Endress+Hauser Analytik Jena multi N/C 2100S Operating Manual page 4

Contents
4
4.1.3 Energy supply .................................................................................................................. 42
4.1.4 Gas supply ........................................................................................................................ 42
4.2 Unpacking and placing the analyzer ............................................................................... 42
5 Connecting add-on devices ...................................................................................... 43
5.1 Autosampler AS 60 ......................................................................................................... 43
5.2 Chemiluminescence detector (CLD) ................................................................................ 45
5.3 External solids module HT 1300 (not for multi N/C 2100S pharma) .......................... 47
6 Operation ................................................................................................................. 48
6.1 General information for the analysis work ..................................................................... 48
6.2 Switching on the analyzer (standard commissioning) ................................................... 48
6.3 Carrying out the calibration ............................................................................................ 50
6.3.1 Preparing and starting the calibration ............................................................................ 50
6.3.2 Displaying calibration results .......................................................................................... 53
6.3.3 Editing an existing calibration ........................................................................................ 55
6.3.4 Linking calibration parameters to a method .................................................................. 56
6.3.5 Managing calibration data .............................................................................................. 58
6.4 Performing measurements ............................................................................................. 60
6.4.1 Measurement with manual sample supply .................................................................... 60
6.4.2 Measurement with sampler ............................................................................................ 61
7 Maintenance and care .............................................................................................. 63
7.1 Maintenance intervals..................................................................................................... 63
7.2 Adjustment and setup tasks ............................................................................................ 65
7.2.1 Adjust autosampler ......................................................................................................... 65
7.2.2 Adjust the NPOC purging flow (not for multi N/C 2100S pharma) .............................. 68
7.3 Replacing the water traps ............................................................................................... 69
7.4 Replacing the halogen trap ............................................................................................. 72
7.5 Exchanging the catalyst .................................................................................................. 73
7.5.1 Lifetime of the catalyst .................................................................................................... 73
7.5.2 Removing the combustion tube ...................................................................................... 73
7.5.3 Filling the combustion tube ............................................................................................ 75
7.5.4 Inserting the combustion tube ........................................................................................ 76
7.6 Regenerating the TIC reactor .......................................................................................... 78
7.7 Maintaining the TIC condensate container and condensation coil ............................... 79
7.7.1 Removing and cleaning the TIC condensate container and condensation coil ............. 79
7.7.2 Installing the TIC condensate container and condensation coil .................................... 81
7.8 Removing and installing the combustion furnace .......................................................... 83
7.8.1 Removing the combustion furnace ................................................................................. 83
7.8.2 Installing the combustion furnace .................................................................................. 84
7.9 Removing and replacing the pump hose ........................................................................ 85
7.10 Replacing the hose connections ..................................................................................... 88
7.11 Checking the system for tightness .................................................................................. 89
7.12 Replacing the septa ......................................................................................................... 90
8 Fault removal ........................................................................................................... 91
8.1 General information ........................................................................................................ 91
8.2 Error messages in multiWin ............................................................................................ 92
8.3 Status errors - indications in the window System state ................................................ 96
8.4 Equipment faults and analytical problems ..................................................................... 98
9 Transport and storage ............................................................................................ 103
9.1 Transport ....................................................................................................................... 103
9.1.1 Preparing the analyzer for transport ............................................................................ 103
9.1.2 Transport notes ............................................................................................................. 104
9.1.3 Moving the analyzer in the laboratory ......................................................................... 104
9.2 Storage ........................................................................................................................... 105
9.3 Recommissioning after transport or storage ................................................................ 105
multi N/C 2100S