TELEDYNE API T108 Series Addendum To Operational Manual

TELEDYNE API T108 Series Addendum To Operational Manual

Total-sulfides-in-co2 analyzer with model 501ts thermal converter total-sulfides-in-co2 analyzer with model 501ts thermal converter

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TOTAL-SULFIDES-IN-CO
WITH MODEL 501TS THERMAL CONVERTER
Addendum to T100 Operation Manual, PN 06807
(when used in conjunction with both the T100 manual, PN 06807, and
Copyright 2011-2020
Teledyne API
MODEL T108
Also supports operation of:
Model T108U Analyzer
the T100U addendum, PN 06840)
© TELEDYNE API (TAPI)
9970 Carroll Canyon Road
SAN DIEGO, CA 92131-1106
USA
Toll-free Phone: 800-324-5190
Phone: +1 858-657-9800
Fax: +1 858-657-9816
Email:
api-sales@teledyne.com
Website: http://www.teledyne-api.com/
ANALYZER
2
07268C DCN8258
05 October 2020

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Summary of Contents for TELEDYNE API T108 Series

  • Page 1 Also supports operation of: Model T108U Analyzer (when used in conjunction with both the T100 manual, PN 06807, and the T100U addendum, PN 06840) © TELEDYNE API (TAPI) 9970 Carroll Canyon Road SAN DIEGO, CA 92131-1106 Toll-free Phone: 800-324-5190 Phone: +1 858-657-9800...
  • Page 3 ABOUT THIS MANUAL This T108 addendum is to be used in conjunction with the T100 operation manual. It also supports the T108U analyzer when used in conjunction with both the T100 manual and the T100U manual. Note We recommend that all users read this manual in its entirety before operating the instrument.
  • Page 4 Teledyne API – Model T108 Addendum to T100 Manual This page intentionally left blank. 07268C DCN8258...
  • Page 5: Table Of Contents

    TABLE OF CONTENTS INTRODUCTION ....................5 1.1. Specifications ....................5 1.2. The T108 Total-Sulfides-in-CO Analyzer ............. 5 1.3. Configurations ....................6 1.4. The 501TS – Total Reduced Sulfur Converter ..........10 1.4.1. Heater Characteristics and Control ..............10 1.5. Installation ....................12 1.6.
  • Page 6 Teledyne API – Model T108 Addendum to T100 Manual This page intentionally left blank. 07268C DCN8258...
  • Page 7: Introduction

    (178mm x 432mm x 559mm) 1.2. THE T108 TOTAL-SULFIDES-IN-CO ANALYZER The Teledyne API Model T108 Total Sulfides in CO Analyzer, is designed to measure mixed sulfur impurities, collectively referred to as Total Sulfides (TS), in carbon dioxide (CO ) gas. Since there is no...
  • Page 8: Configurations

    Introduction Teledyne API – Model T108 Addendum to T100 Manual Since the gas being analyzed is essentially CO , which generally contains no oxygen, the analyzer includes an oxygenator to add approximately 6% oxygen to the sample before it passes through the converter.
  • Page 9: Figure 1-1. Basic Pneumatics Configuration

    Teledyne API – Model T108 Addendum to T100 Manual Introduction Figure 1-1. Basic Pneumatics Configuration 07268C DCN8258...
  • Page 10: Figure 1-2. Pneumatics With Izs/Permeation Tube Option

    Introduction Teledyne API – Model T108 Addendum to T100 Manual Figure 1-2. Pneumatics with IZS/Permeation Tube Option 07268C DCN8258...
  • Page 11: Figure 1-3. Pneumatics With 702 Calibrator Option

    Teledyne API – Model T108 Addendum to T100 Manual Introduction Figure 1-3. Pneumatics with 702 Calibrator Option 07268C DCN8258...
  • Page 12: The 501Ts - Total Reduced Sulfur Converter

    Introduction Teledyne API – Model T108 Addendum to T100 Manual 1.4. THE 501TS – TOTAL REDUCED SULFUR CONVERTER The 501TS oxidizes reduced sulfur compounds to SO in a high temperature quartz oven. 1.4.1. Heater Characteristics and Control A front-panel-mounted, programmable digital temperature controller regulates power to the heater.
  • Page 13: Figure 1-4. 501Ts Converter Chassis Layout

    Teledyne API – Model T108 Addendum to T100 Manual Introduction Figure 1-4. 501TS Converter Chassis Layout 07268C DCN8258...
  • Page 14: Installation

    Introduction Teledyne API – Model T108 Addendum to T100 Manual 1.5. INSTALLATION The T108 consists of two chassis: the analyzer and the converter. There is a power cord for each that should be plugged into the correct AC mains receptacle. See the model label on the rear panel of each chassis for the voltage and frequency configuration.
  • Page 15: Operation And Calibration

    Teledyne API – Model T108 Addendum to T100 Manual Introduction Figure 1-5. T108-to-501TS Rear Panel Pneumatic Connections 1.6. OPERATION AND CALIBRATION Refer to the T100 manual for the overall operation of the SO analyzer. This unit has some unique operating characteristics and calibration procedures detailed below.
  • Page 16: Ts And Zero Air Scrubbers

    Introduction Teledyne API – Model T108 Addendum to T100 Manual 1.6.1. CO Source A source of CO that is free of sulfides is required for accurate zero calibration of the instrument. If the ‘zero gas’ used to zero the instrument is contaminated, the process gas will read artificially low, sometimes even showing a negative TS concentration.
  • Page 17: Troubleshooting And Service

    2. TROUBLESHOOTING AND SERVICE NO POWER: Plugged in? Switched on? Circuit breaker tripped? NOT HEATING: View the PV value. Is it heating? Socket in place on back of temperature controller? Check 501TS wiring diagram in Appendix A. Thermocouple failed? Check that its leads are securely connected to the wiring block at the back of the controller.
  • Page 18: So Analyzer Maintenance

    Troubleshooting and Service Teledyne API – Model T108 Addendum to T100 Manual 2.1 SO ANALYZER MAINTENANCE Maintenance of the SO analyzer is covered in the Maintenance section of its respective manual. Unlike the T100, the T108 has one standard charcoal scrubber on the rear panel of the SO analyzer instrument chassis, and another special charcoal scrubber inside the chassis.
  • Page 19: Sample Diluter Maintenance

    Teledyne API – Model T108 Addendum to T100 Manual Troubleshooting and Service use it to measure CO flow. Or use a flowmeter such as a soap bubble, or BIOS – DryCal flowmeter that measures volume flow 2. Allow the T108 to stabilize at span for at least 30 minutes.
  • Page 20: Thermocouple Replacement

    Troubleshooting and Service Teledyne API – Model T108 Addendum to T100 Manual 2.5 THERMOCOUPLE REPLACEMENT Continuous operation at 1000 ºC will eventually degrade the performance of the thermocouple used to sense the temperature of the quartz oven. The following instructions describe how to install a new thermocouple into the Converter Heater Block.
  • Page 21: Figure 2-5. Quartz Tube Cavity For Thermocouple

    Teledyne API – Model T108 Addendum to T100 Manual Troubleshooting and Service 10. In for installing the new thermocouple, look into the end of the Heater Block. You will preparation see that there is an indentation (cavity) in the fat part of the quartz tube. This is where the thermocouple you are installing will reside.
  • Page 22: Technical Support

    Apply power now. The converter is now ready for operation. 2.6 TECHNICAL SUPPORT For Technical Assistance regarding the use and maintenance of this instrument or any other Teledyne API product, contact Teledyne API’s Technical Support Department: Telephone: 800-324-5190 Email: api-techsupport@teledyne.com or access any of the service options on our website at http://www.teledyne-api.com/...
  • Page 23: Instrument Test & Calibration Record

    Teledyne API – Model T108 Addendum to T100 Manual Instrument Test & Calibration Record 3. INSTRUMENT TEST & CALIBRATION RECORD For T108 test and calibration information, refer to Table 3-1. For T108U test and calibration information, refer to Table 3-2.
  • Page 24: Table 3-2. Test And Calibration Values For T108U

    Instrument Test & Calibration Record Teledyne API – Model T108 Addendum to T100 Manual Table 3-2. Test and Calibration Values for T108U TEST OBSERVED UNITS ACCEPTABLE VALUE(S) PARAMETERS VALUE RANGE 5 - 20,000 STAB1 ≤0.05 ppb with zero air STAB2 ≤0.1 ppb with zero air...
  • Page 25: Table 3-3. Test And Calibrations Values W/ Co2 Where Applicable

    Teledyne API – Model T108 Addendum to T100 Manual Instrument Test & Calibration Record Table 3-3. Test and Calibrations Values w/ CO2 where applicable Span and Cal Values Acceptable Value Parameter Observed Value Units Nominal Range TS Span Conc. 20 - 20,000 TS Slope 1.0 +/- .3...
  • Page 26 Appendix A - Model 501 Interconnects 07268C DCN8258...

This manual is also suitable for:

T108u

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