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Summary of Contents for IKA C 6000 global standards
- Page 1 20000016667 C 6000_112018 IKA C 6000 global standards IKA C 6000 isoperibol Operating instructions Source language: German...
- Page 3 Device setup Front Lift RFID sensor field for decomposition vessel detection Decomposition vessel Touch screen 4a: Interface for USB (stick and printer) Mains switch Fig. 1 Back Interfaces for PC communication (Balance/Ethernet/ USB/Sample Rack) Water filter Main fuses Mains socket 10: Condenser/thermostat inlet (IN) 11: Condenser/thermostat outlet (OUT) 12: Discharge hose (EMPTY)
- Page 4 Dangerous spots Fig. 4...
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Page 5: Table Of Contents
Content Page 1 Declaration of conformity 2 Warranty 3 Warning symbols 4 Safety instructions 5 Correct use 5.1 Use 5.2 Area of use 5.3 Recommended method of operation in working mode 6 Useful information 6.1 Determining the calorific value 6.2 Corrections 6.2.1 Acid correction 6.3 Note on the sample 6.4 Complete combustion... -
Page 6: Declaration Of Conformity
2006/42/EC, 2014/30/EU and 2011/65/EU and conforms with the following standards or normative documents: EN 61010-1, EN 61010- 2-051 and EN 61326-1. 2 Warranty In accordance with IKA warranty conditions, the warranty period The warranty does not cover worn out parts, nor does it is 24 months. For claims under the warranty please contact your apply to faults resulting from improper use, insufficient care local dealer. -
Page 7: Safety Instructions
• The IKA C 6000 global standards/isoperibol calorimeter sys- tem may be used only in conjunction with the decomposition Do not use oil or grease! vessels C 6010 or C 6012 (Chapter 15 Technical data). - Page 8 • Contact the IKA Maintenance Department to perform the We recommend that you send the pressure test. Comply with the safety instructions in this NOTE pressure vessel to our factory for respect.
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Page 9: Correct Use
5 Correct use 5.1 Use The IKA C 6000 global standards/isoperibol calorimeter system is The calorific value of the sample can then be calculated from the used for calorific value determination of solid and liquid substances. resulting increase in temperature, the sample mass and the known This is done by placing a known quantity of a substance in a thermal capacity of the overall system. -
Page 10: Useful Information
6 Useful information The decomposition vessel C 6010/C 6012 is manufactured in 33 MPa and a leakage test with oxygen at 3 MPa. Some materials accordance with the directive for pressure equipment tend to explode when combusted (e.g. due to formation of 2014/68/EU. -
Page 11: Acid Correction
QExtern2. You should keep the with a water trap. amount of burning aid used to a minimum. The IKA C 6000 global standards/isoperibol calorimeter system is a high-precision measuring instrument used for routinely determining the calorific value of solid and liquid substances. -
Page 12: Complete Combustion
For more detailed information on calibration, please see the the calorimeter system is calibrated after initial start-up, after relevant standards. If the IKA C 6000 global standards/isoperibol is operated with several decomposition vessels, you will need to maintenance work, after parts are replaced and at specified time determine the heat capacity of the system for each decomposition intervals. -
Page 13: System Properties
Operation without cooling unit: Connects to tap with pressure • Includes printer connection (USB, network, RS 232 (Fig. 2, 6)) reducer IKA C 25; temperature range 12 °C - 20 °C; water • USB drive connection (Fig. 1, 4a) consumption per measurement approx. 4 L; max. pressure 1 bar to 1.5 bar (Chapter 15 Technical data). -
Page 14: Setting Up And Assembly
4-5 L of water). This improves the usable life of the water. Make sure the filter casing is always securely closed. IKA recommends that you use the system with the recirculating condenser RC 2 at a speed of 2800 1/min (place of installation... -
Page 15: Water Supply Line
Follow the instructions in Chapter NOTE “11.3 Modules”. The pressure control valve IKA C 25 must be on the tap for the calorimeter to be operated and it is preset to a output pressure of approx. 1.5 bar. The valve is fitted inthe line to the water connection. -
Page 16: Peripheral Devices
8.2.6 Peripheral devices The peripheral devices and the WARNING calorimeter must be switched off when they are connected. PC RS232 Baud rate: 9600 Data bits: Stop bits: Parity: none Handshake: none Balance RS232 Serial connection for a balance interface (Mettler, Ohaus, Sartorius, Kern). For further information, see Chapter “11.3.1 Balance”. -
Page 17: Operator Panel And Display
9 Operator panel and display • The menu option selected has a blue background in the • Inactive symbols have a grey background. display. • When using a keyboard the input field has a yellow background. 9.1 Explanation of the display Symbol Function Change the working mode (Different working... -
Page 18: Commissioning
10 Commissioning 10.1 Switching on After the IKA C 6000 global NOTE standards/isoperibol calorimeter has been switched on, the display is active and can be operated using a stylus or finger. The cover opens automatically. While the software is loading, the information screen is displayed for about 30 seconds. -
Page 19: Menu Structure
10.4 Menu structure Factory settings Measurements Edit measurement Open......................Delete......................Modify......................Print....................... Export......................Evaluate......................Unselect......................Multiple selection on/off................. Simulation...................... Meas. <-> calib....................New measurement............................. Start measurement............................ Vessel Edit vessel Delete......................Modify......................Open calibration Select calibrations..........Edit calibrations Statistics...... -
Page 20: Menu Details, Main Menu
10.5 Menu details, main menu You can reach individual menu NOTE items by moving horizontally. Progress bar (Item A) Press on the progress bar to display the data about the current measurement or data about the last measurement (Chapter 11.6.3 Opening a completed measurement). Item C Item D Explanation... -
Page 21: Operation
11 Operation 11.1 Procedure Follow the operating instructions As a rule the weighted sample must be selected in such a NOTE for the decomposition vessel way that the temperature increase during the measurement C 6010/C 6012. is below 5 K and comes close to the temperature increase of the calibration (max. -
Page 22: Calibration
11.2.3 Calibration The decomposition vessel must be calibrated to carry out a measurement. The C-value of the decomposition vessel can be determined using calibrations. Go to the “Decomposition vessel” menu. To edit, select a decomposition vessel from the list and press Select “Open calibration”. -
Page 23: Balance
“TARE” key needs to be pressed. If a balance is connected to the IKA C 6000 global standards/ isoperibol calorimeter, the weighted sample can be sent directly from the balance to the IKA C 6000 global standards/isoperibol calorimeter. -
Page 24: Sample Rack
11.3.2 Sample rack Changing the assignment of the CAUTION sample rack whilst the IKA C 6000 global standards/isoperibol calori- meter is switched off is not permitted! You can prepare and run as you NOTE wish a maximum of 12 measure- ments in the sample rack. -
Page 25: Printer
Other print operations are not NOTE possible with this. We recommend the IKA C 1.50 printer with serial settings 9600-8-N-1. A serial printer can be connected to PC port of the C 6000. This printer prints the sequential record of the measurements. -
Page 26: Settings
11.4 Settings Menu Function in the submenu Measurement settings Measurement and procedure settings Ignition and combus- Manage ignition and combustion aids tion aids Units Set unit to be used Reference combustion Set reference combustion value value User Manage user Evaluation standard Set evaluation standard to be used Date/time Set date and time... -
Page 27: Creating Ignition And Combustion Aids
Select an external “External energies” list. Press to create a new ignition and combustion aid. The default factory setting “IKA cotton wool thread” is preset as standard with 50 J and cannot be edited or deleted. Enter a unique name (max. 30 characters). -
Page 28: Creating Users
11.4.5 Creating users Users created NOTE administered. Users that have been created can be selected from a drop-down list when a new measurement is created (Chapter 11.5.1 Creating a measurement). Go to the menu “Settings, User overview”. Press to create a new user. Enter a unique name (max. -
Page 29: Audio Settings
11.4.9 Audio settings notification sound before NOTE ignition cannot be deactivated. Go to the menu “Audio settings”. Select: - activate key tones - change the system volume (“+” louder, “-” quieter) (test current volume setting) Save the inputs. 11.5 Carrying out a measurement 11.5.1 Creating a measurement Go to the “Measurement”... -
Page 30: Simulation
11.5.3 Simulation If a simulation is carried out with an existing measurement the values of the measurement are automatically entered in the simulation input form. Go to the “Measurement” menu. To edit, select the measurement from the list and press Select the simulation. -
Page 31: Measurement Procedure
11.5.5 Measurement procedure Graph view Item Function Displays the current phase of the measurement Displays information about the selected measurement (name, sample weight, name of the decomposition vessel, C-value of the decomposition vessel) Progress bar for the current measurement Cancel button to end the current measurement Graph view shows the duration of the experiment and the temperature over time Graph view... -
Page 32: Opening A Completed Measurement
Carry out software update software Update Carry out firmware update firmware Factory The device will is reset to delivery state. settings You can update your device using a USB drive (Fig. 1, 4a). For more information on the procedure see: https://www.ika.com/fut... -
Page 33: Maintenance Programs
11.7.1 Maintenance programs You can select several programs. NOTE Ticking the box activates the menu item. Programs that are running are shown in blue. Programs shown grey inactive. Go to the “Maintenance, Maintenance programs” menu. Select the “Submenu” symbol. Select one or more programs. Item Function Go back to the menu using the arrow button. -
Page 34: Information
For this purpose request the form “Certificate of compliance” Food Water containing detergent from IKA, or download and print the form from the IKA website Fuels Water containing detergent www.ika.com. If your appliance requires repair, return it in its original packaging. -
Page 35: Emptying Water
12.1.3 Emptying water The system messages guide you NOTE through the emptying process. Please observe the chapters “De- vice configuration”, “7.3 Scope of delivery” and “8 Installation and assembly”. Go to the “Maintenance” menu. Select “Empty device”. Preparation: Switch off the condenser. Disconnect the hoses from the device (IN, OUT). -
Page 36: Error Codes
13 Error codes Proceed as follows: Additional user messages may ap- NOTE Switch off the device using the device switch. pear on the display during com- Take corrective measures missioning. Follow the instructions shown. Restart the device An error during operation is indicated by an error message on the display. - Page 37 “Wait”. If the system test was unsuccessful, can be performed only once the system test has been completed switch the C 6000 off and on again. successfully. If the system test is unsuccessful again, please contact IKA Service de- partment.
- Page 38 If the system test was unsuccessful, ed successfully. switch the C 6000 off and on again. If the system test is unsuccessful again, please contact IKA Service de- partment. E24: The stability criterion for the reg- Acknowledge the error message to...
- Page 39 Display Message Cause Remedial action E34: When activating the sample rack Remove all crucibles from the sample Invalid initial sample rack an assignment was found that no rack and reset the occupation. occupation. longer corresponds to the saved Measurements prepared assignment.
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Page 40: Accessories And Consumables
C 12 A Combustion bag, 70 x 40 mm (100 x) C 12 Combustion bag, 40 x 35 mm (100 x) AOD 1.11 Control standard for sulphur and chlorine AOD 1.12 Control standard for fluorine and bromine For further accessories see www.ika.com... -
Page 41: Technical Data
15 Technical data IKA C 6000 global IKA C 6000 isoberibol standards Measuring range max. 40000 Measuring mode adiabatic 22 °C Measuring mode dynamic 22 °C Measuring mode isoperibol 22 °C Measuring mode adiabatic 25 °C Measuring mode dynamic 25 °C Measuring mode isoperibol 25 °C... - Page 42 IKA C 6000 global IKA C 6000 isoberibol standards Evaluation as per DIN EN 15170 Evaluation as per DIN EN 14918 Evaluation as per ASTM D240 Evaluation as per ASTM D4809 Evaluation as per ASTM D1989 Evaluation as per ASTM D5865...
- Page 44 IKA-Werke GmbH & Co.KG Janke & Kunkel-Str. 10 D-79219 Staufen Tel. +49 7633 831-0 Fax +49 7633 831-98 sales@ika.de www.ika.com 20010627a...
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