag Figure 5-4. Slave failure response format. Command Code Error Code 5-2 | 5910 Moisture Analyzer...
Special Addresses Addresses $F0 through $FF are reserved for special functions with address $F0 used as a broadcast address. Address $F0 Node address $F0 is used as a single point address, i.e. it is intended for use in configura- tions with a single slave. The slave will respond to all messages with node address $F0. You must be careful to prevent multiple slaves from receiving commands with the broad- cast address as this will cause a bus contention.
5-7b for a list of defined handles for system variables. Note that each system variable will have an associated format. This format can be read via the Data Format command (J). Example Master: >34F0512[CR] Slave: A1234540[CR] 5-4 | 5910 Moisture Analyzer...
Write Data (H) The data field of this frame contains the handle for a system variable. See Figures 5-7a and 5-7b for a list of defined handles for system variables. Note that each system variable will have an associated format. This format can be read via the Data Format command (J).
All failure responses consist of an ASCII ‘N’ followed by a two byte hexadecimal ASCII failure code. Defined failure codes are given in the table below. Example: Slave: N01[CR] Failure Code Description Unknown Command Byte Check Sum Parameter Out of Range Figure 5-6. Defined Failure Codes. 5-6 | 5910 Moisture Analyzer...
Hold current outputs during zero cycle Integer 1(hold) EnableAlarm1 Enable or disable concentration alarm Integer 1(enable) ModelName Analyzer model name String[16] AMETEK 5910 UHP DryerDateCode Dryer production code String[10] 010080009 DryerPpbHours Dryer consumption in 1000 of ppB hours Float 200000.00 CurrentPpbHours...
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Reference frequency reading Float 1156 Hz WeekDay Analyzer date parameter Integer MoistureSpan Concentration coefficient Float 1.00 ZeroCycleCount Zero cycles count down counter Integer EquilCycles Equilibration cycles counter Integer FrequencyOffset Zero correction coefficient Float Figure 5-7b. Variable Table. 5-8 | 5910 Moisture Analyzer...
TROUBLESHOOTING Alarms Following is a table of alarm messages (Figure 6-1) for the AMETEK 5910 Moisture Ana- lyzer. If there is a problem, the alarm will appear on the LCD screen on the third and fourth line. Figure 6-1. Alarm message table.
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CAUTION Mass Flow Controller The Mass Flow Controller (MFC) (AMETEK Part # 271115001) is located below the Mass Flow Meter (MFM). Both are attached to the controller mounting bracket. See Figure 7-1. Removing the mass flow controller Follow these instructions to remove the mass flow controller from the 5910 analyzer.
Attach the mounting bracket to the mounting plate using the two (2) kep nuts (Figure 7-1). Do not tighten all the way so that there is some leeway of movement when following the next step. 7-2 | 5910 Moisture Analyzer...
Attach the MFC cable to the analog board at position P3. Mass Flow Meter The Mass Flow Meter (MFM) (AMETEK Part # 271189001) is attached to the controller mounting bracket above the Mass Flow Controller (MFC). See Figure 7-1. Removing the mass flow meter Follow these instructions to remove the mass flow meter from the 5910 analyzer.
(AMETEK Part # 591016901) and REF for the reference solenoid valve assembly (AMETEK Part # 591092901). They are connected by wire to the PCB board at the location marked on the side of the valve wire connector.
The pressure regulator assembly is located attached to the assembly bracket behind the inlet valve assembly. The bracket is attached to the mounting plate for the sampling sys- tem. Removing the pressure regulator Follow these instructions to remove the pressure regulator assembly from the 5910 ana- lyzer. Service and Parts...
Do not tighten all the way. Attach the valves and tubing to the VCR ports on the pressure regula- tor assembly. Use a fresh VCR gasket on the inlet side and an orifice 7-6 | 5910 Moisture Analyzer...
Towards Inlet assembly. Diaphragm Valve The diaphragm valve (AMETEK Part # 271221001) is located next to the pressure regu- lator on the inlet side of the sampling system. It is attached to the mounting plate using the diaphragm valve mounting bracket.
Purifiers The gas purifiers are located at the rear of the 5910 analyzer above the sample inlet valve, and on the side (Figure 7-9). They are held in place with 1/4” VCR nuts.
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Hex Screws Hex Screws Hex Screws Hex Screws Diaphragm Diaphragm Valve Valve Mounting Mounting Bracket Bracket Elbow Elbow Elbow Figure 7-8. Diaphragm valve assembly. Accessing the purifier locations Remove the top cover of the analyzer by removing the 2 screws on the side and the 4 screws on the top.
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Installing the purifiers Figure 7-9. Purifiers and VCR nuts. Read the Gas Compatibility Warning in the beginning of this manual under “Special Warnings and Information” section before removing or installing the CAUTION purifier. 7-10 | 5910 Moisture Analyzer...
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Check to make sure that you have two purifiers ready to install. You should also have 2 VCR gaskets for each purifier. The purifiers will be marked as either inert gas or oxygen purifiers and will have an arrow to indicate the correct positioning in the analyzer based on the gas flow.
Board Connections Analog Board Sensor LCD Display Front Panel DC Power System Alarm (Single) (Dual) Figure 7-9. Analog board connections. Thermistor Sensor LCD Display Front Panel Single Fan and Dual Fan DC Power System Alarm 7-12 | 5910 Moisture Analyzer...
User Interface Board Heater Wire 120 Volt System RS-485 Alarm Figure 7-10. Circuit Side User Interface board connections. Component side and circuit side. Heater Wire 120-Volt RS-485 System Alarm Service and Parts 7-13...
RS-485 Figure 7-11. MCU board connections. Reference Valve P3-1 Sample Valve P3-3 RS-485 P3-1 Reference Valve P3-3 Sample Valve RS-232 Stepper Motor Board Motor DC Power Figure 7-12. Stepper Motor board connections. DC Power Motor 7-14 | 5910 Moisture Analyzer...
Purifier (H , Inerts and Oxygen) 272603001 Assembly FRU Electronic Enclosure Fan 5910/5920 591069901 Stepper Motor Board 591053901 Stepper Motor Assembly 591087901 RS-232 Connector Cover Assembly 591277901 * May require retrofit kit - contact AMETEK Service. Service and Parts 7-15...
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Follow the instructions on the subsequent screens to complete the installation. When you get to the Setup Complete screen, click Finish to complete the installation. The default location for the 5910 software is in the AMETEK, Inc. folder. ...
Click the Setup button to configure PC Communications. The Serial Port Communica- tion screen opens (Figure A-2). Port Select the COM port on your computer where the connec- tion to the analyzer is installed. Figure A-2. PC Serial Communications setup screen. A-2 | 5910 Moisture Analyzer...
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Baud Rate Select the baud rate at which data will be transferred. RS-232 Port Click if the analyzer is connected to an RS-232 port. RS-485 Port Click if the analyzer is connected to an RS-485 port. Address Type the network address to which the analyzer is con- nected.
For initial setup of PC communication parameters, use the Setup button on the Gen- eral tab. NOTE Configuring Multiple Analyzers Use the Device Communications tab to set the analyzer’s communication parameters to agree with the PC settings when controlling analyzers in a daisy chain. A-4 | 5910 Moisture Analyzer...
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Changing Communication Parameters • Change the ANALYZER parameter(s) first. • Click Apply to confirm the change. This may cause the analyzer to go off-line. • Change the PC settings or physical wires/cables. • Reset the analyzer by recycling power. Figure A-3. Device Communications setup screen.
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Check this box to enable the concentration alarm. High Limit Enter the high limit for the concentration alarm. Low Limit Enter the low limit for the concentration alarm. To Save settings on the Setup tab, click Apply. A-6 | 5910 Moisture Analyzer...
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Schedule Tab Use the Schedule tab to schedule routine Zero. Figure A-5. Schedule tab. Abort Button Click to terminate verification or zero. Zero Now Button Click to begin zero cycle now. Adjust Offset check box Checked The analyzer performs an offset adjustment at the end of the zero cycle.
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Saving Your Settings To save settings on the Schedule tab, click Apply. To save settings and exit the program, click Apply+Exit. To abort changes you have made, click Cancel+Exit. This will close the Configurator software program. A-8 | 5910 Moisture Analyzer...
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Status Tab Use the Status tab to view current readings and the status of the analyzer. Figure A-6. Status tab. Upload Data Click Upload Data to save data from the analyzer to a file. The Save As screen opens so that you can browse to where you want to save the file.
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Rate The preferred data collection rate is “0.5” minutes and is set as the default. A record is created every 30 seconds. The collection rate can be increased to one minute or more. A-10 | 5910 Moisture Analyzer...
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QUICK REFERENCE CARD Reference Chapter 3 of the 5910 Moisture Analyzer manual. INSTALLATION AND START-UP Incoming sample temperature 0 °C and 100 °C Optimum input gas temperature 60 °C ± 5 °C ANALYZER PARAMETERS Minimum input pressure 20 PSIG Zero Key:...