Endress+Hauser analytikjena multi N/C pharma HT Operating Manual page 4

Table of contents
3.8 System suitability test....................................................................................................................................... 34
4 Installation and commissioning ..................................................................................................................................... 36
4.1 Installation conditions ...................................................................................................................................... 36
4.1.1 Ambient conditions .......................................................................................................................................... 36
4.1.2 Device layout and space requirements ............................................................................................................ 36
4.1.3 Power supply..................................................................................................................................................... 37
4.1.4 Gas supply ......................................................................................................................................................... 37
4.2 Unpacking and setting up the device............................................................................................................... 37
4.2.1 Installing and commissioning the analyzer..................................................................................................... 38
4.3 Connecting accessories..................................................................................................................................... 41
4.3.1 The AS 10e and AS 21hp autosamplers ......................................................................................................... 41
4.3.2 AS vario autosampler ...................................................................................................................................... 48
4.3.3 EPA Sampler .................................................................................................................................................... 54
4.3.4 Chemiluminescence detector (CLD)................................................................................................................. 59
4.3.5 Integrated solids module.................................................................................................................................. 60
5 Operation ........................................................................................................................................................................ 65
5.1 General notes.................................................................................................................................................... 65
5.2 Switching on the analyzer ................................................................................................................................ 66
5.3 Switching off the analyzer................................................................................................................................ 67
5.4 Carrying out calibration .................................................................................................................................... 68
5.4.1 Preparing and starting calibration................................................................................................................... 68
5.4.2 Displaying the calibration results..................................................................................................................... 70
5.4.3 Editing calibration ............................................................................................................................................ 71
5.4.4 Linking a calibration to a method.................................................................................................................... 71
5.4.5 Managing calibration data............................................................................................................................... 73
5.5 Performing measurements .............................................................................................................................. 73
5.5.1 Measurement with manual sample feed ........................................................................................................ 73
5.5.2 Measurement with autosampler ..................................................................................................................... 74
5.6 Operating the integrated solids module ......................................................................................................... 75
6 Maintenance and care.................................................................................................................................................... 77
6.1 Maintenance overview ..................................................................................................................................... 77
6.2 Adjustment and setting.................................................................................................................................... 78
6.2.1 General notes for adjusting the autosampler ................................................................................................. 78
6.2.2 Adjusting the AS vario autosampler ................................................................................................................ 79
6.2.3 Adjusting the EPA Sampler .............................................................................................................................. 80
6.2.4 Setting the NPOC purge flow ........................................................................................................................... 83
6.3 Syringe pump maintenance ............................................................................................................................. 85
6.4 Replacing the pump hose................................................................................................................................. 85
6.5 Replacing the hose connections ...................................................................................................................... 87
6.6 Checking the system for leaks.......................................................................................................................... 88
6.7 Replacing the catalyst....................................................................................................................................... 89
6.7.1 Removing the combustion tube....................................................................................................................... 89
6.7.2 Filling the combustion tube ............................................................................................................................. 90
6.7.3 Installing the combustion tube ........................................................................................................................ 92
6.8 Removing and installing the combustion furnace .......................................................................................... 94
6.8.1 Removing the combustion furnace.................................................................................................................. 94
6.8.2 Installing the combustion furnace ................................................................................................................... 95
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multi N/C pharma HT