IKA C 200 Operating Instructions Manual
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IKA C 200 Operating Instructions Manual

IKA C 200 Operating Instructions Manual

Calorimeter system
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20000008742
C200_012016
Calorimeter System C 200
Operating instructions
EN

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Summary of Contents for IKA C 200

  • Page 1 20000008742 C200_012016 Calorimeter System C 200 Operating instructions...

  • Page 3: Table Of Contents

    Transport, storage, place of installation Conditions of transport and storage Place of installation Unpacking Delivery scope Installations and starting up Calorimeter C 200 Installation Switchin on the system Display and operating elements Configuring the system System settings Filling the calorimeter for the first time...
  • Page 4 Service menue Operation Description of service menue options Cleaning and maintenance Inner vessel filter Filler Micro filter Maintaining the water circulation Decomposition vessels Cleaning informations - Accessories and consumables ® Accessories Consumables Technical data...

  • Page 5: Declaration Of Conformity

    Declaration of conformity KONFORMITÄTSERKLÄRUNG Wir erklären in alleiniger Verantwortung, dass dieses Produkt den Bestimmungen der Richtlinien 2014/35/EU, 2014/68/EU, 2014/30/EU und 2011/65/EU entspricht und mit den folgenden Normen und normative Dokumenten über- einstimmt: EN 61010-1, EN 61010-2 und EN 61326-1. DECLARATION OF CONFIRMITY We declare under our sole responsibility that this product corresponds to the regulations 2014/35/EU, 2014/68/EU, 2014/30/EU and 2011/65/EU and conforms with the standards or standardized documents: N 61010-1, EN 61010-2 and EN 61326-1.

  • Page 6: Safety Instructions

    The of the medium to be processed. following materials, for example, could pose a • Calorimeter system C 200 may only be used to risk: determine the calorific value of solid and fluid – corrosive materials.
  • Page 7 Experiment autoclaves must be of the test activity, operated in special chambers (C 2000, C 5000, C 7000, C 200). 4. who has suitable test equipment if necessary, • The decomposition vessels must undergo re- 5. who can provide appropriate proof of the re- peated tests (internal tests and pressure tests) quirements listed in 1.

  • Page 8: User Information

    Numbers , ,  etc. indicate guidelines in the following sections which must always be carried out in order. 2.2 Warranty and liability Please read these operating instructions carefully. You have purchased an original IKA product, ® ® - WERKE only consider themselves to be...

  • Page 9: Transport, Storage, Place Of Installation

    • In the case of any damage a report must be sent immediately (post, rail or forwarder) 3.4 Delivery scope 1 x Basic device C 200 1 x Power cable 1 x Decomposition vessel C 5010 1 x Operating instructions...

  • Page 10: Installations And Starting Up

    Installation and starting up 4.1 Calorimeter C 200  Measuring cell cover  Tank fillers  Display  Keyboard  Fill level display 4.2 Installation All the connections for draining as well as the pe- ripherals are on the back of the appliance.
  • Page 11  Connecting the water drain  Inner vessel emergency drain  Tank drain  Inner vessel drain Insert the emptying hose (included in package If you use a thermostat to fill the tank, you can contents) into plug-in coupling . Place this in also hang the drain hose in the thermostat.

  • Page 12: Switchin On The System

     Delete button: this key is used to delete the 4.3 Switching on the system last character entered. Switch the calorimeter on at ON/OFF switch  (back of appliance). The appliance is now in Display elements in menu mode: standby mode. If you press the Menu (F3) key, a menu will ap- pear in the display which allows you to enter set- tings.

  • Page 13: Configuring The System

    Set date  Menu header: shows the name of the submenu and the cur- rently selected menu line of the total number of menu lines (for example, 2/5: you are in the se- cond of five lines). There are three different menu lines ,  and : ...

  • Page 14: System Settings

    MENU (F3)  UP/DOWN (F2) to "General"  OK (F1)  Enter the calorific value in the format xxxxx (default: 26460)  OK (F1)  BACK (F3) Calibration values Once you have calibrated the appliance, you will MENU (F3) need to enter the calculated C-values (calibration ...

  • Page 15: Filling The Calorimeter For The First Time

    Time control MENU (F3) Calorimeter C 200 performs the measurement  UP/DOWN (F2) to "Unit" automatically according to a set period of time  OK (F1) and calculates the provisional result. The measu-  UP/DOWN (F2) select the desired unit ring time is set at 14 minutes.

  • Page 16: Switchin Off The System

    4.10 Oxygen station C 248 4.8 Switching off the system The C 200 does not have an integrated oxygen Standby mode filling point for the decomposition vessel. You In order to switch off the calorimeter system, the can use oxygen station C 248 for filling. The C start screen must be displayed.

  • Page 17: Calorimetric Measurements

    Calorimetric measurements In many cases, however, not just the combus- 5.1 Determining the calorific value tion products referred to in the standards are produced. In such cases the fuel sample and the Combustion is carried out in a calorimeter under combustion products must be analysed to pro- specific conditions.

  • Page 18: Information About The Sample

    The cleanliness of the material used in the com- als) can often only be fully combusted using IKA bustible crucible prevents chemical contaminati- ® acetobutyrate capsules C 10, IKA combustion on of the sample (no blank values).

  • Page 19: Calibration

    5.4 Calibration The calorimeter system must be calibrated before The system must be calibrated in every work accurate measurements are possible. This is done mode used. by combusting tablets made of certified benzoic acid (see Accessories) with a known calorific va- If a calorimeter is operated with several de- lue.

  • Page 20: Preparing The Decomposition Vessel

    6.2 Preparing the decomposition vessel Prepare the decomposition vessel as follows:  Cover  Union nut  Handle  Cotton thread  Unscrew the union nut and remove the cover using the handle.  Attach a cotton thread to the centre of the ignition wire using a loop.

  • Page 21: Preparing The Measurement

     Selecting MEASUREMENT (F2) will take you to the "Prepare measurement" menu.  Place the decomposition vessel into the inner vessel of calorimeter C 200. The decomposition vessel must be placed between the three locating bolts.  Enter the noted weighted sample in the marked "Einwaage"...

  • Page 22: Performing The Measurement

    QEXTERNAL2 Correction value for the heat energy from other burning aids e. g. combustible crucible). The de- fault value is 0. TESTNO For each measurement the software automati- cally assigns a number in the form of yymmddnn, with jj representing the year, mm the month, dd the day and nn a consecutive number.

  • Page 23: Cleaning The Decomposition Vessel

     a) The measurement process is fully automatic for automatic measuring procedures (isoperibol, dynamic and time-controlled, see section 4.6). The result will appear once the measuring pro- cess is complete.  After the measurement open the cover to au- tomatically empty the inner vessel. Remove the decomposition vessel and the ignition adaptor.

  • Page 24: Errors In The Measuring Procedure

    (see section 7.2 ”ReInit”). If this does not work, increase is not reached within one minute of ig- switch the appliance off and then back on again. nition (0.05 K). If this does not work either, please contact IKA ® Service.
  • Page 25 (see section 7.2 There is no magnetic rod in the inner vessel or ”Pump”) and check water jet in tank. If there is no the magnetic rod is outside of the magnetic field. water flow, please contact IKA -Service. ® User action:...

  • Page 26: Service Menue

    Meldung: Service menu Füllzeit überschritten 7.1 Operation This menu allows you to directly control and test Please note that you must stop every started ac- various actions and statuses of the calorimeter tion. without performing a measurement. There are also menu items which can be used to start up Exceptions: and shut down the appliance.

  • Page 27: Cleaning And Maintenance

    Pump Reset Switch the pump on with this menu item. The This menu item allows you to restore the default outer vessel will be filled and rinsed (see also sec- settings. tion 4.7). Reinit Requirement: This menu item allows you to reinitialise the Check that there is water in the tank.

  • Page 28: Maintaining The Water Circulation

    In the case of discontinuous use with tap water (single measurements with long gaps) a stabiliser must be added to the water circulation to prevent the formation of algae. Add approx. 4 ml IKA -Aqua-Pro C 5003.1 to the ® tank (see Accessories).

  • Page 29: Ika - Accessories And Consumables

    IKA ® or can - Before using a cleaning or decontamination download a version for printing from the IKA ® method other than that recommended by the website at www.ika.com. manufacturer, check with the manufacturer that...

  • Page 30: Technical Data

    Technical data Table power supply (external): Rated voltage 100 - 240 V AC Frequency 50 / 60 Input power max. Calorimeter: Rated voltage 24 V DC 5A Input power max. Fuses (internal) 1x 2,5 AT Perm. on-time Continuous operation Protection class as per DIN EN 60 529 IP 20 Protection class Overvoltage category...
  • Page 32 - Werke GmbH & Co.KG ® Janke & Kunkel-Str. 10 D-79219 Staufen Tel. +49 7633 831-0 Fax +49 7633 831-98 sales@ika.de www.ika.com 3548801b...

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